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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ #======================================================================= data_I #======================================================================= _audit_creation_method 'Jana2006 Version : 09/09/2010' _journal_name_full 'Inorganic Chemistry' _journal_year 2011 _journal_volume 50 _journal_page_first 3743 _journal_page_last 3751 _journal_paper_doi https://dx.doi.org/10.1021/ic200102z _publ_section_title ;An Incommensurately Modulated Structure of \h'-Phase of Cu~3+x~Si Determined by Quantitative Electron Diffraction Tomography ; _publ_contact_author_name 'Palatinus, Lukas' _publ_contact_author_address ;Institute of Physics of the AS CR v.v.i. Na Slovance 2 182 21 Prague Czechia ; _publ_contact_author_email palat@fzu.cz loop_ _publ_author_name _publ_author_address 'Palatinus, Lukas' ;Institute of Physics of the AS CR v.v.i. Na Slovance 2 182 21 Prague Czechia ; 'Klementova, Mariana' ;Institute of Physics of the AS CR v.v.i. Na Slovance 2 182 21 Prague Czechia Institute of Inorganic Chemistry of the AS CR v.v.i. 250 68 Husinec-Rez 1001 Czechia ; 'Drinek, Vladislav' ;Institute of Chemical Process Fundamentals of the AS CR v.v.i. Rozvojova 135 165 02 Prague 6 Czechia ; 'Petricek, Vaclav' ;Institute of Physics of the AS CR v.v.i. Na Slovance 2 182 21 Prague Czechia ; _publ_section_references ; Petricek, V., Dusek, M. & Palatinus L. (2006). Jana2006. Structure Determination Software Programs. Institute of Physics, Praha, Czech Republic. Palatinus L. & Chapuis G. (2007). J. Appl. Cryst. 40, 786-790. ; # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_formula_sum 'Cu6.626 Ge1 Si1' _chemical_formula_weight 524.3 #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system trigonal _space_group_name_H-M_alt 'P -3 1 m' _space_group_name_Hall '-P 3;-2' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -y,x-y,z 3 -x+y,-x,z 4 -y,-x,-z 5 -x+y,y,-z 6 x,x-y,-z 7 -x,-y,-z 8 y,-x+y,-z 9 x-y,x,-z 10 y,x,z 11 x-y,-y,z 12 -x,-x+y,z _cell_length_a 16.4336 _cell_length_b 16.4336 _cell_length_c 22.2284 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_volume 5198.813 _cell_formula_units_Z 48 _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _cell_measurement_temperature 293 _exptl_crystal_type_of_structure cryst _exptl_crystal_density_diffrn 8.0363 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 11392 _exptl_absorpt_coefficient_mu 0 _exptl_crystal_description ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_size_rad ? _exptl_crystal_colour ? _exptl_absorpt_correction_type ? _exptl_absorpt_process_details ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _diffrn_ambient_temperature 293 _diffrn_radiation_type electrons _diffrn_radiation_wavelength 0.0335 _diffrn_measurement_device 'transmission electron microscope' _diffrn_measurement_device_type 'Philips CM120' _diffrn_measurement_method '\o-scan' _diffrn_reflns_number 6383 _diffrn_reflns_av_R_equivalents 0.1675 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 19 #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_type_symbol Cu Si Ge _refine_special_details ;Tables with modulated positions of individual atoms as function of the modulation phase are available in the supporting information. ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0 0 0.333171 Uiso 0.0253 2 1 d . . . Cu2 Cu 0.25011 0 0.334318 Uiso 0.0253 6 1 d . . . Cu3 Cu 0.666667 0.333333 0.378308 Uiso 0.0253 4 1 d . . . Cu4 Cu 0.248657 0 -0.000352 Uiso 0.0253 6 1 d . . . Cu5 Cu 0 0 0 Uiso 0.0253 1 1 d . . . Cu6 Cu 0.418373 0.08899 0.044374 Uiso 0.0253 12 1 d . . . Cu7 Cu 0.489811 0.244718 0.219169 Uiso 0.0253 12 1 d . . . Cu8 Cu 0.243058 0 0.447464 Uiso 0.0253 6 1 d . . . Cu9 Cu 0.424192 0.087655 0.289583 Uiso 0.0253 12 1 d . . . Cu10 Cu 0.666667 0.333333 0.062011 Uiso 0.0253 4 1 d . . . Cu11 Cu 0.608103 0.215346 0.279012 Uiso 0.0253 12 1 d . . . Cu12 Cu 0.32219 0.162002 0.280357 Uiso 0.0253 12 1 d . . . Cu13 Cu 0.509013 0 0.449433 Uiso 0.0253 6 1 d . . . Cu14 Cu 0.757182 0 0.11567 Uiso 0.0253 6 1 d . . . Cu15 Cu 0.744047 0 0.334042 Uiso 0.0253 6 1 d . . . Cu16 Cu 0.38176 0.38176 0.058 Uiso 0.0253 6 1 d . . . Cu17 Cu 0.563387 0.155446 0.383218 Uiso 0.0253 12 1 d . . . Cu18 Cu 0.596138 0.155284 0.05802 Uiso 0.0253 12 1 d . . . Cu19 Cu 0.491388 -0.000057 0.113798 Uiso 0.0253 6 1 d . . . Cu20 Cu 0.672846 0.088488 0.394624 Uiso 0.0253 12 1 d . . . Cu21 Cu 0.5 0 0 Uiso 0.0253 3 1 d . . . Cu22 Cu 0.789248 0.150886 0.056136 Uiso 0.0253 12 1 d . . . Cu23 Cu 0.662381 0.087157 0.271972 Uiso 0.0253 12 1 d . . . Cu24 Cu 0.497443 0.251187 0.33387 Uiso 0.0253 12 1 d . . . Cu25 Cu 0 0 0.217586 Uiso 0.0253 2 1 d . . . Cu26 Cu 0.506726 0 0.333164 Uiso 0.0253 6 1 d . . . Cu27 Cu 0.504767 0.244834 0.116942 Uiso 0.0253 12 1 d . . . Cu28 Cu 0.50866 0.25433 0 Uiso 0.0253 6 1 d . . . Cu29 Cu 0.365017 0.149928 0.385542 Uiso 0.0253 12 1 d . . . Cu30 Cu 0.174524 0.089073 0.374382 Uiso 0.0253 12 1 d . . . Cu31 Cu 0.740448 0.24754 0.44711 Uiso 0.0253 12 1 d . . . Cu32 Cu 0.169442 0.082826 0.054615 Uiso 0.0253 12 1 d . . . Cu33 Cu 0.38748 0 0.387659 Uiso 0.0253 6 1 d . . . Cu34 Cu 0.497148 0 0.217808 Uiso 0.0253 6 1 d . . . Cu35 Cu 0.743559 0 0.212844 Uiso 0.0253 6 1 d . . . Cu36 Cu 0.751528 0 0.455091 Uiso 0.0253 6 1 d . . . Cu37 Cu 0.258169 0 0.218636 Uiso 0.0253 6 1 d . . . Cu38 Cu 0.251815 0 0.117324 Uiso 0.0253 6 1 d . . . Cu39 Cu 0 0 0.111111 Uiso 0.0253 2 1 d . . . Cu40 Cu 0 0 0.444444 Uiso 0.0253 2 1 d . . . Cu41 Cu 0.8495 0 0.27777 Uiso 0.0253 6 1 d . . . Cu42 Cu 0.85938 0.85938 0.2805 Uiso 0.0253 6 1 d . . . Si1 Si 0.666667 0.333333 0.5 Uiso 0.0253 2 0.5 d . . . Si2 Si 0.666667 0.333333 0.181976 Uiso 0.0253 4 0.5 d . . . Si3 Si 0.419396 0.085553 0.16701 Uiso 0.0253 12 0.5 d . . . Si4 Si 0.420184 0.086704 0.484051 Uiso 0.0253 12 0.5 d . . . Si5 Si 0.664656 0.086741 0.151297 Uiso 0.0253 12 0.5 d . . . Si6 Si 0.168749 0.084364 0.5 Uiso 0.0253 6 0.5 d . . . Si7 Si 0.171111 0.084955 0.176012 Uiso 0.0253 12 0.5 d . . . Si8 Si 0.333641 0.166623 0.158779 Uiso 0.0253 12 0.5 d . . . Si9 Si 0.338245 0.169399 0.5 Uiso 0.0253 6 0.5 d . . . Si10 Si 0.59 0.162 0.1666 Uiso 0.038 12 0.5 d . . . Si11 Si 0.164535 0.582268 0.5 Uiso 0.0253 6 0.5 d . . . Ge1 Ge 0.666667 0.333333 0.5 Uiso 0.0253 2 0.5 d . . . Ge2 Ge 0.666667 0.333333 0.181976 Uiso 0.0253 4 0.5 d . . . Ge3 Ge 0.419396 0.085553 0.16701 Uiso 0.0253 12 0.5 d . . . Ge4 Ge 0.420184 0.086704 0.484051 Uiso 0.0253 12 0.5 d . . . Ge5 Ge 0.664656 0.086741 0.151297 Uiso 0.0253 12 0.5 d . . . Ge6 Ge 0.168749 0.084364 0.5 Uiso 0.0253 6 0.5 d . . . Ge7 Ge 0.171111 0.084955 0.176012 Uiso 0.0253 12 0.5 d . . . Ge8 Ge 0.333641 0.166623 0.158779 Uiso 0.0253 12 0.5 d . . . Ge9 Ge 0.338245 0.169399 0.5 Uiso 0.0253 6 0.5 d . . . Ge10 Ge 0.59 0.162 0.1666 Uiso 0.0253 12 0.5 d . . . Ge11 Ge 0.164535 0.582268 0.5 Uiso 0.0253 6 0.5 d . . . # # h, k, l, m1, m2, Fo, phase determined ab initio by charge flipping # loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_index_m_2 _refln_F_meas _refln_phase_calc 0 1 0 -2 -1 95.12 180 0 0 1 1 0 41.88 180 0 1 1 -2 0 19.18 0 0 1 2 -2 -2 27.73 0 0 1 1 -1 -1 20.24 0 0 0 0 2 1 77.70 0 0 1 2 -1 0 88.13 180 0 0 1 2 2 7.20 0 0 0 3 2 1 18.19 0 0 1 0 -1 1 15.25 180 0 0 2 2 0 11.73 0 1 1 1 -2 0 9.39 180 -1 2 2 -2 -2 22.35 180 0 1 0 0 0 332.48 0 0 1 3 -1 1 38.57 0 0 1 3 -1 -2 30.37 0 1 1 4 -2 0 19.41 180 0 1 1 0 1 10.06 0 0 1 3 0 0 98.78 180 0 1 2 0 -1 45.63 180 -1 2 0 -1 -2 48.59 0 0 0 5 2 0 0.00 0 -1 2 3 -1 -2 4.56 0 1 1 3 -1 1 14.96 0 0 1 4 0 1 68.64 0 0 2 0 -2 -1 96.53 0 0 1 1 0 -2 0.63 180 -1 2 1 -1 -1 110.75 180 0 1 2 0 2 15.50 180 0 1 5 0 -1 129.69 180 0 2 1 -2 0 27.74 180 1 1 2 -1 0 289.94 0 0 2 3 -2 -1 144.90 0 0 2 2 -2 -2 18.24 180 0 1 1 1 0 5.95 0 0 1 2 1 1 284.42 180 0 1 4 0 -2 6.88 0 -1 2 4 -1 -1 300.82 180 0 2 4 -2 0 18.98 0 0 1 0 1 2 49.65 180 1 1 6 -1 1 99.30 0 -1 2 1 0 -2 21.45 0 0 1 4 1 0 139.42 0 0 1 5 0 2 5.42 180 1 1 2 0 2 9.09 0 1 1 5 -1 0 491.05 0 0 2 5 -2 -2 16.12 180 1 1 1 0 1 38.56 0 0 1 3 1 2 160.02 0 0 1 3 1 -1 121.48 0 0 2 6 -2 -1 73.54 180 0 1 5 1 1 85.49 0 -1 2 2 0 -1 253.27 0 -1 2 4 0 -2 2.97 180 0 2 1 -1 -1 46.72 180 0 2 2 -1 0 612.26 180 1 1 4 0 1 294.13 180 1 1 5 0 2 0.00 0 0 1 7 0 -2 6.24 0 0 1 0 2 1 105.17 180 -1 2 0 0 0 878.36 0 0 2 0 -1 1 38.56 180 -1 2 5 0 -1 319.25 0 0 2 4 -1 -1 472.33 0 0 1 7 1 0 147.30 0 0 1 6 1 2 216.79 0 0 1 6 1 -1 223.44 0 0 1 1 2 2 0.00 0 0 1 3 2 1 194.46 0 -1 2 3 0 0 177.69 0 1 1 3 0 0 187.01 0 0 1 2 2 0 9.57 0 0 2 3 -1 -2 158.35 0 0 2 3 -1 1 30.42 0 0 2 5 -1 0 335.27 180 1 2 1 -2 0 3.78 0 -1 3 2 -2 -2 66.61 0 -1 2 7 0 -2 41.69 180 -1 2 0 1 -1 18.74 0 0 1 4 2 2 0.00 0 1 1 7 0 1 482.42 180 1 2 4 -2 0 8.69 180 -1 2 3 1 -1 78.02 0 1 1 3 1 2 59.42 0 0 1 5 2 0 0.00 0 -1 3 0 -2 -1 59.48 180 0 1 6 2 1 116.17 0 -1 2 6 0 0 209.23 0 1 1 6 0 0 274.57 0 -1 2 1 1 0 4.52 180 0 2 7 -1 -1 385.18 0 -1 3 5 -2 -2 15.55 0 0 2 6 -1 -2 81.21 0 0 2 6 -1 1 74.71 0 0 2 0 0 0 546.33 0 1 1 2 1 1 128.12 0 -1 3 3 -2 -1 6.40 180 1 2 3 -2 -1 63.69 180 0 2 1 0 1 7.43 0 0 2 3 0 0 150.04 0 0 2 2 0 -1 51.58 180 -1 2 4 1 0 53.46 180 0 1 9 1 -1 22.71 0 0 2 8 -1 0 70.69 180 0 1 7 2 2 2.41 0 -1 2 6 1 -1 78.94 0 1 1 6 1 2 50.98 0 1 1 5 1 1 44.18 0 0 2 4 0 1 41.04 0 1 2 7 -2 0 0.00 0 -1 3 0 -1 -2 77.57 180 1 1 1 1 0 3.57 180 0 2 1 0 -2 0.00 0 -1 2 2 1 1 62.76 180 0 1 8 2 0 0.65 0 -1 3 6 -2 -1 42.86 0 1 2 6 -2 -1 42.80 0 0 2 2 0 2 23.75 0 0 2 5 0 -1 71.73 180 -1 3 1 -2 0 0.00 0 -1 3 3 -1 -2 10.82 0 1 2 3 -1 1 1.61 0 1 2 2 -2 -2 14.90 0 0 2 6 0 0 213.90 0 -1 3 8 -2 -2 5.89 180 -1 3 1 -1 -1 8.13 0 1 1 4 1 0 60.91 180 0 1 9 2 1 9.03 180 1 1 9 0 0 278.71 0 1 2 2 -1 0 223.91 180 0 2 4 0 -2 1.25 180 0 2 9 -1 -2 62.84 0 0 3 0 -2 -1 100.80 0 -1 2 7 1 0 45.88 180 1 1 1 2 2 0.00 0 -1 3 4 -2 0 5.27 180 -1 2 2 2 0 2.20 0 -1 2 5 1 1 67.66 180 0 2 5 0 2 2.10 180 0 3 1 -2 0 7.86 180 0 3 3 -2 -1 53.64 0 -1 3 4 -1 -1 104.95 0 0 2 7 0 1 165.04 0 1 2 5 -2 -2 0.00 0 0 3 2 -2 -2 40.86 180 -1 3 6 -1 -2 7.23 0 1 2 6 -1 1 35.84 0 1 1 8 1 1 34.71 0 1 1 4 2 2 0.00 0 -1 2 9 1 -1 27.47 180 1 1 9 1 2 13.09 180 1 2 5 -1 0 57.69 0 0 2 1 1 0 0.00 0 -1 2 0 2 1 0.00 0 0 2 2 1 1 122.11 180 0 3 4 -2 0 7.43 180 1 2 1 -1 -1 32.87 0 -1 2 5 2 0 0.00 0 0 2 8 0 -1 0.00 0 -1 3 2 -1 0 103.51 180 1 1 7 1 0 116.44 180 1 2 10 -2 0 21.08 180 -1 2 3 2 1 4.05 0 1 1 3 2 1 11.53 0 1 2 9 -2 -1 37.03 0 0 2 7 0 -2 0.00 0 0 3 5 -2 -2 25.78 180 0 2 0 1 2 21.37 180 0 2 4 1 0 16.90 0 -1 3 7 -2 0 0.00 0 0 2 9 0 0 784.89 0 0 3 6 -2 -1 22.05 0 1 2 4 -1 -1 36.88 0 0 2 3 1 -1 64.83 0 0 2 3 1 2 72.60 0 -1 3 7 -1 -1 87.66 180 -1 2 8 1 1 0.00 0 0 2 5 1 1 51.82 180 -1 3 1 0 -2 0.00 0 0 2 8 0 2 0.00 0 1 2 2 0 2 4.49 0 -1 3 5 -1 0 113.30 0 1 1 7 2 2 1.05 0 1 2 8 -2 -2 0.00 0 1 2 1 0 1 9.06 180 -1 3 2 0 -1 263.20 180 0 3 7 -2 0 7.62 0 1 2 8 -1 0 19.69 180 -1 2 6 2 1 4.60 0 1 1 6 2 1 1.07 0 -1 2 1 2 2 0.53 0 -1 3 4 0 -2 20.41 180 -1 3 9 -1 -2 55.40 0 1 2 9 -1 1 18.17 0 1 1 2 2 0 1.78 180 -1 3 0 -1 1 52.84 180 -1 2 8 2 0 0.00 0 1 2 4 0 1 175.80 0 0 2 7 1 0 165.99 0 1 2 5 0 2 0.00 0 2 2 1 -2 0 24.19 180 0 2 6 1 2 5.26 0 0 2 6 1 -1 54.19 0 0 3 8 -2 -2 10.29 0 1 2 7 -1 -1 149.01 180 -2 4 2 -2 -2 172.12 180 -1 3 0 0 0 73.68 0 1 1 11 1 1 135.11 0 0 3 1 -1 -1 20.89 180 -1 3 3 -1 1 4.09 0 1 2 3 -1 -2 31.89 0 -1 2 4 2 2 0.00 0 -1 3 5 0 -1 193.57 180 0 3 2 -1 0 100.94 180 1 1 10 1 0 1.58 0 -1 3 3 0 0 46.30 180 1 2 3 0 0 39.38 180 0 3 9 -2 -1 65.69 180 1 1 5 2 0 0.00 0 0 2 10 0 -2 0.00 0 0 2 8 1 1 10.85 0 0 2 11 0 -1 253.06 180 2 2 4 -2 0 113.65 0 0 3 0 -1 1 73.27 0 -1 3 8 -1 0 6.64 180 0 3 4 -1 -1 191.44 180 0 2 0 2 1 13.17 180 -1 3 7 0 -2 4.82 0 -2 4 5 -2 -2 158.95 180 0 3 3 -1 1 15.85 0 0 3 3 -1 -2 28.28 0 0 3 5 -1 0 347.91 0 0 2 1 2 2 0.00 0 0 2 3 2 1 84.44 0 1 2 7 0 1 277.54 0 -1 3 6 -1 1 39.22 0 1 2 6 -1 -2 16.54 0 0 2 2 2 0 0.00 0 1 1 10 2 2 2.40 0 -1 2 9 2 1 71.96 180 1 1 9 2 1 70.49 180 -1 2 7 2 2 0.00 0 1 2 8 0 2 21.35 0 1 2 11 -2 -2 5.34 0 0 3 10 -2 0 0.00 0 1 3 1 -2 0 2.50 0 -1 3 6 0 0 69.92 0 1 2 6 0 0 79.92 0 -1 3 1 0 1 0.00 0 -1 4 2 -2 -2 132.11 0 1 2 2 0 -1 100.08 180 0 2 4 2 2 0.00 0 0 2 9 1 -1 10.88 180 0 2 9 1 2 13.17 0 -1 3 8 0 -1 0.00 0 1 2 11 -1 0 251.39 180 2 2 7 -2 0 125.07 0 -2 4 0 -1 -2 208.95 0 0 2 10 1 0 0.00 0 0 3 7 -1 -1 588.21 180 -1 3 0 1 -1 31.95 180 1 1 8 2 0 0.00 0 0 2 5 2 0 1.05 0 0 3 6 -1 1 58.75 0 0 3 6 -1 -2 13.48 0 1 2 10 -1 -1 11.49 180 1 3 4 -2 0 83.97 180 -1 3 4 0 1 58.04 0 0 2 6 2 1 206.07 0 -2 4 3 -1 -2 121.27 0 2 2 3 -1 1 81.93 0 -1 4 0 -2 -1 189.58 180 0 3 11 -2 -2 53.74 0 -1 3 3 1 -1 52.35 0 1 2 3 1 2 134.13 0 -2 4 8 -2 -2 0.00 0 -1 4 5 -2 -2 123.34 0 1 2 5 0 -1 23.61 180 0 3 8 -1 0 12.98 0 -1 4 3 -2 -1 55.91 180 1 3 3 -2 -1 4.73 180 -1 3 1 1 0 1.88 0 0 2 11 1 1 68.18 180 1 2 2 1 1 76.52 0 -1 3 10 0 -2 0.00 0 0 3 12 -2 -1 12.40 180 1 2 9 -1 -2 53.80 0 -1 3 9 -1 1 41.01 0 0 2 7 2 2 0.00 0 0 3 0 0 0 1076.20 0 1 2 10 0 1 42.18 0 0 2 13 0 -2 0.00 0 -1 3 4 1 0 15.43 0 -1 3 9 0 0 835.01 0 1 2 9 0 0 1026.10 0 -2 4 6 -1 -2 28.59 180 2 2 6 -1 1 21.97 180 1 3 7 -2 0 40.99 180 -1 3 7 0 1 107.59 0 -1 3 6 1 -1 145.75 0 1 2 6 1 2 112.05 0 -1 2 10 2 2 0.00 0 1 2 1 0 -2 0.00 0 0 3 1 0 1 1.46 0 0 3 3 0 0 143.97 0 0 2 8 2 0 0.00 0 -1 3 2 0 2 0.00 0 1 2 5 1 1 26.15 180 0 3 2 0 -1 193.98 0 -2 4 1 -1 -1 0.00 0 1 2 11 0 2 22.76 0 1 3 6 -2 -1 56.01 0 -1 4 6 -2 -1 24.99 0 -1 4 1 -2 0 4.49 0 2 2 2 -1 0 252.20 180 1 2 1 1 0 0.00 0 1 1 12 2 1 10.84 0 0 3 9 -1 1 82.25 180 0 3 9 -1 -2 70.36 180 1 3 2 -2 -2 104.22 0 2 2 10 -2 0 5.66 0 -1 3 2 1 1 173.11 0 1 1 13 2 2 0.00 0 -1 4 8 -2 -2 0.00 0 0 2 9 2 1 30.48 0 1 2 8 0 -1 13.78 0 -1 3 11 0 -1 138.95 0 0 3 10 -1 -1 14.41 180 1 2 4 0 -2 7.65 180 0 3 4 0 1 144.52 180 -2 4 4 -1 -1 61.46 180 0 2 12 1 -1 1.66 0 1 1 11 2 0 0.00 0 0 3 1 0 -2 0.68 0 -1 4 4 -2 0 66.21 180 1 2 4 1 0 46.04 180 -1 3 5 0 2 18.95 0 0 3 2 0 2 16.49 180 0 3 5 0 -1 118.69 0 -2 4 1 0 -2 4.71 0 -1 4 0 -1 -2 128.80 180 -1 3 7 1 0 177.24 0 2 2 2 0 2 45.24 180 2 2 5 -1 0 157.73 0 0 3 6 0 0 227.94 0 0 2 13 1 0 0.00 0 1 3 5 -2 -2 62.10 0 -2 4 11 -2 -2 169.18 0 -1 3 5 1 1 10.55 180 1 2 13 -1 -1 111.60 0 0 3 11 -1 0 183.44 180 -1 4 3 -1 -2 0.00 0 1 3 3 -1 1 11.38 180 0 3 4 0 -2 1.22 180 0 2 10 2 2 0.00 0 -2 4 4 0 -2 6.09 180 -2 4 9 -1 -2 175.78 180 2 2 9 -1 1 233.18 180 1 2 8 1 1 12.06 0 -1 4 1 -1 -1 37.44 180 -1 3 9 1 -1 1.75 180 1 2 9 1 2 1.43 180 0 3 5 0 2 0.72 180 1 3 2 -1 0 317.59 180 1 2 7 0 -2 9.61 0 0 3 7 0 1 209.26 180 2 2 5 0 2 28.21 180 1 3 10 -2 0 0.00 0 -1 3 0 1 2 35.57 0 -1 3 10 0 1 0.00 0 1 2 12 -1 -2 49.28 0 1 3 9 -2 -1 151.81 0 -1 4 9 -2 -1 161.01 0 -2 4 7 -1 -1 384.86 180 -1 3 13 0 -2 0.00 0 -1 4 7 -2 0 35.04 180 1 2 7 1 0 140.37 0 1 2 1 2 2 0.00 0 -1 4 4 -1 -1 208.13 0 -1 3 3 1 2 63.01 0 1 2 3 1 -1 27.00 0 1 2 12 0 0 17.18 0 0 4 0 -2 -1 136.27 0 0 2 11 2 0 0.00 0 -1 3 2 2 0 3.76 0 2 2 1 0 1 13.65 180 1 2 13 0 1 110.90 180 -1 3 8 0 2 1.05 0 -1 4 6 -1 -2 3.48 0 1 3 6 -1 1 38.70 0 0 3 8 0 -1 9.58 180 -2 4 2 0 -1 46.27 180 2 2 8 -1 0 35.69 0 1 3 5 -1 0 35.62 180 0 4 1 -2 0 0.00 0 0 4 3 -2 -1 48.55 0 0 3 7 0 -2 3.53 0 1 3 8 -2 -2 0.00 0 -1 4 11 -2 -2 79.41 180 0 4 2 -2 -2 72.16 180 -1 3 8 1 1 0.00 0 1 2 11 0 -1 48.38 180 1 3 1 -1 -1 10.73 180 0 3 12 -1 -2 0.00 0 0 3 12 -1 1 0.00 0 1 2 4 2 2 0.00 0 -2 4 7 0 -2 0.00 0 0 3 9 0 0 19.56 0 -1 4 2 -1 0 402.73 180 2 2 4 0 1 78.93 180 0 2 12 2 1 54.43 0 -1 3 0 2 1 63.48 180 -1 3 10 1 0 9.29 0 2 2 13 -2 0 72.90 180 -1 3 5 2 0 5.39 180 0 4 4 -2 0 51.07 0 0 3 13 -1 -1 185.14 0 0 3 8 0 2 0.00 0 -2 4 5 0 -1 117.44 0 -1 3 6 1 2 122.08 0 1 2 6 1 -1 161.89 0 0 3 1 1 0 0.78 180 1 3 4 -1 -1 233.86 0 1 2 3 2 1 118.54 0 -1 3 3 2 1 115.57 0 2 2 8 0 2 0.00 0 0 3 2 1 1 86.41 0 -1 4 7 -1 -1 27.20 180 0 4 5 -2 -2 96.21 180 0 4 6 -2 -1 38.65 180 -1 4 5 -1 0 167.52 180 1 1 14 2 0 0.00 0 0 3 0 1 2 1.38 0 1 2 10 0 -2 0.00 0 1 2 11 1 1 59.59 180 0 3 10 0 1 0.00 0 0 3 4 1 0 0.00 0 -2 4 10 -1 -1 0.00 0 -2 4 12 -1 -2 53.02 180 2 2 12 -1 1 111.11 180 1 2 7 2 2 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