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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ #======================================================================= data_global #======================================================================= _audit_creation_method 'Jana2020 1.3.45' # 1. PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_paper_category ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full 'CrystEngComm' _journal_year 2023 _journal_volume 25 _journal_issue ? _journal_page_first 2213 _journal_page_last 2226 _journal_paper_doi https://doi.org/10.1039/d3ce00119a _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #======================================================================= # 2. SUBMISSION DETAILS _publ_contact_author_name 'Garcia-Tojal, Javier' _publ_contact_author_address ;Departamento de Qu\'imica Universidad de Burgos 09001 Burgos Spain ; _publ_contact_author_email qipgatoj@ubu.es _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_requested_journal 'CrystEngComm' _publ_requested_category ? #======================================================================= # 3. TITLE AND AUTHOR LIST _publ_section_title ;Theoretical basis (to understand - for the) structural features and trends in the reactivity of thiosemicarbazonecopper(II) complexes. The case of the perchlorate - copper(II) system. ; loop_ _publ_author_name _publ_author_address 'Gil-Garcia, Ruben' ;Departamento de Qu\'imica Universidad de Burgos 09001 Burgos Spain ; 'Madariaga, Gotzon' ;Departamento de F\'isica Facultad de Ciencia y Tecnolog\'ia Universidad del Pa\'is Vasco Apdo. 644 48080 Bilbao Spain ; 'Jimenez-Perez, Alondra' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Herran-Torres,Ignacio' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Gago-Gonzalez, Adrian' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Ugalde, Maria' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Januskaitis, Vaidas' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Barrera-Garcia, Joaquin' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Insausti, Maite' ;Departamento de Qu\'imica Org\'anica e Inorg\'anica Facultad de Ciencia y Tecnolog\'ia Universidad del Pa\'is Vasco Apdo. 644 48080 Bilbao Spain ; 'Galletero, Maria S.' ;Servicio Central de Espectrometr\'a de Masas Universidad de Valencia Av. Dr. Moliner 100 Burjassot Valencia Spain ; 'Borras, Joaquin' ;Departamento de Qu\'imica Inorg\'anica Facultad de Farmacia Universidad de Valencia 46100 Burjassot Valencia Spain ; 'Cuevas, Jose Vicente' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Pedrido, Rosa' ;Departamento de Qu\'imica Inorg\'anica Facultade de Qu\'imica Campus Vida Universidade de Santiago de Compostela 15782 Santiago de Compostela Spain ; 'Gomez-Saiz, Patricia' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; 'Lezama, Luis' ;Departamento de Qu\'imica Org\'anica e Inorg\'anica Facultad de Ciencia y Tecnolog\'ia Universidad del Pa\'is Vasco Apdo. 644 48080 Bilbao Spain ; 'Garcia-Tojal, Javier' ;Departamento de Qu\'mica Universidad de Burgos 09001 Burgos Spain ; #======================================================================= # 4. TEXT _publ_section_references ; Petricek, V., Dusek, M. & Palatinus L. (2014). Z. Kristallogr. 229(5), 345-352. Palatinus L. & Chapuis G. (2007). J. Appl. Cryst. 40, 786-790. ; #======================================================================= data_I #======================================================================= # 5. CHEMICAL DATA _chemical_formula_sum 'C8 H8 Cl Cu N5 O4 S2' _chemical_formula_moiety 'C8 H8 Cu N5 S2, Cl O4' _chemical_formula_weight 401.3 #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system monoclinic _space_group_ssg_name 'C2/m(\a0\g)0s' loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,x2,-x3,-x4+1/2 3 -x1,-x2,-x3,-x4 4 x1,-x2,x3,x4+1/2 5 x1+1/2,x2+1/2,x3,x4 6 -x1+1/2,x2+1/2,-x3,-x4+1/2 7 -x1+1/2,-x2+1/2,-x3,-x4 8 x1+1/2,-x2+1/2,x3,x4+1/2 _cell_length_a 14.950(5) _cell_length_b 6.5697(17) _cell_length_c 15.010(5) _cell_angle_alpha 90 _cell_angle_beta 106.96(2) _cell_angle_gamma 90 _cell_volume 1410.1(7) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 -0.614888 0.000000 0.345313 _cell_formula_units_Z 4 _cell_measurement_reflns_used 1520 _cell_measurement_theta_min 2.73 _cell_measurement_theta_max 24.12 _cell_measurement_temperature 293(2) _cell_special_details ? _exptl_crystal_description prismatic _exptl_crystal_colour Green _exptl_crystal_size_max 0.175 _exptl_crystal_size_mid 0.066 _exptl_crystal_size_min 0.036 _exptl_crystal_density_diffrn 1.8902 _exptl_crystal_F_000 804 _exptl_absorpt_coefficient_mu 2.056 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.8111 _exptl_absorpt_correction_T_max 0.9355 #======================================================================= # 7. EXPERIMENTAL DATA _diffrn_ambient_temperature 293(2) _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71069 _diffrn_source 'Mo Genix 3D VHF' _diffrn_radiation_monochromator 'Graded multilayer mirror (W/Si)' _diffrn_measurement_method 'rotation method' _diffrn_detector_area_resol_mean 5.81 _diffrn_reflns_number 17802 _diffrn_reflns_theta_min 2.79 _diffrn_reflns_theta_max 34.9 _diffrn_reflns_theta_full 20.93 _diffrn_measured_fraction_theta_max 0.88 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.1205 _diffrn_reflns_av_unetI/netI 0.3414 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_k_max 4 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_index_m_1_min -1 _diffrn_reflns_limit_index_m_1_max 1 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? _diffrn_radiation_probe x-ray #======================================================================= # 8. REFINEMENT DATA _refine_special_details ? _reflns_number_total 4656 _reflns_number_gt 1389 _reflns_threshold_expression 'I>2.5\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.1122 _refine_ls_wR_factor_gt 0.1883 _refine_ls_R_factor_all 0.2814 _refine_ls_wR_factor_ref 0.2220 _refine_ls_goodness_of_fit_ref 1.7008 _refine_ls_goodness_of_fit_gt 2.7083 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 4656 _refine_ls_number_parameters 113 _refine_ls_number_restraints 4 _refine_ls_number_constraints 17 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(I)+0.0004I^2^)' _refine_ls_hydrogen_treatment 'constr' _refine_ls_shift/su_max 0.0005 _refine_ls_shift/su_mean 0.0000 _refine_diff_density_max 1.64 _refine_diff_density_min -1.91 _refine_ls_extinction_method 'none' _refine_ls_extinction_coef ? _refine_ls_extinction_expression ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C 0.0033 0.0016 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Cl 0.1484 0.1585 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Cu 0.3201 1.2651 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' N 0.0061 0.0033 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' S 0.1246 0.1234 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_cell_refinement 'STOE X-AREA' _computing_data_reduction 'STOE X-RED' _computing_structure_refinement 'JANA (Petricek et al., 2014)' loop_ _restr_distance_atom_site_label_1 _restr_distance_site_symmetry_1 _restr_distance_atom_site_label_2 _restr_distance_site_symmetry_2 _restr_distance_target _restr_distance_target_weight_param N4 . H4n2 . 0.86 0.001 loop_ _restr_angle_atom_site_label_1 _restr_angle_site_symmetry_1 _restr_angle_atom_site_label_2 _restr_angle_site_symmetry_2 _restr_angle_atom_site_label_3 _restr_angle_site_symmetry_3 _restr_angle_target _restr_angle_target_weight_param C7 . N4 . H4n1 . 120 0.01 loop_ _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param _restr_equal_distance_class_average _restr_equal_distance_class_esd 1 ? 0.86 0.001 loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_site_symmetry_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_id N4 . H4n2 . 1 N4 . H4n1 . 1 loop_ _restr_equal_angle_class_class_id _restr_equal_angle_class_target_weight_param _restr_equal_angle_class_average _restr_equal_angle_class_esd 1 ? 120 0.01 loop_ _restr_equal_angle_atom_site_label_1 _restr_equal_angle_site_symmetry_1 _restr_equal_angle_atom_site_label_2 _restr_equal_angle_site_symmetry_2 _restr_equal_angle_atom_site_label_3 _restr_equal_angle_site_symmetry_3 _restr_equal_angle_class_id C7 . N4 . H4n1 . 1 C7 . N4 . H4n2 . 1 #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.22560(7) 0.5 0.14679(7) Uani 0.0499(4) 4 1 d . . . S1 S 0.06735(19) 0.5 0.12702(18) Uani 0.0499(8) 4 1 d . . . S2 S 0.2352(2) 0.5 -0.16011(19) Uani 0.0546(19) 4 1 d . . . N1 N 0.3661(5) 0.5 0.2017(5) Uani 0.0555(8) 4 1 d . . . N2 N 0.2354(5) 0.5 0.2784(5) Uani 0.0476(7) 4 1 d . . . N3 N 0.1570(5) 0.5 0.3054(5) Uani 0.0446(10) 4 1 d . . . H3n H 0.160399 0.5 0.363643 Uani 0.0430(13) 4 1 d . . . N4 N 0.0005(5) 0.5 0.2719(5) Uani 0.0460(18) 4 1 d . . . H4n2 H 0.0069(8) 0.5 0.3307(5) Uani 0.043(2) 4 1 d . . . H4n1 H -0.0545(5) 0.5 0.2327(8) Uani 0.049(2) 4 1 d . . . N5 N 0.2202(5) 0.5 0.0183(5) Uani 0.0521(7) 4 1 d . . . C1 C 0.4310(6) 0.5 0.1608(7) Uani 0.0604(11) 4 1 d . . . H1 H 0.412334 0.5 0.096025 Uani 0.0591(11) 4 1 d . . . C2 C 0.5251(7) 0.5 0.2050(7) Uani 0.069(2) 4 1 d . . . H2 H 0.569311 0.5 0.172456 Uani 0.074(2) 4 1 d . . . C3 C 0.5487(7) 0.5 0.2963(8) Uani 0.073(3) 4 1 d . . . H3 H 0.612041 0.5 0.328717 Uani 0.081(4) 4 1 d . . . C4 C 0.4855(6) 0.5 0.3470(7) Uani 0.065(2) 4 1 d . . . H4 H 0.504003 0.5 0.411724 Uani 0.068(3) 4 1 d . . . C5 C 0.3947(7) 0.5 0.2959(6) Uani 0.0569(14) 4 1 d . . . C6 C 0.3164(6) 0.5 0.3353(6) Uani 0.0507(12) 4 1 d . . . H6 H 0.325645 0.5 0.399279 Uani 0.0504(17) 4 1 d . . . C7 C 0.0751(7) 0.5 0.2417(6) Uani 0.0460(11) 4 1 d . . . C8 C 0.2260(6) 0.5 -0.0549(6) Uani 0.0532(11) 4 1 d . . . Cl1 Cl 0.339(2) -0.002(7) 0.4496(17) Uani 0.0535(13) 8 0.5 d . . . O1 O 0.298(3) -0.132(10) 0.490(4) Uani 0.207(9) 8 0.5 d . . . O2 O 0.279(3) 0.092(10) 0.379(3) Uani 0.194(9) 8 0.5 d . . . O3 O 0.394(3) -0.103(10) 0.408(3) Uani 0.173(9) 8 0.5 d . . . O4 O 0.384(4) 0.138(10) 0.516(3) Uani 0.098(9) 8 0.5 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cu1 Cu 0.0478(6) 0.0692(9) 0.0359(5) 0 0.0173(4) 0 S1 S 0.0481(6) 0.074(2) 0.0317(9) 0 0.0180(5) 0 S2 S 0.064(2) 0.066(5) 0.0436(6) 0 0.0319(10) 0 N1 N 0.0479(6) 0.074(2) 0.0461(7) 0 0.0160(5) 0 N2 N 0.0521(9) 0.0573(17) 0.0344(5) 0 0.0144(5) 0 N3 N 0.0556(12) 0.049(2) 0.0319(7) 0 0.0167(7) 0 H3n H 0.0608(17) 0.039(3) 0.0318(8) 0 0.0170(9) 0 N4 N 0.0566(13) 0.053(5) 0.0344(17) 0 0.0227(13) 0 H4n2 H 0.0620(18) 0.040(6) 0.0349(18) 0 0.0246(16) 0 H4n1 H 0.0547(12) 0.064(5) 0.037(2) 0 0.0238(13) 0 N5 N 0.0499(9) 0.0739(17) 0.0380(5) 0 0.0216(5) 0 C1 C 0.0478(7) 0.081(3) 0.0555(12) 0 0.0196(7) 0 H1 H 0.0491(8) 0.078(3) 0.0555(12) 0 0.0237(8) 0 C2 C 0.0477(6) 0.093(6) 0.0679(19) 0 0.0186(8) 0 H2 H 0.0483(7) 0.099(7) 0.077(3) 0 0.0230(10) 0 C3 C 0.0489(7) 0.098(8) 0.0673(19) 0 0.0115(9) 0 H3 H 0.0493(7) 0.112(11) 0.077(2) 0 0.0093(10) 0 C4 C 0.0519(9) 0.084(7) 0.0555(12) 0 0.0079(8) 0 H4 H 0.0560(13) 0.083(10) 0.0554(12) 0 0.0039(10) 0 C5 C 0.0506(8) 0.072(4) 0.0462(7) 0 0.0114(6) 0 C6 C 0.0543(11) 0.058(3) 0.0382(5) 0 0.0113(5) 0 H6 H 0.0595(16) 0.051(5) 0.0376(5) 0 0.0096(6) 0 C7 C 0.0527(10) 0.058(3) 0.0319(10) 0 0.0189(8) 0 C8 C 0.0542(14) 0.073(3) 0.0400(5) 0 0.0252(6) 0 Cl1 Cl 0.051(3) 0.081(2) 0.0330(12) -0.018(2) 0.0193(13) -0.006(2) O1 O 0.416(16) 0.111(10) 0.188(13) -0.104(11) 0.238(12) -0.036(9) O2 O 0.225(13) 0.209(19) 0.071(8) 0.026(13) -0.076(8) 0.003(10) O3 O 0.078(14) 0.281(13) 0.179(15) -0.058(11) 0.069(13) -0.171(10) O4 O 0.078(17) 0.135(15) 0.064(11) -0.002(14) -0.004(11) -0.051(11) loop_ _atom_site_Fourier_wave_vector_seq_id _atom_site_Fourier_wave_vector_q1_coeff 1 1 loop_ _atom_site_occ_special_func_atom_site_label _atom_site_occ_special_func_crenel_c _atom_site_occ_special_func_crenel_w Cl1 0.2229 0.5 O1 0.2622 0.5 O2 0.2352 0.5 O3 0.1742 0.5 O4 0.2179 0.5 loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Cu1y1 Cu1 y 1 S1y1 S1 y 1 S2y1 S2 y 1 N1y1 N1 y 1 N2y1 N2 y 1 N3y1 N3 y 1 H3ny1 H3n y 1 N4y1 N4 y 1 H4n2y1 H4n2 y 1 H4n1y1 H4n1 y 1 N5y1 N5 y 1 C1y1 C1 y 1 H1y1 H1 y 1 C2y1 C2 y 1 H2y1 H2 y 1 C3y1 C3 y 1 H3y1 H3 y 1 C4y1 C4 y 1 H4y1 H4 y 1 C5y1 C5 y 1 C6y1 C6 y 1 H6y1 H6 y 1 C7y1 C7 y 1 C8y1 C8 y 1 Cl1x1 Cl1 x 1 Cl1y1 Cl1 y 1 Cl1z1 Cl1 z 1 O1x1 O1 x 1 O1y1 O1 y 1 O1z1 O1 z 1 O2x1 O2 x 1 O2y1 O2 y 1 O2z1 O2 z 1 O3x1 O3 x 1 O3y1 O3 y 1 O3z1 O3 z 1 O4x1 O4 x 1 O4y1 O4 y 1 O4z1 O4 z 1 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Cu1y1 -0.0099(3) 0.0368(3) S1y1 -0.0271(5) 0.0464(5) S2y1 0.0298(7) 0.0116(7) N1y1 -0.0122(5) 0.0304(5) N2y1 -0.0304(4) 0.0325(4) N3y1 -0.0429(5) 0.0289(5) H3ny1 -0.0504(5) 0.0213(5) N4y1 -0.0611(7) 0.0218(7) H4n2y1 -0.0654(8) 0.0106(8) H4n1y1 -0.0661(8) 0.0219(9) N5y1 0.0099(4) 0.0327(4) C1y1 -0.0076(6) 0.0274(6) H1y1 -0.0009(6) 0.0233(6) C2y1 -0.0131(9) 0.0322(9) H2y1 -0.0105(10) 0.0329(10) C3y1 -0.0223(10) 0.0377(10) H3y1 -0.0240(12) 0.0443(12) C4y1 -0.0296(9) 0.0346(9) H4y1 -0.0380(10) 0.0353(10) C5y1 -0.0245(6) 0.0315(6) C6y1 -0.0334(5) 0.0296(5) H6y1 -0.0422(6) 0.0256(6) C7y1 -0.0450(5) 0.0336(5) C8y1 0.0198(5) 0.0257(5) Cl1x1 -0.0034(11) 0.015(4) Cl1y1 -0.0388(14) -0.011(9) Cl1z1 0.0019(9) 0.002(3) O1x1 -0.005(2) 0.025(5) O1y1 -0.040(4) -0.028(12) O1z1 0.0011(18) 0.009(5) O2x1 -0.0076(14) 0.008(5) O2y1 -0.046(4) -0.043(16) O2z1 0.0011(13) -0.003(4) O3x1 0.007(2) 0.022(5) O3y1 -0.027(5) 0.009(13) O3z1 0.0050(17) 0.006(4) O4x1 -0.0085(17) 0.005(6) O4y1 -0.030(4) 0.014(14) O4z1 0.0003(15) -0.005(5) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_ssg_symmetry_1 _geom_bond_site_ssg_symmetry_2 _geom_bond_distance_av _geom_bond_distance_min _geom_bond_distance_max _geom_bond_publ_flag Cu1 S1 . . 2.299(4) 2.297(4) 2.301(4) ? Cu1 N1 . . 2.022(7) 2.020(7) 2.024(7) ? Cu1 N2 . . 1.938(7) 1.938(7) 1.939(7) ? Cu1 N5 . . 1.907(7) 1.906(7) 1.908(7) ? S1 C7 . . 1.692(9) 1.691(9) 1.692(9) ? S2 C8 . . 1.625(10) 1.624(10) 1.625(10) ? N1 C1 . . 1.292(14) 1.291(14) 1.292(14) ? N1 C5 . . 1.353(12) 1.352(12) 1.354(12) ? N2 N3 . . 1.349(12) 1.348(12) 1.350(12) ? N2 C6 . . 1.263(10) 1.261(10) 1.264(10) ? N3 H3n . . 0.860(7) 0.860(7) 0.861(7) ? N3 C7 . . 1.317(10) 1.315(10) 1.318(10) ? N4 H4n2 . . 0.860(11) 0.860(11) 0.861(11) ? N4 H4n1 . . 0.861(9) 0.860(9) 0.862(9) ? N4 C7 . . 1.321(13) 1.320(13) 1.322(13) ? N5 C8 . . 1.128(12) 1.128(12) 1.129(12) ? C1 H1 . . 0.931(10) 0.930(10) 0.931(10) ? C1 C2 . . 1.370(12) 1.369(12) 1.372(12) ? C2 H2 . . 0.930(11) 0.930(11) 0.931(11) ? C2 C3 . . 1.312(15) 1.311(15) 1.313(15) ? C3 H3 . . 0.931(10) 0.930(10) 0.932(10) ? C3 C4 . . 1.375(17) 1.374(17) 1.375(17) ? C4 H4 . . 0.931(10) 0.930(10) 0.931(10) ? C4 C5 . . 1.353(12) 1.351(12) 1.354(12) ? C5 C6 . . 1.458(15) 1.457(15) 1.458(15) ? C6 H6 . . 0.930(9) 0.930(9) 0.931(9) ? Cl1 O1 . . 1.31(10) 1.30(12) 1.31(12) ? Cl1 O2 . . 1.33(7) 1.32(9) 1.34(9) ? Cl1 O3 . . 1.36(9) 1.35(12) 1.36(12) ? Cl1 O4 . . 1.39(9) 1.38(12) 1.40(12) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_ssg_symmetry_1 _geom_angle_site_ssg_symmetry_2 _geom_angle_site_ssg_symmetry_3 _geom_angle_av _geom_angle_min _geom_angle_max _geom_angle_publ_flag S1 Cu1 N1 . . . 164.1(2) 164.1(2) 164.1(2) ? S1 Cu1 N2 . . . 84.3(2) 84.3(2) 84.4(2) ? S1 Cu1 N5 . . . 97.5(2) 97.4(2) 97.6(2) ? N1 Cu1 N2 . . . 79.8(3) 79.7(3) 79.9(3) ? N1 Cu1 N5 . . . 98.4(3) 98.3(3) 98.4(3) ? N2 Cu1 N5 . . . 178.2(3) 178.2(3) 178.2(3) ? Cu1 S1 C7 . . . 96.1(3) 96.0(3) 96.1(3) ? Cu1 N1 C1 . . . 130.0(6) 129.9(6) 130.0(6) ? Cu1 N1 C5 . . . 113.6(7) 113.6(7) 113.7(7) ? C1 N1 C5 . . . 116.4(8) 116.3(8) 116.5(8) ? Cu1 N2 N3 . . . 119.5(5) 119.4(5) 119.6(5) ? Cu1 N2 C6 . . . 117.6(7) 117.5(7) 117.6(7) ? N3 N2 C6 . . . 122.9(8) 122.9(8) 123.0(8) ? N2 N3 H3n . . . 120.38 120.32 120.45 ? N2 N3 C7 . . . 119.2(7) 119.1(7) 119.2(7) ? H3n N3 C7 . . . 120.43 120.38 120.49 ? H4n2 N4 H4n1 . . . 120.0(14) 120.0(14) 120.1(14) ? H4n2 N4 C7 . . . 120.0(11) 119.9(11) 120.0(11) ? H4n1 N4 C7 . . . 120.0(11) 120.0(11) 120.1(11) ? Cu1 N5 C8 . . . 173.4(7) 173.4(7) 173.4(7) ? N1 C1 H1 . . . 117.31 117.24 117.37 ? N1 C1 C2 . . . 125.3(9) 125.3(9) 125.4(9) ? H1 C1 C2 . . . 117.37 117.31 117.43 ? C1 C2 H2 . . . 122.21 122.16 122.26 ? C1 C2 C3 . . . 115.6(11) 115.6(11) 115.7(11) ? H2 C2 C3 . . . 122.16 122.1 122.23 ? C2 C3 H3 . . . 118.04 117.98 118.1 ? C2 C3 C4 . . . 123.9(9) 123.9(9) 124.0(9) ? H3 C3 C4 . . . 118.02 117.96 118.08 ? C3 C4 H4 . . . 122.37 122.3 122.43 ? C3 C4 C5 . . . 115.2(9) 115.1(9) 115.3(9) ? H4 C4 C5 . . . 122.43 122.37 122.49 ? N1 C5 C4 . . . 123.5(10) 123.5(10) 123.6(10) ? N1 C5 C6 . . . 112.2(8) 112.1(8) 112.2(8) ? C4 C5 C6 . . . 124.3(9) 124.3(9) 124.4(9) ? N2 C6 C5 . . . 116.9(8) 116.8(8) 116.9(8) ? N2 C6 H6 . . . 121.6 121.55 121.66 ? C5 C6 H6 . . . 121.55 121.48 121.61 ? S1 C7 N3 . . . 120.9(8) 120.9(8) 121.0(8) ? S1 C7 N4 . . . 122.3(6) 122.2(6) 122.4(6) ? N3 C7 N4 . . . 116.8(8) 116.7(8) 116.8(8) ? S2 C8 N5 . . . 179.6(8) 179.6(8) 179.6(8) ? O1 Cl1 O2 . . . 112(6) 112(7) 113(6) ? O1 Cl1 O3 . . . 109(7) 109(8) 109(6) ? O1 Cl1 O4 . . . 108(6) 107(6) 108(6) ? O2 Cl1 O3 . . . 103(5) 103(5) 104(5) ? O2 Cl1 O4 . . . 110(7) 109(7) 110(6) ? O3 Cl1 O4 . . . 115(6) 114(7) 115(6) ? #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 2 0 0 0 20232.00 24924.30 936.94 o 4 0 0 0 8969.62 11315.30 407.00 o 6 0 0 0 8834.72 10206.70 118.71 o 8 0 0 0 1458.29 1329.10 629.57 < 12 0 0 0 215.95 370.96 46.63 o 14 0 0 0 1160.67 943.30 165.34 o 16 0 0 0 113.79 44.52 133.55 < 1 1 0 -1 20.76 21.20 74.19 < 1 1 0 0 7796.70 8826.74 184.42 o 1 1 0 1 19.19 42.40 31.80 < 3 1 0 -1 7.45 16.96 27.56 < 3 1 0 0 22100.40 23726.60 381.56 o 3 1 0 1 88.40 72.07 27.56 o 5 1 0 -1 16.22 72.07 29.68 < 5 1 0 0 7568.77 8129.33 148.38 o 5 1 0 1 10.27 95.39 29.68 o 7 1 0 -1 101.73 63.59 31.80 < 7 1 0 0 10528.10 10982.50 116.59 o 7 1 0 1 213.57 201.38 25.44 o 9 1 0 -1 55.84 52.99 122.95 < 9 1 0 1 139.17 158.98 42.40 o 11 1 0 -1 19.82 76.31 46.63 < 11 1 0 0 3932.19 2938.01 220.46 o 11 1 0 1 45.11 16.96 44.52 < 13 1 0 -1 5.58 8.48 33.92 < 13 1 0 0 5484.96 6198.22 129.31 o 13 1 0 1 42.40 139.90 129.31 < 15 1 0 -1 4.54 -23.32 63.59 < 15 1 0 0 286.71 262.85 50.87 o 15 1 0 1 1.89 6.36 103.87 < 17 1 0 -1 11.30 8.48 44.52 < 17 1 0 0 121.09 146.26 127.19 < 17 1 0 1 1.07 10.60 31.80 < 19 1 0 1 0.72 48.75 103.87 < 0 2 0 0 187256.00 202625.00 4657.14 o 0 2 0 1 5339.80 3980.93 332.80 o 2 2 0 -1 198.60 328.57 25.44 o 2 2 0 0 10575.50 10656.10 237.41 o 2 2 0 1 57.71 260.73 27.56 o 4 2 0 -1 885.58 928.46 29.68 o 4 2 0 0 8976.17 8708.03 142.02 o 4 2 0 1 89.20 120.83 21.20 o 6 2 0 -1 171.92 161.10 36.04 o 6 2 0 0 3592.45 3692.64 50.87 o 6 2 0 1 604.20 638.05 29.68 o 8 2 0 -1 0.81 4.24 50.87 < 8 2 0 0 721.80 1036.57 178.06 o 8 2 0 1 40.98 21.20 110.23 < 10 2 0 -1 5.34 29.68 76.31 < 10 2 0 0 1134.96 1507.16 65.71 o 10 2 0 1 0.31 -10.60 131.43 < 12 2 0 -1 7.20 12.72 69.95 < 12 2 0 0 120.60 86.91 116.59 < 12 2 0 1 2.22 114.47 129.31 < 14 2 0 -1 0.32 -16.96 36.04 < 14 2 0 0 757.55 907.26 154.74 o 14 2 0 1 51.16 23.32 122.95 < 16 2 0 -1 0.16 27.56 103.87 < 16 2 0 0 77.69 12.72 129.31 < 16 2 0 1 1.79 48.75 33.92 < 18 2 0 0 108.95 131.43 154.74 < 18 2 0 1 5.83 42.40 38.16 < 1 3 0 0 149.29 99.63 19.08 o 1 3 0 1 21.38 40.28 19.08 < 3 3 0 -1 0.45 8.48 21.20 < 3 3 0 0 2572.32 2193.97 33.92 o 3 3 0 1 478.81 572.34 25.44 o 5 3 0 -1 406.80 676.21 65.71 o 5 3 0 0 3501.31 3493.39 82.67 o 5 3 0 1 159.83 260.73 122.95 < 7 3 0 -1 677.59 546.90 549.02 < 7 3 0 0 3086.35 1356.65 1333.34 < 7 3 0 1 797.51 610.49 165.34 o 9 3 0 -1 5.86 52.99 36.04 < 9 3 0 0 885.34 322.21 311.61 < 9 3 0 1 361.96 209.86 228.94 < 11 3 0 -1 66.51 188.66 44.52 o 11 3 0 0 1813.79 1704.30 86.91 o 11 3 0 1 170.07 178.06 95.39 < 13 3 0 -1 86.46 114.47 38.16 o 13 3 0 0 2209.03 2325.39 205.62 o 13 3 0 1 230.80 156.86 93.27 < 15 3 0 -1 10.01 -14.84 97.51 < 15 3 0 0 136.43 203.50 127.19 < 15 3 0 1 5.83 -31.80 97.51 < 17 3 0 -1 34.88 46.63 101.75 < 17 3 0 0 48.17 154.74 135.66 < 17 3 0 1 2.98 12.72 57.23 < 0 4 0 0 19597.70 21678.90 735.56 o 0 4 0 1 3666.18 3728.68 135.66 o 2 4 0 -1 247.10 383.68 29.68 o 2 4 0 0 2392.90 2153.69 65.71 o 2 4 0 1 331.71 551.14 154.74 o 4 4 0 -1 1137.13 1068.37 546.90 < 4 4 0 0 1764.47 930.58 472.71 < 4 4 0 1 168.98 91.15 44.52 < 6 4 0 -1 104.99 80.55 129.31 < 6 4 0 0 729.45 466.35 434.55 < 6 4 0 1 562.57 294.65 421.83 < 8 4 0 -1 56.74 89.03 116.59 < 8 4 0 0 168.98 260.73 135.66 < 8 4 0 1 15.70 59.35 93.27 < 10 4 0 -1 30.94 -46.63 110.23 < 10 4 0 0 330.03 421.83 135.66 o 10 4 0 1 1.57 -21.20 44.52 < 12 4 0 -1 0.07 93.27 103.87 < 12 4 0 0 23.29 101.75 133.55 < 12 4 0 1 9.70 -6.36 91.15 < 14 4 0 -1 7.41 110.23 89.03 < 14 4 0 0 171.48 165.34 48.75 o 14 4 0 1 73.58 86.91 38.16 < 16 4 0 -1 0.08 -69.95 103.87 < 16 4 0 0 25.68 -40.28 118.71 < 16 4 0 1 4.37 -40.28 108.11 < 1 5 0 -1 19.29 137.79 31.80 o 1 5 0 0 37.97 25.44 25.44 < 1 5 0 1 3.51 -25.44 31.80 < 3 5 0 -1 0.33 -29.68 29.68 < 3 5 0 0 453.00 252.25 29.68 o 3 5 0 1 161.39 218.34 31.80 o 5 5 0 -1 279.93 574.46 50.87 o 5 5 0 0 405.54 294.65 46.63 o 5 5 0 1 58.78 112.35 31.80 o 7 5 0 -1 381.88 712.24 161.10 o 7 5 0 0 424.66 455.75 46.63 o 7 5 0 1 444.59 267.09 48.75 o 9 5 0 -1 0.62 -52.99 40.28 < 9 5 0 0 180.62 175.94 44.52 o 9 5 0 1 193.31 315.85 52.99 o 11 5 0 -1 33.97 142.02 101.75 < 11 5 0 0 306.89 292.53 50.87 o 11 5 0 1 89.07 63.59 38.16 < 13 5 0 -1 65.12 211.98 93.27 < 13 5 0 0 314.22 301.01 74.19 o 13 5 0 1 146.79 116.59 122.95 < 15 5 0 0 38.08 -129.31 116.59 < 15 5 0 1 6.33 135.66 36.04 o 0 6 0 0 1411.78 1680.98 103.87 o 0 6 0 1 783.19 881.83 48.75 o 2 6 0 -1 135.06 224.70 65.71 o 2 6 0 0 340.57 209.86 31.80 o 2 6 0 1 47.97 129.31 61.47 < 4 6 0 -1 334.10 551.14 36.04 o 4 6 0 0 122.43 44.52 36.04 < 4 6 0 1 29.64 8.48 25.44 < 6 6 0 -1 51.22 80.55 31.80 o 6 6 0 0 86.93 182.30 137.79 < 6 6 0 1 167.10 521.46 46.63 o 8 6 0 -1 7.04 57.23 38.16 < 8 6 0 0 28.67 93.27 46.63 < 8 6 0 1 4.76 63.59 27.56 < 10 6 0 -1 7.02 -25.44 57.23 < 10 6 0 0 25.56 38.16 50.87 < 10 6 0 1 0.06 29.68 44.52 < 12 6 0 -1 0.03 -10.60 63.59 < 12 6 0 0 0.32 144.15 44.52 o 12 6 0 1 3.33 33.92 44.52 < 14 6 0 1 20.69 91.15 33.92 o 1 7 0 -1 0.12 -61.47 50.87 < 1 7 0 0 0.28 57.23 76.31 < 1 7 0 1 4.12 -27.56 40.28 < 3 7 0 -1 1.13 -2.12 31.80 < 3 7 0 0 30.17 4.24 40.28 < 3 7 0 1 32.11 31.80 33.92 < 5 7 0 -1 30.20 33.92 52.99 < 5 7 0 0 26.63 -36.04 57.23 < 5 7 0 1 12.49 29.68 36.04 < 7 7 0 -1 59.78 97.51 33.92 o 7 7 0 0 25.10 -21.20 44.52 < 7 7 0 1 79.57 78.43 33.92 < 9 7 0 -1 1.95 -14.84 33.92 < 9 7 0 0 19.33 -59.35 48.75 < 9 7 0 1 42.41 86.91 69.95 < 11 7 0 0 22.74 -38.16 46.63 < 11 7 0 1 20.50 19.08 38.16 < 0 8 0 0 18.56 84.79 46.63 < 0 8 0 1 80.77 105.99 36.04 o 2 8 0 -1 18.78 -91.15 95.39 < 2 8 0 0 19.59 -4.24 114.47 < 2 8 0 1 8.64 25.44 36.04 < 4 8 0 -1 32.41 110.23 40.28 o 4 8 0 0 5.07 -67.83 44.52 < 4 8 0 1 3.41 -2.12 78.43 < 6 8 0 -1 9.31 -44.52 29.68 < 6 8 0 0 4.59 110.23 52.99 < 6 8 0 1 14.47 -8.48 36.04 < -16 0 1 0 9.77 -33.92 118.71 < -12 0 1 0 2134.52 2441.98 197.14 o -8 0 1 0 1301.73 430.31 438.79 < -6 0 1 0 1336.03 1110.76 44.52 o -4 0 1 0 32524.50 36129.40 744.04 o -2 0 1 0 3850.72 4252.27 135.66 o 2 0 1 0 3811.89 4264.98 110.23 o 4 0 1 0 12504.40 12445.20 264.97 o 6 0 1 0 32884.20 33064.20 468.47 o 8 0 1 0 321.08 337.04 40.28 o 10 0 1 0 300.16 -6.36 127.19 < 14 0 1 0 37.64 55.11 129.31 < 16 0 1 0 24.99 -14.84 137.79 < -19 1 1 -1 0.56 99.63 137.79 < -17 1 1 -1 4.50 4.24 46.63 < -17 1 1 0 252.73 491.79 154.74 o -17 1 1 1 0.61 -31.80 144.15 < -15 1 1 1 15.00 50.87 36.04 < -13 1 1 -1 88.01 -14.84 133.55 < -13 1 1 0 0.21 -80.55 114.47 < -13 1 1 1 2.88 -55.11 31.80 < -11 1 1 -1 24.10 -131.43 154.74 < -11 1 1 0 1518.10 1015.37 161.10 o -11 1 1 1 52.30 61.47 42.40 < -9 1 1 -1 3.39 14.84 108.11 < -9 1 1 1 44.88 -40.28 42.40 < -7 1 1 -1 521.43 400.64 29.68 o -7 1 1 0 16051.50 15067.30 190.78 o -7 1 1 1 128.57 237.41 25.44 o -5 1 1 -1 485.14 320.09 33.92 o -5 1 1 0 8406.57 7997.90 190.78 o -5 1 1 1 163.26 404.88 29.68 o -3 1 1 -1 192.96 345.52 29.68 o -3 1 1 0 3696.84 4638.06 127.19 o -3 1 1 1 136.27 48.75 33.92 < -1 1 1 0 8658.02 9187.10 207.74 o -1 1 1 1 536.97 858.51 36.04 o 1 1 1 -1 93.63 19.08 31.80 < 1 1 1 0 14925.70 17193.50 496.03 o 1 1 1 1 719.91 451.51 33.92 o 3 1 1 -1 2.50 19.08 25.44 < 3 1 1 0 390.48 322.21 31.80 o 3 1 1 1 262.57 142.02 27.56 o 5 1 1 -1 31.40 65.71 25.44 o 5 1 1 0 1561.64 1778.49 38.16 o 5 1 1 1 1.35 10.60 21.20 < 7 1 1 -1 60.08 152.62 55.11 o 7 1 1 0 6373.00 6889.26 264.97 o 7 1 1 1 7.65 16.96 19.08 < 9 1 1 -1 0.06 48.75 38.16 < 9 1 1 0 3965.96 3821.95 112.35 o 9 1 1 1 2.60 72.07 33.92 < 11 1 1 -1 23.40 69.95 86.91 < 11 1 1 0 312.45 324.33 38.16 o 11 1 1 1 13.17 -25.44 44.52 < 13 1 1 -1 91.53 135.66 110.23 < 13 1 1 0 872.69 790.67 55.11 o 13 1 1 1 5.16 55.11 82.67 < 15 1 1 -1 0.02 -21.20 31.80 < 15 1 1 0 265.49 105.99 127.19 < 17 1 1 -1 0.02 -131.43 118.71 < -18 2 1 -1 13.53 0.00 108.11 < -18 2 1 0 90.07 152.62 125.07 < -18 2 1 1 0.26 0.00 42.40 < -16 2 1 -1 6.52 42.40 127.19 < -16 2 1 0 6.92 50.87 112.35 < -16 2 1 1 0.62 48.75 40.28 < -14 2 1 1 72.72 129.31 118.71 < -12 2 1 -1 6.80 8.48 103.87 < -12 2 1 1 190.68 281.93 108.11 o -10 2 1 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47.97 42.40 118.71 < 14 2 1 0 9.99 -21.20 135.66 < 14 2 1 1 1.56 -42.40 122.95 < 16 2 1 -1 0.65 101.75 97.51 < 16 2 1 0 12.14 -61.47 129.31 < 16 2 1 1 1.77 21.20 33.92 < 18 2 1 1 0.79 -40.28 93.27 < -17 3 1 -1 21.56 65.71 33.92 < -17 3 1 0 95.39 190.78 135.66 < -17 3 1 1 1.22 -33.92 101.75 < -15 3 1 -1 0.03 59.35 131.43 < -15 3 1 1 37.50 78.43 101.75 < -13 3 1 -1 259.83 156.86 65.71 < -13 3 1 1 62.50 120.83 91.15 < -11 3 1 -1 112.88 50.87 40.28 < -11 3 1 0 447.14 398.52 131.43 o -11 3 1 1 174.83 394.28 127.19 o -9 3 1 -1 74.48 57.23 31.80 < -9 3 1 0 564.69 275.57 99.63 o -9 3 1 1 1.05 16.96 38.16 < -7 3 1 -1 1308.93 1055.65 216.22 o -7 3 1 0 5732.48 6626.41 114.47 o -7 3 1 1 178.86 201.38 78.43 o -5 3 1 -1 854.92 638.05 33.92 o -5 3 1 0 2128.90 2039.22 55.11 o -5 3 1 1 51.65 288.29 52.99 o -3 3 1 -1 356.29 542.66 21.20 o -3 3 1 0 18.80 19.08 19.08 < -3 3 1 1 64.42 -4.24 16.96 < -1 3 1 0 6744.11 7597.27 171.70 o 1 3 1 -1 26.48 214.10 57.23 o 1 3 1 0 1495.96 1621.63 55.11 o 3 3 1 -1 3.53 36.04 19.08 < 3 3 1 0 115.89 211.98 23.32 o 3 3 1 1 162.59 40.28 16.96 < 5 3 1 0 68.33 29.68 129.31 < 5 3 1 1 31.62 55.11 27.56 < 7 3 1 -1 56.49 59.35 133.55 < 7 3 1 0 2413.03 2929.53 82.67 o 7 3 1 1 51.55 19.08 46.63 < 9 3 1 -1 101.24 61.47 48.75 < 9 3 1 0 2284.78 2365.67 116.59 o 9 3 1 1 42.86 69.95 67.83 < 11 3 1 -1 131.61 264.97 105.99 < 11 3 1 0 113.81 42.40 42.40 < 11 3 1 1 44.87 -10.60 38.16 < 13 3 1 -1 228.40 315.85 46.63 o 13 3 1 0 301.79 294.65 165.34 < 13 3 1 1 8.06 -67.83 99.63 < 15 3 1 -1 2.15 -57.23 110.23 < 15 3 1 0 139.26 178.06 67.83 o 15 3 1 1 28.46 63.59 40.28 < 17 3 1 0 70.07 -14.84 139.90 < 17 3 1 1 0.39 -97.51 99.63 < -16 4 1 -1 8.78 -42.40 108.11 < -16 4 1 0 3.94 63.59 148.38 < -16 4 1 1 1.02 63.59 99.63 < -14 4 1 -1 131.27 -38.16 99.63 < -14 4 1 0 98.28 27.56 142.02 < -14 4 1 1 52.33 150.50 91.15 < -12 4 1 -1 24.08 148.38 112.35 < -12 4 1 0 246.16 203.50 135.66 < -12 4 1 1 305.22 407.00 120.83 o -10 4 1 -1 3.18 -33.92 99.63 < -10 4 1 0 53.77 50.87 118.71 < -10 4 1 1 0.38 57.23 116.59 < -8 4 1 -1 91.66 156.86 131.43 < -8 4 1 0 94.36 78.43 127.19 < -8 4 1 1 9.14 -6.36 82.67 < -6 4 1 -1 9.80 16.96 31.80 < -6 4 1 0 271.73 269.21 46.63 o -6 4 1 1 0.36 114.47 131.43 < -4 4 1 -1 307.49 315.85 31.80 o -4 4 1 1 0.46 33.92 44.52 < -2 4 1 -1 103.07 105.99 50.87 < -2 4 1 0 640.22 830.95 33.92 o -2 4 1 1 103.95 33.92 27.56 < 0 4 1 -1 4126.11 5583.48 271.33 o 0 4 1 1 315.41 470.59 44.52 o 2 4 1 -1 230.55 224.70 33.92 o 2 4 1 0 1029.91 402.76 207.74 < 2 4 1 1 473.38 1004.77 101.75 o 4 4 1 -1 174.35 343.40 63.59 o 4 4 1 0 988.91 883.95 99.63 o 4 4 1 1 10.61 8.48 61.47 < 6 4 1 -1 922.10 551.14 273.45 < 6 4 1 0 4171.16 3186.02 1583.47 < 6 4 1 1 616.23 508.75 50.87 o 8 4 1 -1 303.04 288.29 46.63 o 8 4 1 0 212.94 167.46 42.40 o 8 4 1 1 0.66 27.56 31.80 < 10 4 1 -1 168.57 224.70 105.99 < 10 4 1 0 6.50 27.56 46.63 < 10 4 1 1 2.33 27.56 31.80 < 12 4 1 -1 72.60 14.84 89.03 < 12 4 1 0 36.24 42.40 40.28 < 12 4 1 1 25.07 -50.87 50.87 < 14 4 1 -1 29.13 16.96 110.23 < 14 4 1 0 0.61 -74.19 118.71 < 14 4 1 1 3.55 0.00 38.16 < 16 4 1 0 1.56 -42.40 148.38 < 16 4 1 1 1.33 31.80 99.63 < -15 5 1 -1 0.30 63.59 78.43 < -15 5 1 0 0.17 46.63 46.63 < -15 5 1 1 19.66 42.40 112.35 < -13 5 1 -1 133.07 182.30 110.23 < -13 5 1 0 0.12 -44.52 150.50 < -13 5 1 1 50.51 112.35 112.35 < -11 5 1 -1 87.93 29.68 36.04 < -11 5 1 0 60.01 86.91 110.23 < -11 5 1 1 87.01 139.90 91.15 < -9 5 1 -1 56.26 -4.24 131.43 < -9 5 1 0 99.82 114.47 112.35 < -9 5 1 1 7.83 118.71 116.59 < -7 5 1 -1 548.06 582.94 50.87 o -7 5 1 0 683.29 688.93 133.55 o -7 5 1 1 32.65 116.59 120.83 < -5 5 1 -1 461.09 449.39 67.83 o -5 5 1 0 315.79 307.37 55.11 o -5 5 1 1 0.85 125.07 46.63 o -3 5 1 -1 286.07 479.07 48.75 o -3 5 1 0 1.39 36.04 31.80 < -3 5 1 1 14.55 10.60 23.32 < -1 5 1 0 381.99 426.07 33.92 o 1 5 1 -1 6.11 108.11 36.04 o 1 5 1 0 241.18 294.65 31.80 o 1 5 1 1 371.92 354.00 31.80 o 3 5 1 -1 1.14 16.96 25.44 < 3 5 1 0 2.34 74.19 23.32 o 3 5 1 1 51.88 21.20 23.32 < 5 5 1 -1 14.29 76.31 36.04 < 5 5 1 0 48.25 10.60 42.40 < 5 5 1 1 8.41 8.48 48.75 < 7 5 1 -1 25.54 33.92 42.40 < 7 5 1 0 324.66 345.52 31.80 o 7 5 1 1 23.78 40.28 33.92 < 9 5 1 -1 73.90 46.63 33.92 < 9 5 1 0 353.52 258.61 40.28 o 9 5 1 1 27.47 69.95 48.75 < 11 5 1 -1 90.34 186.54 40.28 o 11 5 1 0 39.12 21.20 40.28 < 11 5 1 1 16.73 8.48 59.35 < 13 5 1 -1 121.46 139.90 156.86 < 13 5 1 0 52.12 21.20 46.63 < 13 5 1 1 2.28 -48.75 36.04 < 15 5 1 0 27.87 -10.60 129.31 < 15 5 1 1 13.50 -76.31 52.99 < -14 6 1 -1 44.13 116.59 38.16 o -12 6 1 -1 11.32 101.75 33.92 o -12 6 1 0 11.73 0.00 127.19 < -12 6 1 1 90.44 127.19 114.47 < -10 6 1 -1 0.54 -48.75 38.16 < -10 6 1 0 4.43 -55.11 42.40 < -10 6 1 1 0.18 55.11 86.91 < -8 6 1 -1 22.06 76.31 31.80 < -8 6 1 0 0.90 -76.31 127.19 < -8 6 1 1 2.36 -65.71 129.31 < -6 6 1 -1 1.26 -55.11 118.71 < -6 6 1 0 26.61 80.55 33.92 < -6 6 1 1 3.89 63.59 40.28 < -4 6 1 -1 98.10 110.23 27.56 o -4 6 1 0 137.35 180.18 44.52 o -4 6 1 1 5.88 67.83 40.28 < -2 6 1 -1 131.96 122.95 29.68 o -2 6 1 0 96.38 150.50 29.68 o -2 6 1 1 60.91 27.56 38.16 < 0 6 1 -1 991.16 1422.37 63.59 o 0 6 1 0 79.44 152.62 55.11 o 0 6 1 1 47.76 156.86 40.28 o 2 6 1 -1 61.56 31.80 23.32 < 2 6 1 0 62.92 44.52 52.99 < 2 6 1 1 132.69 370.96 55.11 o 4 6 1 -1 60.05 133.55 31.80 o 4 6 1 0 156.00 93.27 31.80 o 4 6 1 1 1.07 29.68 31.80 < 6 6 1 -1 256.30 364.60 38.16 o 6 6 1 0 264.76 326.45 38.16 o 6 6 1 1 122.63 218.34 57.23 o 8 6 1 -1 87.15 57.23 67.83 < 8 6 1 0 22.04 89.03 36.04 < 8 6 1 1 0.32 38.16 50.87 < 10 6 1 -1 65.45 48.75 33.92 < 10 6 1 0 3.52 -38.16 57.23 < 10 6 1 1 0.44 23.32 27.56 < 12 6 1 -1 27.46 55.11 52.99 < 12 6 1 0 0.85 -42.40 154.74 < 12 6 1 1 3.87 38.16 36.04 < -11 7 1 -1 22.02 -16.96 40.28 < -11 7 1 0 1.74 61.47 127.19 < -9 7 1 -1 14.70 50.87 86.91 < -9 7 1 0 8.57 216.22 146.26 < -9 7 1 1 0.56 -57.23 89.03 < -7 7 1 -1 105.49 89.03 29.68 o -7 7 1 0 24.05 80.55 42.40 < -7 7 1 1 3.33 82.67 93.27 < -5 7 1 -1 102.05 95.39 31.80 o -5 7 1 0 12.57 40.28 89.03 < -5 7 1 1 1.27 8.48 61.47 < -3 7 1 -1 62.86 61.47 38.16 < -3 7 1 0 0.42 -12.72 33.92 < -3 7 1 1 0.80 -99.63 57.23 < -1 7 1 -1 150.87 93.27 31.80 o -1 7 1 0 3.19 -2.12 33.92 < -1 7 1 1 80.02 152.62 78.43 < 1 7 1 -1 2.58 -10.60 27.56 < 1 7 1 0 6.02 89.03 36.04 < 1 7 1 1 63.77 74.19 42.40 < 3 7 1 -1 0.37 -46.63 89.03 < 3 7 1 0 0.69 12.72 40.28 < 3 7 1 1 7.03 38.16 44.52 < 5 7 1 -1 0.03 -16.96 33.92 < 5 7 1 0 12.14 44.52 127.19 < 5 7 1 1 0.04 2.12 46.63 < 7 7 1 -1 6.33 2.12 29.68 < 7 7 1 0 13.72 114.47 129.31 < 7 7 1 1 4.20 -89.03 61.47 < 9 7 1 -1 11.43 46.63 82.67 < 9 7 1 0 20.94 16.96 40.28 < 9 7 1 1 4.96 -65.71 31.80 < 11 7 1 1 2.44 -38.16 38.16 < -8 8 1 -1 1.61 -19.08 29.68 < -6 8 1 -1 0.73 25.44 89.03 < -6 8 1 0 0.72 -59.35 42.40 < -6 8 1 1 1.22 23.32 59.35 < -4 8 1 -1 12.26 -55.11 36.04 < -4 8 1 0 2.55 -80.55 50.87 < -4 8 1 1 0.44 -48.75 29.68 < -2 8 1 -1 24.96 82.67 36.04 < -2 8 1 0 11.43 108.11 40.28 o -2 8 1 1 4.61 4.24 91.15 < 0 8 1 -1 107.21 156.86 52.99 o 0 8 1 0 4.39 0.00 67.83 < 0 8 1 1 4.91 33.92 86.91 < 2 8 1 -1 17.54 -65.71 95.39 < 2 8 1 0 1.03 -203.50 127.19 < 2 8 1 1 6.51 -55.11 99.63 < 4 8 1 -1 12.30 31.80 27.56 < 4 8 1 0 7.38 31.80 74.19 < 4 8 1 1 0.98 55.11 46.63 < 6 8 1 -1 28.06 67.83 46.63 < 6 8 1 0 3.22 -4.24 63.59 < 6 8 1 1 10.73 4.24 42.40 < -8 0 2 0 3441.77 1848.44 1784.85 < -6 0 2 0 10265.80 9863.30 114.47 o -4 0 2 0 10403.10 10596.70 175.94 o -2 0 2 0 1624.16 1789.09 84.79 o 0 0 2 0 8329.14 6174.90 602.02 o 2 0 2 0 21897.60 21990.50 686.81 o 4 0 2 0 3626.13 4002.13 76.31 o 6 0 2 0 1722.84 1733.97 57.23 o 8 0 2 0 853.41 604.14 46.63 o 10 0 2 0 107.61 -19.08 46.63 < 12 0 2 0 264.99 237.41 114.47 < -19 1 2 -1 2.89 -63.59 44.52 < -17 1 2 -1 0.15 -6.36 86.91 < -17 1 2 1 1.53 46.63 137.79 < -15 1 2 -1 6.95 31.80 105.99 < -15 1 2 1 3.10 -105.99 127.19 < -13 1 2 -1 58.71 25.44 33.92 < -13 1 2 0 2860.76 3096.99 76.31 o -13 1 2 1 82.52 137.79 36.04 o -11 1 2 -1 52.06 -19.08 116.59 < -11 1 2 0 633.92 549.02 135.66 o -11 1 2 1 11.63 108.11 101.75 < -9 1 2 -1 14.22 -33.92 93.27 < -9 1 2 1 1.27 12.72 127.19 < -7 1 2 -1 31.66 52.99 21.20 < -7 1 2 0 236.39 235.29 25.44 o -7 1 2 1 99.66 195.02 25.44 o -5 1 2 -1 0.13 2.12 29.68 < -5 1 2 0 537.65 479.07 36.04 o -5 1 2 1 0.81 -21.20 25.44 < -3 1 2 -1 60.20 38.16 27.56 < -3 1 2 0 447.21 390.04 33.92 o -3 1 2 1 102.85 173.82 29.68 o -1 1 2 -1 649.19 671.97 31.80 o -1 1 2 0 25902.90 26980.50 648.65 o -1 1 2 1 3.82 50.87 27.56 < 1 1 2 -1 546.48 589.30 31.80 o 1 1 2 0 929.78 913.62 38.16 o 1 1 2 1 53.01 -2.12 23.32 < 3 1 2 -1 122.94 173.82 23.32 o 3 1 2 0 6908.72 8703.79 116.59 o 3 1 2 1 107.25 154.74 23.32 o 5 1 2 -1 142.14 205.62 21.20 o 5 1 2 0 6272.41 6367.80 57.23 o 5 1 2 1 580.06 606.26 25.44 o 7 1 2 -1 10.54 -27.56 27.56 < 7 1 2 0 1928.70 2009.54 38.16 o 7 1 2 1 111.58 63.59 21.20 o 9 1 2 -1 41.75 -14.84 50.87 < 9 1 2 0 2.85 31.80 36.04 < 9 1 2 1 1.96 42.40 29.68 < 11 1 2 -1 8.46 33.92 42.40 < 11 1 2 0 256.85 366.72 46.63 o 11 1 2 1 3.21 -29.68 46.63 < 13 1 2 -1 0.26 -33.92 33.92 < 13 1 2 0 341.55 284.05 50.87 o 13 1 2 1 0.26 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144.15 23.32 o 2 2 2 0 6170.37 6747.24 110.23 o 2 2 2 1 167.54 207.74 27.56 o 4 2 2 -1 212.49 152.62 21.20 o 4 2 2 0 264.34 362.48 21.20 o 4 2 2 1 167.22 4.24 19.08 < 6 2 2 -1 1247.48 1191.31 203.50 o 6 2 2 0 292.07 135.66 40.28 o 6 2 2 1 2.98 4.24 21.20 < 8 2 2 -1 23.08 84.79 31.80 o 8 2 2 0 166.46 89.03 27.56 o 8 2 2 1 210.20 292.53 33.92 o 10 2 2 -1 1.27 -16.96 36.04 < 10 2 2 0 207.64 199.26 50.87 o 10 2 2 1 0.72 19.08 55.11 < 12 2 2 -1 24.27 12.72 103.87 < 12 2 2 0 165.64 171.70 42.40 o 12 2 2 1 1.66 52.99 42.40 < 14 2 2 1 6.94 -89.03 99.63 < 16 2 2 1 0.07 110.23 112.35 < 18 2 2 1 6.22 16.96 91.15 < -17 3 2 -1 0.19 6.36 36.04 < -17 3 2 0 110.54 91.15 44.52 < -17 3 2 1 8.25 89.03 61.47 < -15 3 2 -1 41.44 154.74 76.31 < -15 3 2 1 1.85 -80.55 97.51 < -13 3 2 -1 149.04 209.86 57.23 o -13 3 2 0 1045.76 1331.22 175.94 o -13 3 2 1 204.91 148.38 114.47 < -11 3 2 -1 171.84 36.04 36.04 < -11 3 2 0 183.32 224.70 59.35 o -11 3 2 1 29.29 40.28 44.52 < -9 3 2 -1 1.42 -8.48 38.16 < -9 3 2 0 663.51 368.84 373.08 < -9 3 2 1 156.23 72.07 84.79 < -7 3 2 -1 315.57 233.18 135.66 < -7 3 2 0 247.47 281.93 144.15 < -7 3 2 1 182.37 197.14 42.40 o -5 3 2 -1 239.00 97.51 23.32 o -5 3 2 0 207.40 167.46 86.91 < -5 3 2 1 373.04 421.83 55.11 o -3 3 2 -1 9.36 8.48 16.96 < -3 3 2 0 26.78 61.47 16.96 o -3 3 2 1 112.90 150.50 21.20 o -1 3 2 -1 1119.66 1426.61 31.80 o -1 3 2 0 2165.84 2041.34 61.47 o -1 3 2 1 25.03 16.96 16.96 < 1 3 2 -1 627.56 858.51 31.80 o 1 3 2 0 1165.81 981.46 31.80 o 3 3 2 -1 192.30 320.09 65.71 o 3 3 2 0 264.09 727.08 120.83 o 3 3 2 1 60.50 95.39 19.08 o 5 3 2 -1 145.72 241.65 61.47 o 5 3 2 0 754.50 589.30 72.07 o 5 3 2 1 1139.55 1030.21 273.45 o 7 3 2 -1 166.26 105.99 38.16 o 7 3 2 0 604.51 788.56 36.04 o 7 3 2 1 564.76 330.68 36.04 o 9 3 2 -1 30.36 14.84 89.03 < 9 3 2 0 89.97 80.55 31.80 o 9 3 2 1 2.16 2.12 29.68 < 11 3 2 -1 54.26 2.12 38.16 < 11 3 2 0 68.71 38.16 42.40 < 11 3 2 1 14.93 10.60 31.80 < 13 3 2 -1 6.81 -8.48 82.67 < 13 3 2 1 3.82 38.16 133.55 < 15 3 2 -1 16.07 -46.63 40.28 < 15 3 2 0 37.52 125.07 48.75 o 15 3 2 1 0.72 57.23 57.23 < 17 3 2 0 1.79 38.16 133.55 < 17 3 2 1 5.45 4.24 103.87 < -16 4 2 -1 0.39 12.72 89.03 < -16 4 2 0 6.22 -57.23 133.55 < -16 4 2 1 9.82 0.00 108.11 < -14 4 2 -1 66.09 91.15 103.87 < -14 4 2 0 54.65 -44.52 133.55 < -14 4 2 1 10.08 55.11 91.15 < -12 4 2 -1 195.09 165.34 108.11 < -12 4 2 0 78.09 -25.44 114.47 < -12 4 2 1 0.31 -74.19 89.03 < -10 4 2 -1 5.19 29.68 101.75 < -10 4 2 0 16.49 -50.87 131.43 < -10 4 2 1 79.54 16.96 101.75 < -8 4 2 -1 161.53 144.15 129.31 < -8 4 2 0 309.80 239.53 127.19 < -8 4 2 1 476.60 635.93 137.79 o -6 4 2 -1 7.42 72.07 40.28 < -6 4 2 0 1218.29 1085.32 110.23 o -6 4 2 1 1557.44 1719.14 69.95 o -4 4 2 -1 55.84 14.84 25.44 < -4 4 2 0 534.07 326.45 31.80 o -4 4 2 1 103.70 188.66 36.04 o -2 4 2 -1 46.11 74.19 33.92 < -2 4 2 0 384.98 322.21 31.80 o -2 4 2 1 40.98 46.63 25.44 < 0 4 2 -1 337.04 233.18 57.23 o 0 4 2 0 1783.23 2299.95 63.59 o 0 4 2 1 671.52 618.97 74.19 o 2 4 2 -1 464.58 298.89 48.75 o 2 4 2 0 343.36 423.95 86.91 o 2 4 2 1 16.98 4.24 27.56 < 4 4 2 -1 270.56 288.29 40.28 o 4 4 2 0 18.11 42.40 27.56 < 4 4 2 1 169.06 59.35 27.56 < 6 4 2 -1 949.36 1064.13 315.85 o 6 4 2 0 7.90 31.80 21.20 < 6 4 2 1 14.35 36.04 23.32 < 8 4 2 -1 0.50 2.12 29.68 < 8 4 2 0 5.63 -4.24 74.19 < 8 4 2 1 157.16 309.49 31.80 o 10 4 2 -1 0.32 33.92 38.16 < 10 4 2 0 59.42 80.55 36.04 < 10 4 2 1 3.08 -50.87 36.04 < 12 4 2 -1 52.21 146.26 38.16 o 12 4 2 0 33.99 -67.83 42.40 < 12 4 2 1 3.30 -8.48 31.80 < 14 4 2 -1 19.66 48.75 89.03 < 14 4 2 0 5.59 163.22 150.50 < 14 4 2 1 6.13 80.55 105.99 < 16 4 2 0 6.29 -10.60 146.26 < 16 4 2 1 0.13 -23.32 91.15 < -15 5 2 -1 24.70 91.15 103.87 < -15 5 2 0 41.30 105.99 137.79 < -15 5 2 1 0.11 -33.92 105.99 < -13 5 2 -1 68.21 12.72 99.63 < -13 5 2 0 148.36 339.16 156.86 < -13 5 2 1 97.61 178.06 118.71 < -11 5 2 -1 70.29 46.63 114.47 < -11 5 2 0 5.92 52.99 127.19 < -11 5 2 1 23.90 -25.44 101.75 < -9 5 2 -1 0.53 59.35 135.66 < -9 5 2 0 75.58 33.92 135.66 < -9 5 2 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6 2 -1 21.35 6.36 103.87 < -14 6 2 0 5.92 -95.39 116.59 < -12 6 2 -1 52.48 -4.24 44.52 < -12 6 2 0 1.98 -59.35 99.63 < -12 6 2 1 0.23 59.35 110.23 < -10 6 2 -1 2.92 57.23 122.95 < -10 6 2 0 6.72 114.47 129.31 < -10 6 2 1 33.04 135.66 133.55 < -8 6 2 -1 32.70 -12.72 133.55 < -8 6 2 0 17.41 -29.68 133.55 < -8 6 2 1 156.60 296.77 127.19 < -6 6 2 -1 0.47 46.63 31.80 < -6 6 2 0 88.54 -78.43 46.63 < -6 6 2 1 369.87 493.91 52.99 o -4 6 2 -1 13.72 -19.08 38.16 < -4 6 2 0 70.55 21.20 33.92 < -4 6 2 1 17.11 -14.84 42.40 < -2 6 2 -1 48.62 16.96 29.68 < -2 6 2 0 32.44 -31.80 40.28 < -2 6 2 1 9.06 36.04 46.63 < 0 6 2 -1 53.24 21.20 25.44 < 0 6 2 0 35.92 36.04 46.63 < 0 6 2 1 196.41 184.42 42.40 o 2 6 2 -1 159.95 112.35 33.92 o 2 6 2 0 5.50 105.99 57.23 < 2 6 2 1 27.71 52.99 29.68 < 4 6 2 -1 86.96 118.71 40.28 o 4 6 2 0 1.14 6.36 33.92 < 4 6 2 1 65.14 97.51 29.68 o 6 6 2 -1 250.07 398.52 33.92 o 6 6 2 0 0.39 -152.62 116.59 < 6 6 2 1 4.78 -40.28 95.39 < 8 6 2 -1 2.98 19.08 33.92 < 8 6 2 0 0.25 -6.36 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12.62 25.44 38.16 < 7 7 2 0 2.64 42.40 48.75 < 7 7 2 1 55.70 16.96 40.28 < 9 7 2 -1 7.11 12.72 93.27 < 9 7 2 0 0.15 23.32 42.40 < 9 7 2 1 2.28 38.16 33.92 < -8 8 2 -1 2.01 -29.68 33.92 < -6 8 2 -1 0.06 10.60 52.99 < -6 8 2 0 1.20 -44.52 36.04 < -6 8 2 1 36.37 -27.56 97.51 < -4 8 2 -1 1.40 0.00 93.27 < -4 8 2 0 2.14 -50.87 46.63 < -4 8 2 1 5.45 50.87 31.80 < -2 8 2 -1 2.98 25.44 36.04 < -2 8 2 0 0.83 59.35 61.47 < -2 8 2 1 3.79 -6.36 33.92 < 0 8 2 -1 4.64 -42.40 38.16 < 0 8 2 0 0.09 -65.71 69.95 < 0 8 2 1 23.38 16.96 42.40 < 2 8 2 -1 10.35 0.00 50.87 < 2 8 2 0 0.89 -23.32 44.52 < 2 8 2 1 5.26 -4.24 31.80 < 4 8 2 -1 12.61 -14.84 36.04 < 4 8 2 0 0.63 2.12 50.87 < 4 8 2 1 7.68 0.00 38.16 < 6 8 2 -1 28.75 89.03 31.80 o 6 8 2 0 0.72 23.32 40.28 < 6 8 2 1 1.21 31.80 27.56 < -8 0 3 0 3258.84 2827.78 250.13 o -6 0 3 0 11464.50 11306.90 203.50 o -4 0 3 0 22.11 50.87 38.16 < -2 0 3 0 1242.09 1223.11 133.55 o 0 0 3 0 27929.50 27663.00 1581.35 o 2 0 3 0 13338.90 14208.80 402.76 o 4 0 3 0 1518.07 1981.99 57.23 o 6 0 3 0 5469.15 5488.09 74.19 o 8 0 3 0 184.61 61.47 44.52 < 10 0 3 0 599.52 517.22 50.87 o 12 0 3 0 12.82 108.11 103.87 < 16 0 3 0 36.45 -110.23 131.43 < -19 1 3 -1 2.71 38.16 110.23 < -17 1 3 -1 3.47 63.59 52.99 < -17 1 3 0 158.18 146.26 127.19 < -17 1 3 1 2.23 4.24 40.28 < -15 1 3 1 15.31 -19.08 122.95 < -13 1 3 1 0.74 2.12 137.79 < -11 1 3 -1 1.42 8.48 36.04 < -11 1 3 0 2821.89 3236.89 203.50 o -11 1 3 1 1.39 -59.35 133.55 < -9 1 3 -1 280.24 184.42 57.23 o -9 1 3 0 3119.97 4173.83 256.49 o -9 1 3 1 25.17 -23.32 44.52 < -7 1 3 -1 10.85 40.28 23.32 < -7 1 3 0 9199.62 11220.00 156.86 o -7 1 3 1 132.87 105.99 31.80 o -5 1 3 -1 281.45 250.13 25.44 o -5 1 3 0 1064.79 1051.41 33.92 o -5 1 3 1 292.99 294.65 23.32 o -3 1 3 -1 1.40 6.36 27.56 < -3 1 3 0 3647.90 3942.78 131.43 o -3 1 3 1 89.84 61.47 23.32 o -1 1 3 -1 30.07 4.24 29.68 < -1 1 3 0 14657.50 15694.80 777.96 o -1 1 3 1 1.12 8.48 33.92 < 1 1 3 -1 0.12 4.24 23.32 < 1 1 3 0 6.38 2.12 25.44 < 1 1 3 1 479.21 542.66 33.92 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2 3 -1 0.37 8.48 44.52 < -12 2 3 1 46.13 110.23 116.59 < -10 2 3 -1 5.67 19.08 36.04 < -10 2 3 0 1697.60 1748.81 65.71 o -10 2 3 1 29.86 -23.32 46.63 < -8 2 3 -1 518.72 275.57 74.19 o -8 2 3 0 2383.32 2293.59 148.38 o -8 2 3 1 0.83 8.48 31.80 < -6 2 3 -1 649.11 508.75 25.44 o -6 2 3 0 6941.19 6236.37 63.59 o -6 2 3 1 281.77 273.45 52.99 o -4 2 3 -1 5.14 -40.28 29.68 < -4 2 3 0 823.14 754.64 23.32 o -4 2 3 1 40.88 -8.48 16.96 < -2 2 3 -1 8.16 -4.24 16.96 < -2 2 3 0 1774.22 1591.95 61.47 o -2 2 3 1 315.22 457.87 23.32 o 0 2 3 -1 16.27 61.47 16.96 o 0 2 3 0 6902.09 7474.32 211.98 o 0 2 3 1 242.27 337.04 19.08 o 2 2 3 -1 474.98 311.61 23.32 o 2 2 3 0 5863.99 5288.83 114.47 o 2 2 3 1 24.83 2.12 16.96 < 4 2 3 -1 475.15 368.84 33.92 o 4 2 3 0 3230.64 3400.12 42.40 o 4 2 3 1 11.78 -10.60 19.08 < 6 2 3 -1 221.75 110.23 38.16 o 6 2 3 0 2093.55 1854.80 277.69 o 8 2 3 -1 39.80 8.48 29.68 < 8 2 3 0 348.54 228.94 25.44 o 8 2 3 1 0.74 14.84 25.44 < 10 2 3 -1 8.11 33.92 29.68 < 10 2 3 0 584.55 680.45 97.51 o 10 2 3 1 27.18 42.40 31.80 < 12 2 3 -1 4.96 -8.48 40.28 < 12 2 3 0 2.73 40.28 139.90 < 12 2 3 1 34.54 76.31 59.35 < 14 2 3 -1 0.76 31.80 97.51 < 14 2 3 1 28.86 25.44 48.75 < 16 2 3 -1 4.32 29.68 110.23 < 16 2 3 0 22.70 -137.79 131.43 < -17 3 3 -1 13.19 -6.36 38.16 < -17 3 3 0 62.28 97.51 48.75 < -17 3 3 1 9.85 -74.19 40.28 < -15 3 3 -1 6.28 84.79 101.75 < -15 3 3 0 106.91 10.60 114.47 < -15 3 3 1 38.16 133.55 40.28 o -13 3 3 -1 223.99 184.42 48.75 o -13 3 3 0 851.66 801.27 48.75 o -13 3 3 1 19.80 23.32 63.59 < -11 3 3 -1 8.36 -14.84 44.52 < -11 3 3 0 1102.64 964.50 78.43 o -11 3 3 1 24.82 99.63 33.92 o -9 3 3 -1 542.64 506.63 44.52 o -9 3 3 0 1369.12 947.54 330.68 o -9 3 3 1 13.55 -25.44 31.80 < -7 3 3 -1 284.40 315.85 63.59 o -7 3 3 0 2765.86 2656.08 116.59 o -7 3 3 1 504.52 582.94 50.87 o -5 3 3 -1 58.57 48.75 21.20 < -5 3 3 0 113.89 258.61 33.92 o -5 3 3 1 7.82 10.60 36.04 < -3 3 3 -1 11.36 29.68 16.96 < -3 3 3 0 238.10 286.17 19.08 o -3 3 3 1 136.68 33.92 19.08 < -1 3 3 -1 30.29 38.16 19.08 < -1 3 3 0 743.49 752.52 23.32 o -1 3 3 1 0.65 23.32 14.84 < 1 3 3 -1 44.77 25.44 14.84 < 1 3 3 0 14.85 23.32 16.96 < 1 3 3 1 510.50 447.27 27.56 o 3 3 3 -1 686.06 381.56 93.27 o 3 3 3 0 271.70 148.38 82.67 < 3 3 3 1 110.99 129.31 36.04 o 5 3 3 -1 504.31 383.68 95.39 o 5 3 3 0 4418.83 4237.43 125.07 o 5 3 3 1 0.62 42.40 27.56 < 7 3 3 -1 311.82 481.19 40.28 o 7 3 3 0 942.75 949.66 38.16 o 7 3 3 1 191.89 131.43 38.16 o 9 3 3 -1 9.05 10.60 27.56 < 9 3 3 0 9.20 33.92 33.92 < 9 3 3 1 44.35 38.16 38.16 < 11 3 3 -1 1.28 12.72 40.28 < 11 3 3 0 189.48 169.58 38.16 o 11 3 3 1 122.72 112.35 31.80 o 13 3 3 -1 15.49 27.56 112.35 < 15 3 3 -1 0.05 -23.32 38.16 < 15 3 3 0 64.00 122.95 131.43 < -16 4 3 -1 1.12 110.23 89.03 < -16 4 3 0 4.72 -61.47 116.59 < -16 4 3 1 3.38 -36.04 99.63 < -14 4 3 -1 75.03 -80.55 84.79 < -14 4 3 0 224.35 354.00 125.07 o -14 4 3 1 13.86 -2.12 89.03 < -12 4 3 -1 0.23 131.43 120.83 < -12 4 3 0 6.10 40.28 135.66 < -12 4 3 1 71.74 59.35 105.99 < -10 4 3 -1 0.70 80.55 110.23 < -10 4 3 0 390.34 504.51 146.26 o -10 4 3 1 123.47 112.35 101.75 < -8 4 3 -1 198.10 82.67 93.27 < -8 4 3 0 691.61 667.73 52.99 o -8 4 3 1 56.85 80.55 36.04 < -6 4 3 -1 603.73 623.21 40.28 o -6 4 3 0 1537.36 1490.20 67.83 o -6 4 3 1 65.37 171.70 44.52 o -4 4 3 -1 122.62 169.58 25.44 o -4 4 3 0 394.47 205.62 29.68 o -4 4 3 1 128.75 377.32 40.28 o -2 4 3 -1 115.19 78.43 25.44 o -2 4 3 0 716.09 489.67 27.56 o -2 4 3 1 565.11 724.96 33.92 o 0 4 3 -1 203.64 354.00 52.99 o 0 4 3 0 1824.01 1568.63 332.80 o 0 4 3 1 314.76 195.02 76.31 o 2 4 3 -1 17.59 -4.24 27.56 < 2 4 3 0 1152.70 790.67 63.59 o 2 4 3 1 63.57 78.43 27.56 o 4 4 3 -1 560.45 623.21 40.28 o 4 4 3 0 884.65 960.26 31.80 o 4 4 3 1 2.35 -4.24 25.44 < 6 4 3 -1 120.54 146.26 23.32 o 6 4 3 0 394.30 411.24 31.80 o 6 4 3 1 349.17 133.55 27.56 o 8 4 3 -1 86.28 42.40 25.44 < 8 4 3 0 75.19 21.20 27.56 < 8 4 3 1 5.88 -2.12 25.44 < 10 4 3 -1 4.30 -8.48 33.92 < 10 4 3 0 137.38 209.86 112.35 < 10 4 3 1 32.82 82.67 122.95 < 12 4 3 -1 0.69 67.83 33.92 < 12 4 3 0 0.55 38.16 46.63 < 12 4 3 1 40.02 -12.72 44.52 < 14 4 3 -1 0.11 67.83 101.75 < 14 4 3 0 29.82 -6.36 148.38 < 14 4 3 1 38.44 61.47 84.79 < 16 4 3 1 3.54 -29.68 86.91 < -15 5 3 -1 4.80 -36.04 84.79 < -15 5 3 0 30.33 69.95 122.95 < -15 5 3 1 20.19 57.23 91.15 < -13 5 3 -1 138.09 91.15 103.87 < -13 5 3 0 116.06 48.75 161.10 < -13 5 3 1 14.18 57.23 110.23 < -11 5 3 -1 6.50 114.47 112.35 < -11 5 3 0 171.91 82.67 122.95 < -11 5 3 1 12.49 95.39 97.51 < -9 5 3 -1 242.45 313.73 133.55 < -9 5 3 0 264.00 392.16 146.26 o -9 5 3 1 15.74 42.40 95.39 < -7 5 3 -1 250.96 434.55 48.75 o -7 5 3 0 314.38 281.93 65.71 o -7 5 3 1 315.95 311.61 48.75 o -5 5 3 -1 5.14 33.92 27.56 < -5 5 3 0 0.42 -2.12 25.44 < -5 5 3 1 51.23 150.50 55.11 o -3 5 3 -1 0.28 44.52 27.56 < -3 5 3 0 81.34 86.91 23.32 o -3 5 3 1 35.65 19.08 27.56 < -1 5 3 -1 57.84 -6.36 40.28 < -1 5 3 0 134.08 224.70 27.56 o -1 5 3 1 26.14 27.56 23.32 < 1 5 3 -1 2.28 63.59 25.44 < 1 5 3 0 14.67 2.12 23.32 < 1 5 3 1 272.72 317.97 57.23 o 3 5 3 -1 92.83 99.63 55.11 < 3 5 3 0 147.33 108.11 42.40 o 3 5 3 1 104.51 211.98 36.04 o 5 5 3 -1 327.37 368.84 44.52 o 5 5 3 0 531.57 466.35 42.40 o 5 5 3 1 18.66 23.32 23.32 < 7 5 3 -1 133.78 241.65 27.56 o 7 5 3 0 138.97 86.91 29.68 o 7 5 3 1 110.45 122.95 36.04 o 9 5 3 -1 5.78 50.87 29.68 < 9 5 3 0 15.75 112.35 42.40 o 9 5 3 1 29.38 127.19 110.23 < 11 5 3 -1 0.71 110.23 55.11 < 11 5 3 0 21.39 38.16 44.52 < 11 5 3 1 59.86 52.99 40.28 < 13 5 3 -1 8.66 57.23 38.16 < 13 5 3 0 25.24 -55.11 48.75 < 13 5 3 1 26.76 21.20 33.92 < -14 6 3 -1 26.16 -40.28 84.79 < -14 6 3 0 15.04 -42.40 135.66 < -12 6 3 -1 0.27 175.94 127.19 < -12 6 3 0 0.13 12.72 122.95 < -12 6 3 1 20.76 23.32 110.23 < -10 6 3 -1 0.36 -89.03 122.95 < -10 6 3 0 33.98 48.75 110.23 < -10 6 3 1 33.84 -137.79 125.07 < -8 6 3 -1 53.23 59.35 125.07 < -8 6 3 0 82.53 14.84 131.43 < -8 6 3 1 9.87 61.47 122.95 < -6 6 3 -1 194.08 222.58 46.63 o -6 6 3 0 102.73 93.27 46.63 < -6 6 3 1 37.18 144.15 40.28 o -4 6 3 -1 27.86 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4 8 3 -1 11.54 12.72 25.44 < 4 8 3 0 2.67 21.20 42.40 < 4 8 3 1 0.92 36.04 55.11 < 6 8 3 1 8.51 12.72 27.56 < -10 0 4 0 122.11 84.79 122.95 < -8 0 4 0 5003.88 2719.67 2645.48 < -6 0 4 0 2181.77 2329.63 63.59 o -4 0 4 0 11004.60 11807.10 466.35 o -2 0 4 0 18510.30 17594.10 705.88 o 0 0 4 0 6029.70 6259.69 154.74 o 2 0 4 0 79.78 57.23 31.80 < 4 0 4 0 4950.42 4521.48 93.27 o 6 0 4 0 10132.50 9759.44 173.82 o 8 0 4 0 440.63 281.93 411.24 < 10 0 4 0 522.45 447.27 46.63 o 12 0 4 0 259.42 322.21 146.26 < 16 0 4 0 14.43 120.83 129.31 < -19 1 4 -1 0.52 -16.96 110.23 < -17 1 4 -1 1.50 59.35 31.80 < -17 1 4 0 111.50 125.07 154.74 < -17 1 4 1 0.76 110.23 89.03 < -15 1 4 -1 1.13 8.48 40.28 < -15 1 4 0 247.18 301.01 139.90 < -15 1 4 1 12.94 -4.24 122.95 < -13 1 4 -1 17.36 -2.12 112.35 < -13 1 4 0 30.53 16.96 120.83 < -13 1 4 1 4.01 -57.23 40.28 < -11 1 4 -1 57.34 80.55 42.40 < -11 1 4 0 849.93 549.02 417.60 < -11 1 4 1 43.30 118.71 57.23 < -9 1 4 -1 14.56 12.72 33.92 < -9 1 4 0 59.41 97.51 38.16 o -9 1 4 1 20.06 42.40 74.19 < -7 1 4 -1 654.86 714.36 31.80 o -7 1 4 0 11655.30 11039.80 203.50 o -7 1 4 1 27.02 0.00 25.44 < -5 1 4 -1 268.42 383.68 27.56 o -5 1 4 0 2568.53 2342.35 76.31 o -5 1 4 1 478.52 718.60 29.68 o -3 1 4 -1 173.20 322.21 33.92 o -3 1 4 0 387.80 430.31 33.92 o -3 1 4 1 17.73 36.04 27.56 < -1 1 4 -1 222.08 269.21 36.04 o -1 1 4 0 2441.81 2798.10 152.62 o -1 1 4 1 16.15 -59.35 72.07 < 1 1 4 -1 7.56 10.60 21.20 < 1 1 4 0 2428.07 2649.72 46.63 o 1 1 4 1 169.05 241.65 29.68 o 3 1 4 -1 182.43 120.83 19.08 o 3 1 4 0 143.24 203.50 23.32 o 3 1 4 1 49.06 74.19 19.08 o 5 1 4 -1 39.40 33.92 19.08 < 5 1 4 0 596.50 671.97 95.39 o 5 1 4 1 71.26 74.19 21.20 o 7 1 4 -1 5.12 10.60 31.80 < 7 1 4 0 2980.40 3569.70 59.35 o 7 1 4 1 36.41 44.52 25.44 < 9 1 4 -1 6.01 57.23 31.80 < 9 1 4 0 1393.03 1163.76 580.82 < 9 1 4 1 0.95 42.40 33.92 < 11 1 4 -1 25.85 29.68 36.04 < 11 1 4 0 1655.43 2340.23 72.07 o 11 1 4 1 4.81 -12.72 42.40 < 13 1 4 0 960.39 900.90 180.18 o 13 1 4 1 21.59 42.40 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2 4 -1 891.06 1017.49 29.68 o 0 2 4 0 7945.07 8057.26 320.09 o 0 2 4 1 211.50 127.19 19.08 o 2 2 4 -1 1188.46 1293.06 40.28 o 2 2 4 0 245.75 250.13 19.08 o 2 2 4 1 309.13 275.57 21.20 o 4 2 4 -1 127.61 209.86 33.92 o 4 2 4 0 1120.48 888.18 122.95 o 4 2 4 1 312.60 245.89 31.80 o 6 2 4 -1 56.76 161.10 40.28 o 6 2 4 0 6601.27 6613.69 76.31 o 6 2 4 1 30.95 -14.84 31.80 < 8 2 4 -1 5.56 -16.96 31.80 < 8 2 4 0 657.98 695.29 31.80 o 8 2 4 1 0.70 21.20 27.56 < 10 2 4 -1 151.97 65.71 69.95 < 10 2 4 0 183.12 131.43 33.92 o 10 2 4 1 1.23 69.95 36.04 < 12 2 4 -1 1.67 -50.87 114.47 < 12 2 4 1 3.36 186.54 120.83 < 14 2 4 1 1.33 0.00 122.95 < -19 3 4 -1 1.19 8.48 42.40 < -17 3 4 -1 6.90 6.36 40.28 < -17 3 4 0 57.51 6.36 38.16 < -17 3 4 1 1.82 82.67 33.92 < -15 3 4 -1 14.32 -59.35 131.43 < -15 3 4 0 79.38 4.24 42.40 < -15 3 4 1 34.18 105.99 38.16 o -13 3 4 -1 34.74 27.56 31.80 < -13 3 4 0 15.30 105.99 48.75 < -13 3 4 1 33.17 110.23 40.28 o -11 3 4 -1 205.30 171.70 36.04 o -11 3 4 0 388.49 362.48 42.40 o -11 3 4 1 90.64 120.83 33.92 o -9 3 4 -1 24.14 33.92 31.80 < -9 3 4 0 40.15 12.72 25.44 < -9 3 4 1 16.45 80.55 27.56 o -7 3 4 -1 1322.16 1178.59 146.26 o -7 3 4 0 3432.57 3258.09 248.01 o -7 3 4 1 140.73 67.83 33.92 < -5 3 4 -1 83.07 197.14 25.44 o -5 3 4 0 1362.49 1197.67 67.83 o -5 3 4 1 141.83 587.18 48.75 o -3 3 4 -1 443.29 599.90 23.32 o -3 3 4 0 649.77 657.13 27.56 o -3 3 4 1 61.91 23.32 23.32 < -1 3 4 -1 520.68 599.90 21.20 o -1 3 4 0 11.85 12.72 16.96 < -1 3 4 1 84.29 101.75 19.08 o 1 3 4 -1 0.32 -4.24 19.08 < 1 3 4 0 1099.07 1042.93 150.50 o 1 3 4 1 43.26 61.47 19.08 o 3 3 4 -1 257.42 209.86 33.92 o 3 3 4 0 267.90 402.76 38.16 o 3 3 4 1 1.12 19.08 31.80 < 5 3 4 -1 12.14 127.19 29.68 o 5 3 4 0 457.85 570.22 40.28 o 5 3 4 1 0.42 10.60 31.80 < 7 3 4 -1 2.64 2.12 27.56 < 7 3 4 0 752.87 828.83 192.90 o 7 3 4 1 181.00 298.89 59.35 o 9 3 4 -1 1.04 65.71 42.40 < 9 3 4 0 911.87 951.78 114.47 o 9 3 4 1 20.96 44.52 29.68 < 11 3 4 -1 108.25 267.09 46.63 o 11 3 4 0 615.88 682.57 42.40 o 11 3 4 1 15.42 99.63 33.92 o 13 3 4 0 316.39 284.05 133.55 < 13 3 4 1 78.59 103.87 65.71 < 15 3 4 -1 2.42 74.19 127.19 < -18 4 4 -1 14.39 69.95 108.11 < -16 4 4 -1 8.05 -27.56 86.91 < -16 4 4 0 1.36 59.35 120.83 < -16 4 4 1 9.54 31.80 99.63 < -14 4 4 -1 111.86 252.25 112.35 < -14 4 4 0 27.98 120.83 133.55 < -14 4 4 1 20.65 -16.96 108.11 < -12 4 4 -1 17.29 -19.08 105.99 < -12 4 4 0 129.49 186.54 137.79 < -12 4 4 1 25.88 80.55 103.87 < -10 4 4 -1 6.34 2.12 82.67 < -10 4 4 0 3.21 27.56 135.66 < -10 4 4 1 51.15 80.55 101.75 < -8 4 4 -1 58.91 38.16 38.16 < -8 4 4 0 412.61 665.61 50.87 o -8 4 4 1 63.12 178.06 38.16 o -6 4 4 -1 121.49 2.12 31.80 < -6 4 4 0 129.64 67.83 38.16 < -6 4 4 1 50.09 76.31 36.04 < -4 4 4 -1 4.52 67.83 23.32 o -4 4 4 0 1056.63 977.22 38.16 o -4 4 4 1 95.04 23.32 33.92 < -2 4 4 -1 261.03 398.52 103.87 o -2 4 4 0 1802.14 1606.79 122.95 o -2 4 4 1 23.07 -8.48 25.44 < 0 4 4 -1 690.49 682.57 57.23 o 0 4 4 0 1557.07 1475.36 61.47 o 0 4 4 1 224.34 241.65 63.59 o 2 4 4 -1 321.45 392.16 36.04 o 2 4 4 0 117.21 103.87 27.56 o 2 4 4 1 33.24 57.23 33.92 < 4 4 4 -1 90.07 184.42 23.32 o 4 4 4 0 321.00 260.73 36.04 o 4 4 4 1 143.19 171.70 25.44 o 6 4 4 -1 162.18 235.29 25.44 o 6 4 4 0 1330.54 1407.53 33.92 o 6 4 4 1 144.11 74.19 23.32 o 8 4 4 -1 20.28 33.92 25.44 < 8 4 4 0 219.79 89.03 31.80 o 8 4 4 1 1.12 8.48 27.56 < 10 4 4 -1 141.07 209.86 46.63 o 10 4 4 0 38.16 31.80 63.59 < 10 4 4 1 0.41 33.92 31.80 < 12 4 4 0 57.90 184.42 114.47 < 12 4 4 1 2.74 -97.51 36.04 < 14 4 4 -1 6.09 0.00 108.11 < 14 4 4 0 6.48 74.19 133.55 < -15 5 4 -1 10.86 -29.68 89.03 < -15 5 4 0 12.78 -129.31 118.71 < -15 5 4 1 17.08 23.32 91.15 < -13 5 4 -1 15.74 -44.52 80.55 < -13 5 4 0 0.94 108.11 142.02 < -13 5 4 1 23.20 -44.52 110.23 < -11 5 4 -1 119.30 114.47 97.51 < -11 5 4 0 60.64 209.86 131.43 < -11 5 4 1 43.13 38.16 84.79 < -9 5 4 -1 44.64 46.63 40.28 < -9 5 4 0 20.60 -10.60 59.35 < -9 5 4 1 20.28 99.63 114.47 < -7 5 4 -1 479.73 394.28 48.75 o -7 5 4 0 361.88 248.01 67.83 o -7 5 4 1 29.65 118.71 40.28 o -5 5 4 -1 42.17 76.31 25.44 o -5 5 4 0 229.64 158.98 31.80 o -5 5 4 1 1.30 84.79 38.16 < -3 5 4 -1 298.03 402.76 25.44 o -3 5 4 0 24.85 36.04 27.56 < -3 5 4 1 32.26 19.08 23.32 < -1 5 4 -1 113.47 148.38 29.68 o -1 5 4 0 17.92 14.84 25.44 < -1 5 4 1 85.78 184.42 29.68 o 1 5 4 -1 42.15 38.16 23.32 < 1 5 4 0 72.04 95.39 69.95 < 1 5 4 1 8.50 84.79 40.28 < 3 5 4 -1 24.27 23.32 23.32 < 3 5 4 0 8.13 23.32 23.32 < 3 5 4 1 0.38 2.12 38.16 < 5 5 4 -1 1.10 40.28 23.32 < 5 5 4 0 6.40 78.43 36.04 < 5 5 4 1 6.29 84.79 31.80 o 7 5 4 -1 8.11 8.48 25.44 < 7 5 4 0 90.96 108.11 40.28 o 7 5 4 1 79.69 118.71 23.32 o 9 5 4 -1 0.26 -80.55 38.16 < 9 5 4 0 141.66 120.83 42.40 o 9 5 4 1 15.32 16.96 31.80 < 11 5 4 -1 43.24 86.91 42.40 < 11 5 4 0 102.90 152.62 44.52 o 11 5 4 1 13.24 -2.12 38.16 < 13 5 4 -1 36.65 6.36 101.75 < 13 5 4 0 56.89 91.15 122.95 < 13 5 4 1 45.20 55.11 91.15 < -14 6 4 -1 33.12 120.83 91.15 < -14 6 4 0 2.47 -29.68 144.15 < -12 6 4 -1 3.98 23.32 112.35 < -12 6 4 0 18.56 -63.59 120.83 < -12 6 4 1 5.30 -131.43 108.11 < -10 6 4 -1 2.89 -48.75 120.83 < -10 6 4 0 0.06 -10.60 127.19 < -10 6 4 1 11.67 -133.55 116.59 < -8 6 4 -1 12.73 101.75 44.52 < -8 6 4 0 10.07 89.03 127.19 < -8 6 4 1 16.71 67.83 99.63 < -6 6 4 -1 21.40 -44.52 29.68 < -6 6 4 0 15.55 -50.87 31.80 < -6 6 4 1 4.18 50.87 44.52 < -4 6 4 -1 10.62 -25.44 31.80 < -4 6 4 0 129.87 76.31 38.16 < -4 6 4 1 3.71 33.92 31.80 < -2 6 4 -1 133.62 178.06 46.63 o -2 6 4 0 138.78 72.07 44.52 < -2 6 4 1 14.88 -16.96 31.80 < 0 6 4 -1 206.69 260.73 89.03 o 0 6 4 0 85.60 105.99 110.23 < 0 6 4 1 50.38 105.99 61.47 < 2 6 4 -1 52.44 42.40 38.16 < 2 6 4 0 14.42 -63.59 31.80 < 2 6 4 1 14.11 59.35 31.80 < 4 6 4 -1 38.88 108.11 55.11 < 4 6 4 0 64.81 -6.36 133.55 < 4 6 4 1 31.81 91.15 33.92 o 6 6 4 -1 65.63 50.87 36.04 < 6 6 4 0 86.37 63.59 42.40 < 6 6 4 1 30.77 42.40 23.32 < 8 6 4 -1 4.05 -69.95 38.16 < 8 6 4 0 19.22 48.75 74.19 < 8 6 4 1 0.52 80.55 29.68 o 10 6 4 -1 38.83 -12.72 93.27 < 10 6 4 0 4.02 -116.59 133.55 < 10 6 4 1 0.34 -42.40 40.28 < 12 6 4 1 0.16 -120.83 131.43 < -11 7 4 -1 22.97 -14.84 137.79 < -11 7 4 0 2.65 -57.23 133.55 < -11 7 4 1 5.77 -27.56 112.35 < -9 7 4 0 4.39 -25.44 110.23 < -9 7 4 1 1.13 80.55 108.11 < -7 7 4 1 1.88 25.44 89.03 < -5 7 4 1 0.20 190.78 91.15 < -3 7 4 1 2.48 16.96 97.51 < -1 7 4 1 10.27 46.63 84.79 < 1 7 4 -1 5.56 8.48 31.80 < 1 7 4 0 3.49 -69.95 112.35 < 1 7 4 1 1.74 80.55 33.92 < 3 7 4 -1 4.62 -16.96 29.68 < 3 7 4 0 1.28 29.68 59.35 < 3 7 4 1 0.03 -4.24 25.44 < 5 7 4 -1 0.14 2.12 61.47 < 5 7 4 0 1.78 93.27 125.07 < 5 7 4 1 0.39 52.99 91.15 < 7 7 4 -1 1.40 -12.72 99.63 < 7 7 4 0 3.06 114.47 195.02 < 7 7 4 1 10.72 72.07 52.99 < 9 7 4 0 11.04 69.95 48.75 < 9 7 4 1 3.76 2.12 52.99 < -4 8 4 -1 3.66 -86.91 74.19 < -2 8 4 -1 12.97 -16.96 40.28 < -2 8 4 0 4.05 -25.44 52.99 < -2 8 4 1 0.25 -120.83 120.83 < 0 8 4 -1 23.33 -19.08 93.27 < 0 8 4 0 4.27 29.68 114.47 < 0 8 4 1 3.97 4.24 36.04 < 2 8 4 -1 11.44 6.36 67.83 < 2 8 4 0 1.05 -50.87 114.47 < 2 8 4 1 1.30 -91.15 86.91 < 4 8 4 -1 8.06 42.40 31.80 < 4 8 4 0 3.67 -21.20 40.28 < 4 8 4 1 2.88 -63.59 36.04 < -18 0 5 0 5.86 -31.80 122.95 < -16 0 5 0 33.56 33.92 110.23 < -12 0 5 0 1867.91 2058.30 199.26 o -10 0 5 0 177.51 417.60 144.15 o -8 0 5 0 1155.29 1416.01 197.14 o -6 0 5 0 490.45 459.99 33.92 o -4 0 5 0 3684.33 3461.59 313.73 o -2 0 5 0 6184.20 6081.63 457.87 o 0 0 5 0 2981.14 2969.80 105.99 o 2 0 5 0 689.16 794.91 57.23 o 4 0 5 0 110.24 76.31 27.56 o 6 0 5 0 288.00 262.85 67.83 o 8 0 5 0 6.97 -25.44 44.52 < 10 0 5 0 228.69 65.71 46.63 < -19 1 5 -1 0.17 -110.23 38.16 < -19 1 5 0 75.69 59.35 40.28 < -19 1 5 1 6.85 65.71 36.04 < -17 1 5 -1 0.15 21.20 97.51 < -17 1 5 0 61.47 192.90 125.07 < -17 1 5 1 3.59 67.83 36.04 < -15 1 5 -1 1.45 -55.11 31.80 < -15 1 5 0 1514.98 1653.42 148.38 o -15 1 5 1 6.53 27.56 93.27 < -13 1 5 -1 2.13 14.84 31.80 < -13 1 5 0 82.92 110.23 133.55 < -13 1 5 1 1.04 33.92 33.92 < -11 1 5 -1 9.75 -4.24 31.80 < -11 1 5 0 542.65 451.51 52.99 o -11 1 5 1 4.34 16.96 31.80 < -9 1 5 -1 38.38 25.44 31.80 < -9 1 5 0 155.47 209.86 36.04 o -9 1 5 1 0.33 -12.72 36.04 < -7 1 5 -1 6.44 16.96 21.20 < -7 1 5 0 3544.98 3936.42 93.27 o -7 1 5 1 41.04 16.96 27.56 < -5 1 5 -1 81.84 69.95 25.44 o -5 1 5 0 481.68 489.67 27.56 o -5 1 5 1 29.63 6.36 19.08 < -3 1 5 -1 5.73 -14.84 40.28 < -3 1 5 0 46.81 31.80 31.80 < -3 1 5 1 0.53 57.23 23.32 < -1 1 5 -1 12.34 29.68 29.68 < -1 1 5 0 18164.70 17581.40 633.81 o -1 1 5 1 723.79 911.50 50.87 o 1 1 5 -1 85.95 2.12 19.08 < 1 1 5 0 2052.04 1952.31 69.95 o 1 1 5 1 45.11 48.75 25.44 < 3 1 5 -1 89.02 133.55 19.08 o 3 1 5 0 7.58 14.84 19.08 < 3 1 5 1 32.75 36.04 19.08 < 5 1 5 -1 178.72 165.34 27.56 o 5 1 5 0 95.52 2.12 23.32 < 5 1 5 1 306.28 190.78 40.28 o 7 1 5 -1 57.53 10.60 36.04 < 7 1 5 0 12.11 137.79 27.56 o 7 1 5 1 33.85 16.96 38.16 < 9 1 5 -1 13.74 21.20 33.92 < 9 1 5 0 138.05 95.39 55.11 < 9 1 5 1 0.82 12.72 29.68 < 11 1 5 -1 1.23 -4.24 63.59 < 11 1 5 0 46.29 78.43 67.83 < 11 1 5 1 13.53 -14.84 29.68 < 13 1 5 1 4.88 33.92 36.04 < 15 1 5 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-3 5 5 -1 2.07 -40.28 25.44 < -3 5 5 0 1.39 14.84 31.80 < -3 5 5 1 78.14 91.15 27.56 o -1 5 5 -1 32.72 105.99 31.80 o -1 5 5 0 569.95 597.78 40.28 o -1 5 5 1 726.35 674.09 40.28 o 1 5 5 -1 35.21 108.11 23.32 o 1 5 5 0 129.79 82.67 23.32 o 1 5 5 1 80.73 14.84 25.44 < 3 5 5 -1 35.30 16.96 29.68 < 3 5 5 0 0.82 21.20 29.68 < 3 5 5 1 20.26 -29.68 33.92 < 5 5 5 -1 57.76 110.23 25.44 o 5 5 5 0 1.80 -40.28 36.04 < 5 5 5 1 115.62 78.43 55.11 < 7 5 5 -1 70.55 65.71 21.20 o 7 5 5 0 5.24 -27.56 42.40 < 7 5 5 1 63.57 44.52 29.68 < 9 5 5 -1 16.47 -4.24 33.92 < 9 5 5 0 4.49 -72.07 46.63 < 9 5 5 1 12.60 38.16 33.92 < 11 5 5 -1 18.59 27.56 61.47 < 11 5 5 0 0.15 -31.80 63.59 < 11 5 5 1 18.08 50.87 52.99 < 13 5 5 0 27.57 42.40 118.71 < 13 5 5 1 11.03 -8.48 38.16 < -14 6 5 -1 0.55 42.40 103.87 < -14 6 5 0 0.95 -69.95 142.02 < -12 6 5 -1 1.46 16.96 97.51 < -12 6 5 0 10.99 67.83 116.59 < -12 6 5 1 18.85 105.99 108.11 < -10 6 5 -1 6.60 -16.96 112.35 < -10 6 5 0 13.32 252.25 125.07 < -10 6 5 1 8.12 -44.52 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0 0 6 0 16490.00 15680.00 360.36 o 2 0 6 0 2661.97 2933.77 82.67 o 4 0 6 0 2681.61 2753.59 93.27 o 6 0 6 0 436.76 642.29 61.47 o 8 0 6 0 611.36 691.05 57.23 o 10 0 6 0 120.98 135.66 48.75 o -19 1 6 -1 5.33 -21.20 36.04 < -19 1 6 0 360.53 358.24 48.75 o -19 1 6 1 0.98 0.00 67.83 < -17 1 6 -1 0.39 -4.24 27.56 < -17 1 6 0 189.26 250.13 50.87 o -17 1 6 1 0.02 -42.40 31.80 < -15 1 6 -1 32.17 2.12 97.51 < -15 1 6 1 8.34 101.75 125.07 < -13 1 6 -1 0.28 74.19 42.40 < -13 1 6 0 846.40 748.28 127.19 o -13 1 6 1 79.07 252.25 44.52 o -11 1 6 -1 0.70 -29.68 33.92 < -11 1 6 0 3226.33 3556.98 211.98 o -11 1 6 1 4.35 61.47 48.75 < -9 1 6 -1 177.55 59.35 31.80 < -9 1 6 0 7217.49 7133.04 165.34 o -9 1 6 1 49.81 42.40 40.28 < -7 1 6 -1 57.54 131.43 44.52 o -7 1 6 0 396.10 347.64 33.92 o -7 1 6 1 4.20 38.16 42.40 < -5 1 6 -1 291.84 220.46 25.44 o -5 1 6 0 1891.68 1770.01 82.67 o -5 1 6 1 295.91 150.50 36.04 o -3 1 6 -1 17.70 14.84 36.04 < -3 1 6 0 894.87 979.34 40.28 o -3 1 6 1 0.02 -21.20 21.20 < -1 1 6 -1 603.38 744.04 38.16 o -1 1 6 0 8860.13 8922.12 451.51 o -1 1 6 1 7.14 -8.48 36.04 < 1 1 6 -1 225.85 237.41 27.56 o 1 1 6 0 910.70 1204.03 44.52 o 1 1 6 1 661.95 563.86 29.68 o 3 1 6 -1 1.35 44.52 23.32 < 3 1 6 0 4038.36 2901.97 413.36 o 3 1 6 1 129.22 122.95 23.32 o 5 1 6 -1 10.47 29.68 33.92 < 5 1 6 0 11127.90 10382.60 186.54 o 5 1 6 1 65.74 31.80 40.28 < 7 1 6 -1 44.44 14.84 48.75 < 7 1 6 0 3513.44 3675.69 65.71 o 7 1 6 1 35.91 108.11 36.04 o 9 1 6 -1 31.41 50.87 33.92 < 9 1 6 0 272.05 180.18 57.23 o 9 1 6 1 7.46 67.83 27.56 < 11 1 6 -1 1.93 116.59 46.63 < 11 1 6 0 648.05 629.57 42.40 o 11 1 6 1 21.84 -23.32 65.71 < 13 1 6 -1 9.61 -114.47 93.27 < 13 1 6 1 6.08 78.43 129.31 < 15 1 6 -1 0.02 6.36 95.39 < 15 1 6 0 74.94 -31.80 131.43 < 15 1 6 1 0.22 48.75 93.27 < -18 2 6 -1 1.21 23.32 50.87 < -18 2 6 0 18.43 72.07 57.23 < -18 2 6 1 0.59 -78.43 67.83 < -16 2 6 -1 3.50 -25.44 33.92 < -16 2 6 0 0.04 21.20 40.28 < -16 2 6 1 7.64 10.60 36.04 < -14 2 6 -1 6.29 -29.68 40.28 < -14 2 6 0 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504.51 65.71 o 8 2 6 1 13.81 63.59 31.80 < 10 2 6 -1 67.08 108.11 29.68 o 10 2 6 0 33.22 16.96 52.99 < 10 2 6 1 0.50 -8.48 29.68 < 12 2 6 1 23.22 -48.75 103.87 < 14 2 6 -1 1.11 120.83 137.79 < 14 2 6 0 9.32 19.08 48.75 < 14 2 6 1 10.08 65.71 112.35 < -19 3 6 -1 22.63 -55.11 74.19 < -17 3 6 -1 3.43 -23.32 36.04 < -17 3 6 0 75.68 142.02 57.23 < -17 3 6 1 0.17 -48.75 44.52 < -15 3 6 -1 96.31 116.59 33.92 o -15 3 6 0 413.31 521.46 40.28 o -15 3 6 1 36.82 44.52 65.71 < -13 3 6 -1 1.04 -23.32 33.92 < -13 3 6 0 464.30 394.28 40.28 o -13 3 6 1 306.93 237.41 38.16 o -11 3 6 -1 13.08 -8.48 29.68 < -11 3 6 0 1104.76 1165.88 59.35 o -11 3 6 1 37.76 33.92 23.32 < -9 3 6 -1 228.62 101.75 29.68 o -9 3 6 0 2737.99 2505.57 84.79 o -9 3 6 1 20.95 63.59 27.56 < -7 3 6 -1 325.10 459.99 55.11 o -7 3 6 0 441.48 351.88 38.16 o -7 3 6 1 86.95 2.12 33.92 < -5 3 6 -1 31.61 14.84 91.15 < -5 3 6 0 913.31 989.93 127.19 o -5 3 6 1 112.14 12.72 50.87 < -3 3 6 1 85.54 -14.84 125.07 < -1 3 6 -1 1897.16 1772.13 169.58 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-12.72 52.99 < 11 1 7 -1 31.58 125.07 112.35 < 11 1 7 0 1944.80 2020.14 188.66 o 11 1 7 1 11.22 16.96 78.43 < 13 1 7 -1 10.73 -69.95 42.40 < 13 1 7 0 573.19 398.52 150.50 o 13 1 7 1 7.78 16.96 46.63 < -18 2 7 -1 2.14 12.72 36.04 < -18 2 7 0 82.27 67.83 50.87 < -18 2 7 1 8.83 63.59 101.75 < -16 2 7 -1 33.76 -21.20 31.80 < -16 2 7 0 166.40 129.31 38.16 o -16 2 7 1 2.37 72.07 33.92 < -14 2 7 -1 31.19 99.63 40.28 < -14 2 7 0 282.28 256.49 46.63 o -14 2 7 1 17.03 14.84 48.75 < -12 2 7 -1 15.33 -23.32 31.80 < -12 2 7 0 1023.15 1276.10 144.15 o -12 2 7 1 1.00 8.48 46.63 < -10 2 7 -1 25.56 6.36 27.56 < -10 2 7 0 222.13 235.29 29.68 o -10 2 7 1 84.50 99.63 25.44 o -8 2 7 -1 31.89 40.28 29.68 < -8 2 7 0 100.71 99.63 25.44 o -8 2 7 1 69.28 14.84 29.68 < -6 2 7 -1 160.49 61.47 27.56 < -6 2 7 1 147.88 -36.04 97.51 < -4 2 7 -1 18.52 23.32 25.44 < -4 2 7 0 2528.58 2393.22 72.07 o -4 2 7 1 172.88 264.97 36.04 o -2 2 7 -1 706.72 328.57 163.22 < -2 2 7 0 12466.60 5786.98 5842.09 < -2 2 7 1 50.37 67.83 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3 7 0 201.79 148.38 133.55 < 13 3 7 1 26.27 -10.60 31.80 < -18 4 7 -1 2.93 0.00 108.11 < -16 4 7 -1 49.37 114.47 105.99 < -16 4 7 0 38.19 31.80 137.79 < -16 4 7 1 3.80 -78.43 99.63 < -14 4 7 -1 31.43 207.74 86.91 < -14 4 7 0 46.25 84.79 112.35 < -14 4 7 1 26.86 112.35 103.87 < -12 4 7 -1 19.85 0.00 38.16 < -12 4 7 0 185.60 426.07 82.67 o -12 4 7 1 2.72 118.71 33.92 o -10 4 7 -1 7.66 36.04 31.80 < -10 4 7 0 75.11 63.59 38.16 < -10 4 7 1 96.53 27.56 63.59 < -8 4 7 -1 151.39 182.30 48.75 o -8 4 7 0 73.17 89.03 61.47 < -8 4 7 1 7.82 -27.56 44.52 < -6 4 7 -1 433.28 298.89 38.16 o -6 4 7 0 718.17 741.92 46.63 o -6 4 7 1 574.48 298.89 78.43 o -4 4 7 -1 9.86 44.52 36.04 < -4 4 7 0 613.83 661.37 80.55 o -4 4 7 1 136.49 93.27 114.47 < -2 4 7 -1 784.62 860.63 48.75 o -2 4 7 0 3689.51 3692.64 86.91 o -2 4 7 1 10.54 -14.84 36.04 < 0 4 7 -1 1053.48 915.74 320.09 o 0 4 7 0 3221.44 2232.12 788.56 o 0 4 7 1 201.41 91.15 36.04 o 2 4 7 -1 290.90 466.35 65.71 o 2 4 7 0 181.01 74.19 27.56 o 2 4 7 1 4.34 -2.12 25.44 < 4 4 7 -1 260.17 491.79 52.99 o 4 4 7 0 485.84 445.15 31.80 o 4 4 7 1 320.73 262.85 29.68 o 6 4 7 -1 0.61 23.32 29.68 < 6 4 7 0 435.92 436.67 40.28 o 6 4 7 1 391.94 326.45 33.92 o 8 4 7 -1 2.18 67.83 44.52 < 8 4 7 0 25.73 4.24 84.79 < 8 4 7 1 12.38 33.92 63.59 < 10 4 7 -1 62.92 -10.60 84.79 < 10 4 7 0 98.42 38.16 48.75 < 10 4 7 1 10.84 -10.60 33.92 < 12 4 7 -1 0.02 25.44 69.95 < -15 5 7 -1 43.92 19.08 112.35 < -15 5 7 0 36.66 80.55 137.79 < -15 5 7 1 8.81 -61.47 89.03 < -13 5 7 -1 181.49 110.23 110.23 < -13 5 7 0 172.16 243.77 131.43 < -13 5 7 1 5.42 50.87 110.23 < -11 5 7 -1 115.88 122.95 57.23 < -11 5 7 0 82.36 101.75 131.43 < -11 5 7 1 0.21 59.35 33.92 < -9 5 7 -1 226.64 241.65 40.28 o -9 5 7 0 85.51 69.95 40.28 < -9 5 7 1 83.60 101.75 36.04 o -7 5 7 -1 16.04 118.71 76.31 < -7 5 7 0 72.93 93.27 42.40 < -7 5 7 1 237.21 419.71 44.52 o -5 5 7 -1 1.41 36.04 50.87 < -5 5 7 0 201.99 118.71 42.40 o -5 5 7 1 2.44 33.92 38.16 < -3 5 7 -1 397.01 387.92 137.79 o -3 5 7 0 213.62 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100.64 228.94 144.15 < -6 6 7 1 125.37 186.54 50.87 o -4 6 7 -1 5.59 -6.36 114.47 < -4 6 7 0 98.55 89.03 135.66 < -4 6 7 1 21.28 -40.28 129.31 < -2 6 7 -1 306.30 267.09 31.80 o -2 6 7 0 311.05 273.45 52.99 o -2 6 7 1 2.79 12.72 55.11 < 0 6 7 -1 320.49 392.16 40.28 o 0 6 7 0 208.39 245.89 146.26 < 0 6 7 1 48.84 31.80 112.35 < 2 6 7 -1 84.48 50.87 27.56 < 2 6 7 0 37.26 8.48 61.47 < 2 6 7 1 0.33 -2.12 33.92 < 4 6 7 -1 77.68 103.87 25.44 o 4 6 7 0 43.13 -59.35 59.35 < 4 6 7 1 88.14 65.71 27.56 < 6 6 7 -1 1.60 -33.92 27.56 < 6 6 7 0 43.05 21.20 67.83 < 6 6 7 1 100.75 40.28 42.40 < 8 6 7 -1 1.37 57.23 36.04 < 8 6 7 0 2.38 -36.04 59.35 < 8 6 7 1 2.22 33.92 31.80 < 10 6 7 1 2.79 -31.80 36.04 < -11 7 7 -1 31.28 40.28 116.59 < -11 7 7 0 10.29 0.00 118.71 < -9 7 7 -1 37.26 25.44 89.03 < -9 7 7 0 3.02 36.04 120.83 < -9 7 7 1 8.27 129.31 103.87 < -5 7 7 1 1.55 50.87 80.55 < -3 7 7 -1 57.08 82.67 144.15 < -3 7 7 0 3.20 -169.58 125.07 < -3 7 7 1 0.44 -46.63 42.40 < -1 7 7 -1 8.48 -31.80 40.28 < -1 7 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10.93 -112.35 80.55 < 11 3 8 -1 33.74 -80.55 110.23 < 11 3 8 0 2.60 -118.71 129.31 < 11 3 8 1 1.36 21.20 108.11 < 13 3 8 0 35.02 27.56 129.31 < 13 3 8 1 6.03 42.40 91.15 < -16 4 8 -1 0.65 -38.16 97.51 < -16 4 8 0 7.44 -25.44 116.59 < -16 4 8 1 4.70 -4.24 82.67 < -14 4 8 -1 91.73 110.23 38.16 o -14 4 8 0 125.96 158.98 52.99 o -14 4 8 1 134.08 171.70 103.87 < -12 4 8 -1 5.86 -23.32 31.80 < -12 4 8 0 103.52 63.59 76.31 < -12 4 8 1 105.95 224.70 67.83 o -10 4 8 -1 74.17 80.55 31.80 o -10 4 8 0 320.58 347.64 80.55 o -10 4 8 1 3.25 89.03 31.80 o -8 4 8 -1 36.45 91.15 42.40 < -8 4 8 0 188.16 133.55 44.52 o -8 4 8 1 500.70 631.69 131.43 o -6 4 8 -1 119.41 52.99 44.52 < -6 4 8 0 259.33 269.21 36.04 o -6 4 8 1 305.22 351.88 40.28 o -4 4 8 -1 211.43 139.90 46.63 o -4 4 8 0 0.06 -57.23 46.63 < -4 4 8 1 272.74 135.66 50.87 o -2 4 8 -1 213.24 245.89 55.11 o -2 4 8 0 459.70 724.96 65.71 o -2 4 8 1 311.84 343.40 38.16 o 0 4 8 -1 245.73 375.20 36.04 o 0 4 8 0 0.72 42.40 40.28 < 0 4 8 1 12.19 52.99 33.92 < 2 4 8 -1 4.18 67.83 29.68 < 2 4 8 0 181.10 105.99 33.92 o 2 4 8 1 61.56 169.58 46.63 o 4 4 8 -1 433.17 559.62 50.87 o 4 4 8 0 877.67 724.96 82.67 o 4 4 8 1 1.35 6.36 27.56 < 6 4 8 -1 333.45 326.45 46.63 o 6 4 8 0 496.69 536.30 57.23 o 6 4 8 1 91.85 50.87 46.63 < 8 4 8 -1 20.98 -57.23 50.87 < 8 4 8 0 5.67 154.74 65.71 < 8 4 8 1 0.56 14.84 108.11 < 10 4 8 -1 34.44 27.56 40.28 < 10 4 8 0 14.50 -12.72 129.31 < 10 4 8 1 14.68 -31.80 44.52 < 12 4 8 -1 0.08 2.12 91.15 < -15 5 8 -1 2.93 -31.80 103.87 < -15 5 8 0 65.79 -118.71 146.26 < -15 5 8 1 62.86 173.82 95.39 < -13 5 8 -1 57.13 23.32 82.67 < -13 5 8 0 15.44 40.28 142.02 < -13 5 8 1 3.74 44.52 33.92 < -11 5 8 -1 1.91 -38.16 48.75 < -11 5 8 0 0.29 -52.99 42.40 < -11 5 8 1 14.97 33.92 65.71 < -9 5 8 -1 74.85 76.31 38.16 < -9 5 8 0 11.23 -29.68 38.16 < -9 5 8 1 82.87 52.99 67.83 < -7 5 8 -1 402.60 334.92 36.04 o -7 5 8 0 208.88 144.15 48.75 o -7 5 8 1 64.32 55.11 38.16 < -5 5 8 -1 187.99 379.44 52.99 o -5 5 8 0 1.88 36.04 42.40 < -5 5 8 1 39.18 118.71 59.35 < -3 5 8 -1 75.41 337.04 131.43 o -3 5 8 0 6.71 91.15 139.90 < -3 5 8 1 78.92 404.88 139.90 o -1 5 8 -1 154.22 245.89 42.40 o -1 5 8 0 302.21 262.85 42.40 o -1 5 8 1 443.79 555.38 44.52 o 1 5 8 -1 26.45 -8.48 44.52 < 1 5 8 0 22.58 25.44 27.56 < 1 5 8 1 39.75 133.55 42.40 o 3 5 8 -1 66.53 33.92 36.04 < 3 5 8 0 30.44 -16.96 65.71 < 3 5 8 1 15.38 10.60 27.56 < 5 5 8 -1 7.26 -50.87 27.56 < 5 5 8 0 9.51 -16.96 52.99 < 5 5 8 1 237.62 201.38 31.80 o 7 5 8 -1 10.04 31.80 29.68 < 7 5 8 0 36.81 -69.95 131.43 < 7 5 8 1 0.11 8.48 44.52 < 9 5 8 -1 20.16 -82.67 165.34 < 9 5 8 0 8.96 -156.86 154.74 < 9 5 8 1 9.45 -57.23 91.15 < 11 5 8 0 0.90 -2.12 55.11 < 11 5 8 1 1.13 -25.44 40.28 < -14 6 8 -1 21.18 76.31 84.79 < -12 6 8 -1 1.09 -21.20 38.16 < -12 6 8 0 10.80 80.55 82.67 < -12 6 8 1 38.90 46.63 33.92 < -10 6 8 -1 23.08 114.47 40.28 o -10 6 8 0 28.00 76.31 59.35 < -10 6 8 1 12.15 -27.56 44.52 < -8 6 8 -1 1.05 25.44 38.16 < -8 6 8 0 8.95 72.07 63.59 < -8 6 8 1 165.82 209.86 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118.71 < -1 7 8 0 2.91 -6.36 156.86 < -1 7 8 1 66.01 195.02 97.51 < 1 7 8 -1 6.01 89.03 50.87 < 1 7 8 0 1.17 -52.99 150.50 < 1 7 8 1 7.02 -52.99 112.35 < 3 7 8 -1 7.46 55.11 40.28 < 3 7 8 0 0.15 -52.99 44.52 < 3 7 8 1 5.88 -4.24 59.35 < 5 7 8 -1 0.21 46.63 36.04 < 5 7 8 0 0.21 8.48 44.52 < 5 7 8 1 47.69 19.08 36.04 < -18 0 9 0 0.43 40.28 146.26 < -16 0 9 0 1.64 -8.48 129.31 < -14 0 9 0 304.68 303.13 142.02 < -12 0 9 0 1051.84 1085.32 146.26 o -10 0 9 0 94.62 112.35 33.92 o -6 0 9 0 9145.38 10270.30 383.68 o -4 0 9 0 5811.90 5197.68 648.65 o -2 0 9 0 10445.20 10662.50 152.62 o 0 0 9 0 1154.38 1318.50 52.99 o 2 0 9 0 506.80 604.14 154.74 o 4 0 9 0 3802.01 4814.00 95.39 o 6 0 9 0 373.12 97.51 46.63 < 8 0 9 0 288.91 12.72 50.87 < 10 0 9 0 300.72 296.77 129.31 < 12 0 9 0 298.14 298.89 142.02 < -19 1 9 -1 5.28 -46.63 40.28 < -19 1 9 0 784.03 756.76 125.07 o -17 1 9 -1 1.58 80.55 101.75 < -17 1 9 0 404.37 563.86 163.22 o -17 1 9 1 0.06 10.60 57.23 < -15 1 9 -1 37.82 101.75 29.68 o -15 1 9 0 1663.96 1587.71 82.67 o -15 1 9 1 1.72 -36.04 46.63 < -13 1 9 -1 6.16 27.56 36.04 < -13 1 9 0 784.29 894.54 72.07 o -13 1 9 1 40.61 125.07 38.16 o -11 1 9 -1 0.01 -57.23 25.44 < -11 1 9 0 498.20 701.65 52.99 o -11 1 9 1 29.79 108.11 46.63 < -9 1 9 -1 49.35 31.80 114.47 < -9 1 9 0 10148.50 4597.79 4644.42 < -9 1 9 1 101.09 135.66 40.28 o -5 1 9 -1 18.15 -12.72 38.16 < -5 1 9 0 557.25 510.86 154.74 o -5 1 9 1 175.62 241.65 137.79 < -3 1 9 -1 3.25 23.32 46.63 < -3 1 9 0 64.96 131.43 44.52 o -3 1 9 1 2.68 27.56 48.75 < -1 1 9 -1 78.40 156.86 42.40 o -1 1 9 0 2639.68 2486.49 69.95 o -1 1 9 1 2.70 -23.32 55.11 < 1 1 9 -1 47.44 -4.24 52.99 < 1 1 9 0 640.60 608.38 50.87 o 1 1 9 1 145.57 36.04 76.31 < 3 1 9 -1 10.33 42.40 33.92 < 3 1 9 0 187.01 250.13 46.63 o 3 1 9 1 37.93 72.07 48.75 < 5 1 9 -1 6.50 -8.48 29.68 < 5 1 9 0 9480.18 8050.90 137.79 o 5 1 9 1 136.28 125.07 36.04 o 7 1 9 -1 0.80 -50.87 29.68 < 7 1 9 0 393.33 786.44 59.35 o 7 1 9 1 8.84 2.12 29.68 < 9 1 9 -1 35.40 -8.48 36.04 < 9 1 9 0 761.97 332.80 135.66 < 9 1 9 1 10.91 -86.91 110.23 < 11 1 9 -1 0.61 -59.35 91.15 < 11 1 9 1 4.55 27.56 46.63 < 13 1 9 -1 3.00 120.83 93.27 < 13 1 9 1 0.11 97.51 120.83 < -18 2 9 -1 0.18 -6.36 36.04 < -18 2 9 0 0.01 -33.92 38.16 < -18 2 9 1 7.74 -36.04 40.28 < -16 2 9 -1 9.35 -31.80 31.80 < -16 2 9 0 0.65 36.04 40.28 < -16 2 9 1 0.11 57.23 42.40 < -14 2 9 -1 33.30 -14.84 36.04 < -14 2 9 0 125.87 63.59 52.99 < -14 2 9 1 12.21 -23.32 25.44 < -12 2 9 -1 35.80 63.59 29.68 < -12 2 9 0 800.29 777.96 93.27 o -12 2 9 1 93.11 122.95 29.68 o -10 2 9 -1 23.75 72.07 52.99 < -10 2 9 0 123.20 252.25 105.99 < -10 2 9 1 107.85 188.66 31.80 o -8 2 9 -1 267.63 74.19 72.07 < -8 2 9 0 8982.35 5814.54 1532.60 o -8 2 9 1 883.82 650.77 84.79 o -6 2 9 -1 42.78 93.27 110.23 < -6 2 9 1 410.55 -40.28 120.83 < -4 2 9 -1 136.53 267.09 52.99 o -4 2 9 0 5071.64 5062.02 175.94 o -4 2 9 1 20.04 -10.60 44.52 < -2 2 9 -1 507.62 525.70 144.15 o -2 2 9 0 4488.12 2202.44 2132.49 < -2 2 9 1 229.41 59.35 86.91 < 0 2 9 -1 0.62 -21.20 33.92 < 0 2 9 0 256.16 298.89 86.91 o 0 2 9 1 237.81 72.07 82.67 < 2 2 9 -1 19.28 6.36 27.56 < 2 2 9 0 378.90 381.56 201.38 < 2 2 9 1 21.43 52.99 38.16 < 4 2 9 -1 33.03 67.83 105.99 < 4 2 9 0 2302.53 3209.34 137.79 o 4 2 9 1 126.17 86.91 36.04 < 6 2 9 -1 3.28 12.72 29.68 < 6 2 9 0 138.20 14.84 29.68 < 6 2 9 1 0.10 -14.84 57.23 < 8 2 9 -1 12.03 -27.56 63.59 < 8 2 9 0 226.91 -29.68 69.95 < 8 2 9 1 31.60 6.36 44.52 < 10 2 9 -1 16.89 4.24 103.87 < 10 2 9 0 141.52 133.55 131.43 < 10 2 9 1 3.10 -50.87 97.51 < 12 2 9 -1 28.27 6.36 129.31 < 12 2 9 0 166.59 197.14 137.79 < -17 3 9 -1 9.70 63.59 44.52 < -17 3 9 0 180.03 385.80 69.95 o -17 3 9 1 0.09 -55.11 67.83 < -15 3 9 -1 148.56 165.34 27.56 o -15 3 9 0 671.81 729.20 42.40 o -15 3 9 1 19.24 -61.47 33.92 < -13 3 9 -1 22.00 42.40 33.92 < -13 3 9 0 467.52 381.56 52.99 o -13 3 9 1 167.30 262.85 29.68 o -11 3 9 -1 1.84 19.08 38.16 < -11 3 9 0 279.64 504.51 63.59 o -11 3 9 1 67.68 139.90 31.80 o -9 3 9 -1 59.31 2.12 38.16 < -9 3 9 0 3364.24 3135.14 80.55 o -9 3 9 1 211.93 169.58 36.04 o -7 3 9 -1 50.55 25.44 31.80 < -7 3 9 0 371.57 250.13 40.28 o -7 3 9 1 36.14 -19.08 42.40 < -5 3 9 -1 87.14 10.60 67.83 < -5 3 9 0 260.16 188.66 38.16 o -5 3 9 1 307.19 322.21 40.28 o -3 3 9 -1 1.99 16.96 33.92 < -3 3 9 0 566.60 428.19 101.75 o -3 3 9 1 5.55 -8.48 44.52 < -1 3 9 -1 693.43 735.56 57.23 o -1 3 9 0 1084.44 771.60 271.33 o -1 3 9 1 46.30 4.24 23.32 < 1 3 9 -1 31.34 103.87 38.16 o 1 3 9 0 75.88 -4.24 31.80 < 1 3 9 1 304.76 324.33 36.04 o 3 3 9 -1 42.54 167.46 78.43 < 3 3 9 0 160.92 199.26 33.92 o 3 3 9 1 88.50 105.99 31.80 o 5 3 9 -1 157.74 165.34 33.92 o 5 3 9 0 3639.51 3442.51 97.51 o 5 3 9 1 676.24 415.48 40.28 o 7 3 9 -1 16.97 42.40 112.35 < 7 3 9 0 110.07 169.58 144.15 < 7 3 9 1 17.93 31.80 97.51 < 9 3 9 1 18.49 -38.16 101.75 < 11 3 9 -1 6.88 -2.12 55.11 < 11 3 9 0 20.90 127.19 131.43 < 11 3 9 1 25.55 -33.92 108.11 < 13 3 9 1 0.08 -12.72 91.15 < -16 4 9 -1 11.67 10.60 99.63 < -16 4 9 0 0.45 80.55 139.90 < -16 4 9 1 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-7 1 11 1 0.63 -69.95 40.28 < -5 1 11 -1 4.75 55.11 46.63 < -5 1 11 0 169.67 69.95 46.63 < -5 1 11 1 12.05 21.20 38.16 < -3 1 11 -1 61.20 27.56 103.87 < -3 1 11 0 60.91 101.75 44.52 < -3 1 11 1 2.94 6.36 29.68 < -1 1 11 -1 1.57 -4.24 40.28 < -1 1 11 0 6.09 0.00 38.16 < -1 1 11 1 67.09 48.75 80.55 < 1 1 11 -1 69.93 27.56 40.28 < 1 1 11 0 341.31 430.31 142.02 o 1 1 11 1 0.11 -16.96 110.23 < 3 1 11 -1 9.38 -25.44 42.40 < 3 1 11 0 394.24 288.29 33.92 o 3 1 11 1 0.89 -10.60 33.92 < 5 1 11 -1 31.94 8.48 27.56 < 5 1 11 0 221.98 6.36 38.16 < 5 1 11 1 7.48 36.04 33.92 < 7 1 11 -1 5.52 -6.36 36.04 < 7 1 11 0 1582.21 1401.17 122.95 o 7 1 11 1 10.07 -4.24 42.40 < 9 1 11 -1 5.10 25.44 46.63 < 9 1 11 0 123.44 131.43 44.52 o 9 1 11 1 0.02 46.63 42.40 < 11 1 11 1 0.04 -29.68 97.51 < -18 2 11 -1 2.77 46.63 67.83 < -18 2 11 0 3.32 21.20 40.28 < -16 2 11 -1 10.34 4.24 29.68 < -16 2 11 0 1.85 33.92 57.23 < -16 2 11 1 1.12 -14.84 31.80 < -14 2 11 -1 22.73 -6.36 89.03 < -14 2 11 0 20.06 36.04 84.79 < -14 2 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455.75 55.11 o -10 2 19 -1 2.00 -50.87 52.99 < -8 2 19 -1 1.24 -82.67 99.63 < -8 2 19 0 651.08 837.31 144.15 o -6 2 19 -1 2.05 57.23 42.40 < -6 2 19 0 300.96 413.36 78.43 o -4 2 19 -1 80.36 -21.20 63.59 < -4 2 19 0 578.68 523.58 52.99 o -2 2 19 -1 5.13 59.35 48.75 < -7 1 20 -1 2.22 16.96 31.80 < -5 1 20 -1 0.34 2.12 50.87 < # For import please use the tool: #"Structure->New->from Jana2020 embedded in CIF" _Jana_m40_file ; 0 2 0 1 0 24 1 5 1 0.217198 0.000000 0.000000 0.000000 0.000000 0.000000 100000 0.000000 0.000000 0.000000 000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 000000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 000000 Tsc 0 1 Cu1 Cu1 7 0 1.000000 0.225531 0.500000 0.146695 000 0 0 0 0.000000 0.000000 0.000000-0.000000 0.000000-0.000000 0000000000 S1 5 0 1.000000 0.067279 0.500000 0.126925 000 0 0 0 0.000000 0.000000 0.000000-0.000000 0.000000 0.000000 0101000000 S2 5 0 1.000000 0.235109 0.500000-0.160205 000 0 0 0 0.000000 0.000000 0.000000-0.000000 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0.000000 0.000000 0.000000 0.000000 H4n2 0.000000 0.000807 0.000000 0.000522 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 H4n1 0.000000 0.000456 0.000000 0.000753 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 N5 0.000000 0.000475 0.000000 0.000474 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C1 0.000000 0.000614 0.000000 0.000687 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 H1 0.000000-0.100000-0.100000-0.100000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C2 0.000000 0.000651 0.000000 0.000692 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 H2 0.000000-0.100000-0.100000-0.100000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C3 0.000000 0.000738 0.000000 0.000750 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 H3 0.000000-0.100000-0.100000-0.100000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C4 0.000000 0.000622 0.000000 0.000714 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 H4 0.000000-0.100000-0.100000-0.100000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C5 0.000000 0.000675 0.000000 0.000634 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C6 0.000000 0.000628 0.000000 0.000624 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 H6 0.000000-0.100000-0.100000-0.100000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C7 0.000000 0.000647 0.000000 0.000571 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 C8 0.000000 0.000592 0.000000 0.000586 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 pos#1 0.000000 0.000 0.000 0.000 0.000073 0.000000 0.000069 0.000059 0.000391 0.000045 0.000000 0.000037 0.000000 0.000016 0.000038 0.000020 0.000000 0.000022 0.000000 0.000000 0.000073 0.000000 0.000035 0.000000 0.000028 0.000000 0.000071 0.000000 0.000000 0.000252 0.000000 0.000000 0.000291 0.000000 0.000060 0.000000 0.000085 0.000058 0.000000 0.000088 0.000000 Clo4 Cl1 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 O1 0.000000 0.002501 0.007170 0.003105 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 O2 0.000000 0.002106 0.007207 0.002156 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 O3 0.000000 0.002329 0.007368 0.001971 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 O4 0.000000 0.002562 0.007552 0.002731 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 pos#1 0.000000 0.000 0.000 0.000 0.002424 0.006785 0.001701 0.000259 0.001017 0.000115 0.000502 0.000122 0.000417 0.000759 0.004459 0.000914 0.000861 0.000493 0.000975 0.000654 0.000740 0.000290 0.000849 0.002863 0.000714 0.000398 0.000949 0.000000 0.000000 0.003025 0.000000 0.003646 0.008525 0.002539 0.001067 0.001419 0.000906 0.004529 0.000000 0.004263 0.001219 0.000000 0.001291 0.000000 -------------------------- Saved points ------------------------------------ 0 -------------------------- Critical points --------------------------------- 0 -------------------------- Fourier maxima ---------------------------------- 1 1 1 Max1 1 1 1.000000 0.551669 0.004981 0.170060 000 0 1 0 0.98 0.57 0.001244 0.008836 0.000977-0.005868-0.041411-0.007036 0.000000 Max2 1 1 1.000000 0.048653 0.044220 0.251940 000 0 1 0 1.20 0.57 0.007019-0.000015-0.004079 0.005286-0.011744-0.001297 0.000000 Max3 1 1 1.000000 0.361434 0.004397 0.386581 000 0 1 0 0.77 0.57 0.001223 0.021590 0.001333 0.008725 0.056916 0.000874 0.000000 Max4 1 1 1.000000 0.884238 0.004884 0.240989 000 0 1 0 0.98 0.54 0.004693-0.009866-0.002536 0.003576-0.027223-0.001755 0.000000 Max5 1 1 1.000000 0.263031 0.071580 0.158739 000 0 1 0 0.95 0.54 -0.002786-0.009918-0.002268-0.000758 0.008557-0.001157 0.000000 Max6 1 1 1.000000 0.724802 0.020452 0.078317 000 0 1 0 0.88 0.52 -0.012986 0.015745 0.013989-0.008667 0.013323 0.018546 0.000000 Max7 1 1 1.000000 0.754147 0.035840 0.214753 000 0 1 0 0.74 0.52 -0.018263 0.029802 0.017297-0.010991-0.022662 0.007685 0.000000 Max8 1 1 1.000000 0.593625 0.009477 0.103209 000 0 1 0 0.94 0.50 0.003948-0.022876-0.003036-0.000061-0.019337-0.000867 0.000000 Max9 1 1 1.000000 0.008634 0.026195 0.155979 000 0 1 0 0.86 0.50 -0.013396 0.002986-0.004571 0.008378-0.020590 0.000728 0.000000 Max10 1 1 1.000000 0.914375 0.000800 0.108472 000 0 1 0 0.65 0.42 -0.001178 0.030004 0.001381-0.000409-0.022782-0.001108 0.000000 Max11 1 1 1.000000 0.224272 0.006937 0.063010 000 0 1 0 0.64 0.39 0.003126 0.013373 0.002686 0.002861-0.022100-0.000639 0.000000 Max12 1 1 1.000000 0.646708 0.093120 0.478555 000 0 1 0 0.67 0.39 -0.023506 0.001634-0.004273-0.017596-0.022517-0.014992 0.000000 -------------------------- Fourier minima ---------------------------------- 1 1 1 Min1 1 1 1.000000 0.718781 0.048322 0.145071 000 0 0 0 1.91 1.16 Min2 1 1 1.000000 0.721935 0.044171 0.151044 000 0 0 0 1.72 1.12 Min3 1 1 1.000000 0.715201 0.049689 0.138717 000 0 0 0 1.60 1.01 Min4 1 1 1.000000 0.724194 0.034391 0.159148 000 0 0 0 1.23 0.80 Min5 1 1 1.000000 0.047114 0.051263 0.295352 000 0 0 0 1.31 0.75 -------------------------------------------------------------------------------- ; _Jana_m50_file ; Version Jana2020 title sir97 run in space group c 2/m cell 14.9502 6.5697 15.0098 90 106.957 90 esdcell 0.0047 0.0017 0.0045 0 0.024 0 ndim 4 ncomp 1 qi -0.614888 0 0.345313 qr 0 0 0 spgroup C2/m(a0g)0s 12 22 lattice C symmetry x1 x2 x3 x4 symmetry -x1 x2 -x3 -x4+1/2 symmetry -x1 -x2 -x3 -x4 symmetry x1 -x2 x3 x4+1/2 unitsnumb 4 chemform C8 H8 N5 O4 S2 Cl Cu atlist C8 H8 N5 O4 S2 Cl Cu formtab -62 atom C atradius 0.77 color 128073041 atom H atradius 0.46 color 255204204 atom N atradius 0.74 color 176185230 atom O atradius 0.74 color 254003000 atom S atradius 1.04 color 255250000 atom Cl atradius 0.99 color 49252002 atom Cu atradius 1.28 color 34071220 roundmethod 1 end ******************************************************************************* contour tintmap 1 x4lim 0 2 0.02 drawatom Cl1a 0 2 end contour dist angles 1 hamax 2.62 end dist fourier maptype 6 positive 10 negative 5 usesnlim 1 snlmx 0.5 x4lim 0 0.9 0.1 end fourier refine cycles 100 skipbad 1 sinlim 1 wilsonmod 0 refexcl 10 snlmx 0.661 damp 0.5 siglevel 2.5 convlim 0.0005 !equation : xtcos1[Clo4#1]=0 !equation : xtsin1[Clo4#1]=0 !equation : ztcos1[Clo4#1]=0 !equation : ztsin1[Clo4#1]=0 equation : yrcos1[Clo4#1]=0 equation : yrsin1[Clo4#1]=0 !equation : xtcos1[Clo4#1]=xrcos1[Clo4#1] !equation : xtcos1[Clo4#1]=0.614888*x[Cl1]-0.345313*z[Cl1]+0.614888*xtrans[Clo &4#1]-0.345313*ztrans[Clo4#1]+0.5 !equation : xrcos1[Clo4#1]=0.614888*x[Cl1]-0.345313*z[Cl1]+0.614888*xtrans[Clo &4#1]-0.345313*ztrans[Clo4#1]+0.5 !equation : x40[Clo4#1]=-0.614888*0.348403+0.345313*0.451221-0.614888*xtrans[C &lo4#1]+0.345313*ztrans[Clo4#1]+0.0 !equation : x40[Clo4#2]=-0.614888*0.348403+0.345313*0.451221-0.614888*xtrans[C &lo4#2]+0.345313*ztrans[Clo4#2]+0.5 distfix 0.86 0.001 N4 H4N2; distfix = 0.001 N4 H4N2; N4 H4N1; !distfix 1.4 0.01 Cl1a O1a; !distfix = 0.1 Cl1a O1a; Cl1a O2a; Cl1a O3a; Cl1a O4a; anglefix 120 0.01 C7 N4 H4N1; anglefix = 0.01 C7 N4 H4N1; C7 N4 H4N2; !anglefix 109.47 0.01 O1a Cl1a O2a; !anglefix = 1 O1a Cl1a O2a; O1a Cl1a O3a; O1a Cl1a O4a; O2a Cl1a O3a; O2a Cl1a & O4a; O3a Cl1a O4a; keep hydro triang N3 2 1 N2 C7 0.86 H3N keep hydro triang C1 2 1 N1 C2 0.93 H1 keep hydro triang C2 2 1 C1 C3 0.93 H2 keep hydro triang C3 2 1 C2 C4 0.93 H3 keep hydro triang C4 2 1 C3 C5 0.93 H4 keep hydro triang C6 2 1 C5 N2 0.93 H6 keep ADP riding N3 1.5 H3N keep ADP riding C1 1.5 H1 keep ADP riding C2 1.5 H2 keep ADP riding C3 1.5 H3 keep ADP riding C4 1.5 H4 keep ADP riding C6 1.5 H6 keep ADP riding N4 1.5 H4N1 H4N2 keep geom rigidmod Cu1 S1 S2 N1 N2 N3 H3n N4 H4n2 H4n1 N5 C1 H1 C2 H2 C3 H3 C4 & H4 C5 C6 H6 C7 C8 keep geom rigidmod Cl1 O1 O2 O3 O4 end refine nd refine mod2d end mod2d ; _Jana_m90_file ; eformat91 0 datblock Block1 nref 7922 obslim 3 sctom90 1 norefitems 1 diffscales 1 dataave 1 scalelim 10 hklf5 0 indslowest 3 indfastest 1 addcentrsymm 0 sigimethod 2 multave 1 flimprint 5 flimcull -1 avesigwt 0 unstab 0.015897 radtype 1 dattype 1 lambda 0.71075 lpfactor 1 monangle 6.0823 perfmono 0.5 datcolltemp 293 end Data Block1 2 0 0 0 1175.8 44.2 1 0 1 0.0000 4 0 0 0 533.8 19.2 1 0 1 0.0000 6 0 0 0 481.5 5.6 1 0 1 0.0000 8 0 0 0 62.7 29.7 1 0 1 0.0000 12 0 0 0 17.5 2.2 1 0 1 0.0000 14 0 0 0 44.5 7.8 1 0 1 0.0000 16 0 0 0 2.1 6.3 1 0 1 0.0000 1 1 0 -1 1.0 3.5 1 0 1 0.0000 1 1 0 0 416.4 8.7 1 0 1 0.0000 1 1 0 1 2.0 1.5 1 0 1 0.0000 3 1 0 -1 0.8 1.3 1 0 1 0.0000 3 1 0 0 1119.3 18.0 1 0 1 0.0000 3 1 0 1 3.4 1.3 1 0 1 0.0000 5 1 0 -1 3.4 1.4 1 0 1 0.0000 5 1 0 0 383.5 7.0 1 0 1 0.0000 5 1 0 1 4.5 1.4 1 0 1 0.0000 7 1 0 -1 3.0 1.5 1 0 1 0.0000 7 1 0 0 518.1 5.5 1 0 1 0.0000 7 1 0 1 9.5 1.2 1 0 1 0.0000 9 1 0 -1 2.5 5.8 1 0 1 0.0000 9 1 0 1 7.5 2.0 1 0 1 0.0000 11 1 0 -1 3.6 2.2 1 0 1 0.0000 11 1 0 0 138.6 10.4 1 0 1 0.0000 11 1 0 1 0.8 2.1 1 0 1 0.0000 13 1 0 -1 0.4 1.6 1 0 1 0.0000 13 1 0 0 292.4 6.1 1 0 1 0.0000 13 1 0 1 6.6 6.1 1 0 1 0.0000 15 1 0 -1 -1.1 3.0 1 0 1 0.0000 15 1 0 0 12.4 2.4 1 0 1 0.0000 15 1 0 1 0.3 4.9 1 0 1 0.0000 17 1 0 -1 0.4 2.1 1 0 1 0.0000 17 1 0 0 6.9 6.0 1 0 1 0.0000 17 1 0 1 0.5 1.5 1 0 1 0.0000 19 1 0 -1 4.4 4.3 1 0 1 0.0000 19 1 0 0 -1.2 5.7 1 0 1 0.0000 19 1 0 1 2.3 4.9 1 0 1 0.0000 21 1 0 -1 2.6 5.3 1 0 1 0.0000 21 1 0 0 1.7 6.6 1 0 1 0.0000 21 1 0 1 -1.5 1.8 1 0 1 0.0000 0 2 0 0 9558.8 219.7 1 0 1 0.0000 0 2 0 1 187.8 15.7 1 0 1 0.0000 2 2 0 -1 15.5 1.2 1 0 1 0.0000 2 2 0 0 502.7 11.2 1 0 1 0.0000 2 2 0 1 12.3 1.3 1 0 1 0.0000 4 2 0 -1 43.8 1.4 1 0 1 0.0000 4 2 0 0 410.8 6.7 1 0 1 0.0000 4 2 0 1 5.7 1.0 1 0 1 0.0000 6 2 0 -1 7.6 1.7 1 0 1 0.0000 6 2 0 0 174.2 2.4 1 0 1 0.0000 6 2 0 1 30.1 1.4 1 0 1 0.0000 8 2 0 -1 0.2 2.4 1 0 1 0.0000 8 2 0 0 48.9 8.4 1 0 1 0.0000 8 2 0 1 1.0 5.2 1 0 1 0.0000 10 2 0 -1 1.4 3.6 1 0 1 0.0000 10 2 0 0 71.1 3.1 1 0 1 0.0000 10 2 0 1 -0.5 6.2 1 0 1 0.0000 12 2 0 -1 0.6 3.3 1 0 1 0.0000 12 2 0 0 4.1 5.5 1 0 1 0.0000 12 2 0 1 5.4 6.1 1 0 1 0.0000 14 2 0 -1 -0.8 1.7 1 0 1 0.0000 14 2 0 0 42.8 7.3 1 0 1 0.0000 14 2 0 1 1.1 5.8 1 0 1 0.0000 16 2 0 -1 1.3 4.9 1 0 1 0.0000 16 2 0 0 0.6 6.1 1 0 1 0.0000 16 2 0 1 2.3 1.6 1 0 1 0.0000 18 2 0 -1 -0.1 5.8 1 0 1 0.0000 18 2 0 0 6.2 7.3 1 0 1 0.0000 18 2 0 1 2.0 1.8 1 0 1 0.0000 20 2 0 -1 -1.3 2.0 1 0 1 0.0000 20 2 0 0 1.1 6.8 1 0 1 0.0000 20 2 0 1 3.7 3.6 1 0 1 0.0000 22 2 0 0 3.1 7.7 1 0 1 0.0000 22 2 0 1 0.6 1.7 1 0 1 0.0000 1 3 0 -1 20.4 1.0 1 0 1 0.0000 1 3 0 0 4.7 0.9 1 0 1 0.0000 1 3 0 1 1.9 0.9 1 0 1 0.0000 3 3 0 -1 0.4 1.0 1 0 1 0.0000 3 3 0 0 103.5 1.6 1 0 1 0.0000 3 3 0 1 27.0 1.2 1 0 1 0.0000 5 3 0 -1 31.9 3.1 1 0 1 0.0000 5 3 0 0 164.8 3.9 1 0 1 0.0000 5 3 0 1 12.3 5.8 1 0 1 0.0000 7 3 0 -1 25.8 25.9 1 0 1 0.0000 7 3 0 0 64.0 62.9 1 0 1 0.0000 7 3 0 1 28.8 7.8 1 0 1 0.0000 9 3 0 -1 2.5 1.7 1 0 1 0.0000 9 3 0 0 15.2 14.7 1 0 1 0.0000 9 3 0 1 9.9 10.8 1 0 1 0.0000 11 3 0 -1 8.9 2.1 1 0 1 0.0000 11 3 0 0 80.4 4.1 1 0 1 0.0000 11 3 0 1 8.4 4.5 1 0 1 0.0000 13 3 0 -1 5.4 1.8 1 0 1 0.0000 13 3 0 0 109.7 9.7 1 0 1 0.0000 13 3 0 1 7.4 4.4 1 0 1 0.0000 15 3 0 -1 -0.7 4.6 1 0 1 0.0000 15 3 0 0 9.6 6.0 1 0 1 0.0000 15 3 0 1 -1.5 4.6 1 0 1 0.0000 17 3 0 -1 2.2 4.8 1 0 1 0.0000 17 3 0 0 7.3 6.4 1 0 1 0.0000 17 3 0 1 0.6 2.7 1 0 1 0.0000 19 3 0 -1 1.0 5.1 1 0 1 0.0000 19 3 0 0 -3.9 5.5 1 0 1 0.0000 19 3 0 1 -0.8 4.5 1 0 1 0.0000 21 3 0 -1 -4.9 4.9 1 0 1 0.0000 21 3 0 0 2.1 7.6 1 0 1 0.0000 21 3 0 1 4.5 4.1 1 0 1 0.0000 0 4 0 0 1022.7 34.7 1 0 1 0.0000 0 4 0 1 175.9 6.4 1 0 1 0.0000 2 4 0 -1 18.1 1.4 1 0 1 0.0000 2 4 0 0 101.6 3.1 1 0 1 0.0000 2 4 0 1 26.0 7.3 1 0 1 0.0000 4 4 0 -1 50.4 25.8 1 0 1 0.0000 4 4 0 0 43.9 22.3 1 0 1 0.0000 4 4 0 1 4.3 2.1 1 0 1 0.0000 6 4 0 -1 3.8 6.1 1 0 1 0.0000 6 4 0 0 22.0 20.5 1 0 1 0.0000 6 4 0 1 13.9 19.9 1 0 1 0.0000 8 4 0 -1 4.2 5.5 1 0 1 0.0000 8 4 0 0 12.3 6.4 1 0 1 0.0000 8 4 0 1 2.8 4.4 1 0 1 0.0000 10 4 0 -1 -2.2 5.2 1 0 1 0.0000 10 4 0 0 19.9 6.4 1 0 1 0.0000 10 4 0 1 -1.0 2.1 1 0 1 0.0000 12 4 0 -1 4.4 4.9 1 0 1 0.0000 12 4 0 0 4.8 6.3 1 0 1 0.0000 12 4 0 1 -0.3 4.3 1 0 1 0.0000 14 4 0 -1 5.2 4.2 1 0 1 0.0000 14 4 0 0 7.8 2.3 1 0 1 0.0000 14 4 0 1 4.1 1.8 1 0 1 0.0000 16 4 0 -1 -3.3 4.9 1 0 1 0.0000 16 4 0 0 -1.9 5.6 1 0 1 0.0000 16 4 0 1 -1.9 5.1 1 0 1 0.0000 18 4 0 -1 -0.7 4.2 1 0 1 0.0000 18 4 0 0 2.2 7.0 1 0 1 0.0000 18 4 0 1 -1.5 4.8 1 0 1 0.0000 20 4 0 -1 2.2 5.1 1 0 1 0.0000 20 4 0 0 0.3 6.6 1 0 1 0.0000 20 4 0 1 -3.1 5.3 1 0 1 0.0000 1 5 0 -1 6.5 1.5 1 0 1 0.0000 1 5 0 0 1.2 1.2 1 0 1 0.0000 1 5 0 1 -1.2 1.5 1 0 1 0.0000 3 5 0 -1 -1.4 1.4 1 0 1 0.0000 3 5 0 0 11.9 1.4 1 0 1 0.0000 3 5 0 1 10.3 1.5 1 0 1 0.0000 5 5 0 -1 27.1 2.4 1 0 1 0.0000 5 5 0 0 13.9 2.2 1 0 1 0.0000 5 5 0 1 5.3 1.5 1 0 1 0.0000 7 5 0 -1 33.6 7.6 1 0 1 0.0000 7 5 0 0 21.5 2.2 1 0 1 0.0000 7 5 0 1 12.6 2.3 1 0 1 0.0000 9 5 0 -1 -2.5 1.9 1 0 1 0.0000 9 5 0 0 8.3 2.1 1 0 1 0.0000 9 5 0 1 14.9 2.5 1 0 1 0.0000 11 5 0 -1 6.7 4.8 1 0 1 0.0000 11 5 0 0 13.8 2.4 1 0 1 0.0000 11 5 0 1 3.0 1.8 1 0 1 0.0000 13 5 0 -1 10.0 4.4 1 0 1 0.0000 13 5 0 0 14.2 3.5 1 0 1 0.0000 13 5 0 1 5.5 5.8 1 0 1 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