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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ #======================================================================= data_II #======================================================================= _publ_contact_author_name 'Jana, Partha Pratim' _publ_contact_author_address ; CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 SE-22100 ; _publ_contact_author_email 'Partha.Jana@polymat.lth.se' _publ_contact_author_fax '+46462224012' _publ_contact_author_phone '0046462224769' _publ_requested_journal 'Inorganic Chemistry' _publ_requested_category ? #======================================================================= # 3. TITLE AND AUTHOR LIST loop_ _publ_author_name _publ_author_address 'Jana, Partha Pratim' ; CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 SE-22100 ; 'Lidin, Sven' ; CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 SE-22100 ; _publ_section_title ;Structural Impact of Platinum on the Incommensurably Modulated \g-Brass Related Composite Structure Pd~15~Zn~54~ ; _journal_name_full 'Inorganic Chemistry' _journal_volume 51 _journal_page_first 9893 _journal_page_last 9901 _journal_year 2012 _journal_paper_doi https://doi.org/10.1021/ic301326p _publ_section_references ; Petricek, V., Dusek, M. & Palatinus, L. (2006). Jana2006. Structure Determination Software Programs. Institute of Physics, Praha, Czech Republic. Palatinus, L. & Chapuis, G. (2007). <i>J. Appl. Cryst.</i> <b>40</b>, 786--790. ; _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Pd2.496 Pm3.965 Pt1.504 Zn26.546' _chemical_formula_weight 2869.5 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . _space_group_crystal_system orthorhombic _space_group_ssg_name 'Fmmm(\a00)0s0' loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,-x2,x3,-x4 3 -x1,x2,-x3,-x4+1/2 4 x1,-x2,-x3,x4+1/2 5 -x1,-x2,-x3,-x4 6 x1,x2,-x3,x4 7 x1,-x2,x3,x4+1/2 8 -x1,x2,x3,-x4+1/2 9 x1,x2+1/2,x3+1/2,x4 10 -x1,-x2+1/2,x3+1/2,-x4 11 -x1,x2+1/2,-x3+1/2,-x4+1/2 12 x1,-x2+1/2,-x3+1/2,x4+1/2 13 -x1,-x2+1/2,-x3+1/2,-x4 14 x1,x2+1/2,-x3+1/2,x4 15 x1,-x2+1/2,x3+1/2,x4+1/2 16 -x1,x2+1/2,x3+1/2,-x4+1/2 17 x1+1/2,x2,x3+1/2,x4 18 -x1+1/2,-x2,x3+1/2,-x4 19 -x1+1/2,x2,-x3+1/2,-x4+1/2 20 x1+1/2,-x2,-x3+1/2,x4+1/2 21 -x1+1/2,-x2,-x3+1/2,-x4 22 x1+1/2,x2,-x3+1/2,x4 23 x1+1/2,-x2,x3+1/2,x4+1/2 24 -x1+1/2,x2,x3+1/2,-x4+1/2 25 x1+1/2,x2+1/2,x3,x4 26 -x1+1/2,-x2+1/2,x3,-x4 27 -x1+1/2,x2+1/2,-x3,-x4+1/2 28 x1+1/2,-x2+1/2,-x3,x4+1/2 29 -x1+1/2,-x2+1/2,-x3,-x4 30 x1+1/2,x2+1/2,-x3,x4 31 x1+1/2,-x2+1/2,x3,x4+1/2 32 -x1+1/2,x2+1/2,x3,-x4+1/2 _cell_length_a 4.2837(11) _cell_length_b 9.151(2) _cell_length_c 12.948(4) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 507.6(2) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.627700 0.000000 0.000000 _cell_subsystems_number 2 loop_ _cell_subsystem_code _cell_subsystem_description _cell_subsystem_matrix_W_1_1 _cell_subsystem_matrix_W_1_2 _cell_subsystem_matrix_W_1_3 _cell_subsystem_matrix_W_1_4 _cell_subsystem_matrix_W_2_1 _cell_subsystem_matrix_W_2_2 _cell_subsystem_matrix_W_2_3 _cell_subsystem_matrix_W_2_4 _cell_subsystem_matrix_W_3_1 _cell_subsystem_matrix_W_3_2 _cell_subsystem_matrix_W_3_3 _cell_subsystem_matrix_W_3_4 _cell_subsystem_matrix_W_4_1 _cell_subsystem_matrix_W_4_2 _cell_subsystem_matrix_W_4_3 _cell_subsystem_matrix_W_4_4 1 '1st subsystem' 1 0 0 0 0 1 0 0 0 0 1 0 0 0 0 1 2 '2nd subsystem' 1 0 0 1 0 1 0 0 0 0 1 0 0 0 0 1 _cell_formula_units_Z 1 _cell_measurement_reflns_used 4679 _cell_measurement_theta_min 2.98 _cell_measurement_theta_max 29.12 _cell_measurement_temperature 293 _exptl_crystal_type_of_structure comp _exptl_crystal_density_diffrn 9.3847 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 1270 _exptl_absorpt_coefficient_mu 53.65 _exptl_crystal_description ? _exptl_crystal_size_max 0.05 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.03 _exptl_crystal_size_rad ? _exptl_crystal_colour ? _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.35.6 (release 27-01-2011 CrysAlis171 .NET) (compiled Jan 27 2011,13:34:29) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_correction_T_min 0.207 _exptl_absorpt_correction_T_max 1 _diffrn_ambient_temperature 293 _diffrn_source 'Enhance (Mo) X-ray Source' _diffrn_source_power ? _diffrn_source_voltage ? _diffrn_source_current ? _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.7107 _diffrn_radiation_monochromator 'graphite' _diffrn_measurement_device 'four-cycle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Eos' _diffrn_detector ? _diffrn_detector_area_resol_mean 16.1367 _diffrn_measurement_method '\w scans' _diffrn_measurement_specimen_support ? _diffrn_reflns_number 12319 _diffrn_reflns_theta_min 2.99 _diffrn_reflns_theta_max 29.18 _diffrn_reflns_theta_full 24.64 _diffrn_measured_fraction_theta_max 0.91 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0468 _diffrn_reflns_av_unetI/netI 0.0189 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_index_m_1_min -3 _diffrn_reflns_limit_index_m_1_max 3 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? _reflns_number_total 1145 _reflns_number_gt 984 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0335 _refine_ls_wR_factor_gt 0.0878 _refine_ls_R_factor_all 0.0391 _refine_ls_wR_factor_ref 0.0900 _refine_ls_goodness_of_fit_ref 2.09 _refine_ls_goodness_of_fit_gt 2.21 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 1145 _refine_ls_number_parameters 79 _refine_ls_number_restraints 0 _refine_ls_number_constraints 48 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(I)+0.0004I^2^)' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0234 _refine_ls_shift/su_mean 0.0046 _refine_diff_density_max 4.01 _refine_diff_density_min -3.82 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 354(18) _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Pd -0.9988 1.0072 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Pm -0.1753 3.2249 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Pt -1.7033 8.3905 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Zn 0.2839 1.4301 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.35.6 (release 27-01-2011 CrysAlis171 .NET) (compiled Jan 27 2011,13:34:29) ; _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.35.6 (release 27-01-2011 CrysAlis171 .NET) (compiled Jan 27 2011,13:34:29) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.35.6 (release 27-01-2011 CrysAlis171 .NET) (compiled Jan 27 2011,13:34:29) ; loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_subsystem_code Pt1 Pt 0.5 0 0 Uani 0.0091(2) 4 0.376(6) d . . . 1 Pd1 Pd 0.5 0 0 Uani 0.0091(2) 4 0.624(6) d . . . 1 Pm2 Pm 0.5 0.15108(6) 0.17957(4) Uani 0.0133(2) 16 0.248(4) d . . . 1 Zn2 Zn 0.5 0.15108(6) 0.17957(4) Uani 0.0133(2) 16 0.752(4) d . . . 1 Zn1 Zn 0 0 0.12342(7) Uani 0.0156(3) 8 1 d . . . 1 Zn3 Zn 0.75 0.25 0 Uani 0.0149(3) 4 1 d . . . 2 loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pt1 Pt 0.0103(4) 0.0081(4) 0.0088(4) 0 0 0 Pd1 Pd 0.0103(4) 0.0081(4) 0.0088(4) 0 0 0 Pm2 Pm 0.0150(4) 0.0126(4) 0.0124(4) 0 0 -0.00358(19) Zn2 Zn 0.0150(4) 0.0126(4) 0.0124(4) 0 0 -0.00358(19) Zn1 Zn 0.0105(5) 0.0176(5) 0.0186(5) 0 0 0 Zn3 Zn 0.0183(6) 0.0114(5) 0.0149(6) 0 0 0 loop_ _atom_site_Fourier_wave_vector_seq_id _jana_atom_site_Fourier_wave_vector_q1_coeff 1 1 2 2 3 3 loop_ _atom_site_occ_Fourier_id _atom_site_occ_Fourier_atom_site_label _atom_site_occ_Fourier_wave_vector_seq_id Pt1o1 Pt1 1 Pt1o2 Pt1 2 Pt1o3 Pt1 3 Pd1o1 Pd1 1 Pd1o2 Pd1 2 Pd1o3 Pd1 3 Pm2o1 Pm2 1 Pm2o2 Pm2 2 Pm2o3 Pm2 3 Zn2o1 Zn2 1 Zn2o2 Zn2 2 Zn2o3 Zn2 3 loop_ _atom_site_occ_Fourier_param_id _atom_site_occ_Fourier_param_cos _atom_site_occ_Fourier_param_sin Pt1o1 0 0 Pt1o2 0.335(5) 0 Pt1o3 0 0 Pd1o1 0 0 Pd1o2 -0.335(5) 0 Pd1o3 0 0 Pm2o1 0 -0.420(4) Pm2o2 -0.276(3) 0 Pm2o3 0 0.121(2) Zn2o1 0 0.420(4) Zn2o2 0.276(3) 0 Zn2o3 0 -0.121(2) loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Pt1x1 Pt1 x 1 Pt1y1 Pt1 y 1 Pt1z1 Pt1 z 1 Pt1x2 Pt1 x 2 Pt1y2 Pt1 y 2 Pt1z2 Pt1 z 2 Pt1x3 Pt1 x 3 Pt1y3 Pt1 y 3 Pt1z3 Pt1 z 3 Pd1x1 Pd1 x 1 Pd1y1 Pd1 y 1 Pd1z1 Pd1 z 1 Pd1x2 Pd1 x 2 Pd1y2 Pd1 y 2 Pd1z2 Pd1 z 2 Pd1x3 Pd1 x 3 Pd1y3 Pd1 y 3 Pd1z3 Pd1 z 3 Pm2x1 Pm2 x 1 Pm2y1 Pm2 y 1 Pm2z1 Pm2 z 1 Pm2x2 Pm2 x 2 Pm2y2 Pm2 y 2 Pm2z2 Pm2 z 2 Pm2x3 Pm2 x 3 Pm2y3 Pm2 y 3 Pm2z3 Pm2 z 3 Zn2x1 Zn2 x 1 Zn2y1 Zn2 y 1 Zn2z1 Zn2 z 1 Zn2x2 Zn2 x 2 Zn2y2 Zn2 y 2 Zn2z2 Zn2 z 2 Zn2x3 Zn2 x 3 Zn2y3 Zn2 y 3 Zn2z3 Zn2 z 3 Zn1x1 Zn1 x 1 Zn1y1 Zn1 y 1 Zn1z1 Zn1 z 1 Zn1x2 Zn1 x 2 Zn1y2 Zn1 y 2 Zn1z2 Zn1 z 2 Zn1x3 Zn1 x 3 Zn1y3 Zn1 y 3 Zn1z3 Zn1 z 3 Zn3x1 Zn3 x 1 Zn3y1 Zn3 y 1 Zn3z1 Zn3 z 1 Zn3x2 Zn3 x 2 Zn3y2 Zn3 y 2 Zn3z2 Zn3 z 2 Zn3x3 Zn3 x 3 Zn3y3 Zn3 y 3 Zn3z3 Zn3 z 3 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Pt1x1 0 0 Pt1y1 0 0.02462(10) Pt1z1 0 0 Pt1x2 0 0.00319(17) Pt1y2 0 0 Pt1z2 0 0 Pt1x3 0 0 Pt1y3 0 0.00128(8) Pt1z3 0 0 Pd1x1 0 0 Pd1y1 0 0.02462(10) Pd1z1 0 0 Pd1x2 0 0.00319(17) Pd1y2 0 0 Pd1z2 0 0 Pd1x3 0 0 Pd1y3 0 0.00128(8) Pd1z3 0 0 Pm2x1 -0.0673(2) 0 Pm2y1 0 -0.01914(8) Pm2z1 0 0.00348(5) Pm2x2 0 -0.01341(16) Pm2y2 0.00522(7) 0 Pm2z2 -0.00311(5) 0 Pm2x3 0.00616(17) 0 Pm2y3 0 0.00480(7) Pm2z3 0 -0.00145(5) Zn2x1 -0.0673(2) 0 Zn2y1 0 -0.01914(8) Zn2z1 0 0.00348(5) Zn2x2 0 -0.01341(16) Zn2y2 0.00522(7) 0 Zn2z2 -0.00311(5) 0 Zn2x3 0.00616(17) 0 Zn2y3 0 0.00480(7) Zn2z3 0 -0.00145(5) Zn1x1 0 0 Zn1y1 0 0.05153(13) Zn1z1 0 0 Zn1x2 0 0.0128(3) Zn1y2 0 0 Zn1z2 0.00838(9) 0 Zn1x3 0 0 Zn1y3 0 0.00324(15) Zn1z3 0 0 Zn3x1 0 0 Zn3y1 0 0.05653(14) Zn3z1 0 0 Zn3x2 0 -0.0378(5) Zn3y2 0 0 Zn3z2 0 0 Zn3x3 0 0 Zn3y3 0 0.00185(13) Zn3z3 0 0 loop_ _atom_site_U_Fourier_id _atom_site_U_Fourier_atom_site_label _atom_site_U_Fourier_tens_elem _atom_site_U_Fourier_wave_vector_seq_id Pt1U111 Pt1 U11 1 Pt1U221 Pt1 U22 1 Pt1U331 Pt1 U33 1 Pt1U121 Pt1 U12 1 Pt1U131 Pt1 U13 1 Pt1U231 Pt1 U23 1 Pt1U112 Pt1 U11 2 Pt1U222 Pt1 U22 2 Pt1U332 Pt1 U33 2 Pt1U122 Pt1 U12 2 Pt1U132 Pt1 U13 2 Pt1U232 Pt1 U23 2 Pt1U113 Pt1 U11 3 Pt1U223 Pt1 U22 3 Pt1U333 Pt1 U33 3 Pt1U123 Pt1 U12 3 Pt1U133 Pt1 U13 3 Pt1U233 Pt1 U23 3 Pd1U111 Pd1 U11 1 Pd1U221 Pd1 U22 1 Pd1U331 Pd1 U33 1 Pd1U121 Pd1 U12 1 Pd1U131 Pd1 U13 1 Pd1U231 Pd1 U23 1 Pd1U112 Pd1 U11 2 Pd1U222 Pd1 U22 2 Pd1U332 Pd1 U33 2 Pd1U122 Pd1 U12 2 Pd1U132 Pd1 U13 2 Pd1U232 Pd1 U23 2 Pd1U113 Pd1 U11 3 Pd1U223 Pd1 U22 3 Pd1U333 Pd1 U33 3 Pd1U123 Pd1 U12 3 Pd1U133 Pd1 U13 3 Pd1U233 Pd1 U23 3 Pm2U111 Pm2 U11 1 Pm2U221 Pm2 U22 1 Pm2U331 Pm2 U33 1 Pm2U121 Pm2 U12 1 Pm2U131 Pm2 U13 1 Pm2U231 Pm2 U23 1 Pm2U112 Pm2 U11 2 Pm2U222 Pm2 U22 2 Pm2U332 Pm2 U33 2 Pm2U122 Pm2 U12 2 Pm2U132 Pm2 U13 2 Pm2U232 Pm2 U23 2 Pm2U113 Pm2 U11 3 Pm2U223 Pm2 U22 3 Pm2U333 Pm2 U33 3 Pm2U123 Pm2 U12 3 Pm2U133 Pm2 U13 3 Pm2U233 Pm2 U23 3 Zn2U111 Zn2 U11 1 Zn2U221 Zn2 U22 1 Zn2U331 Zn2 U33 1 Zn2U121 Zn2 U12 1 Zn2U131 Zn2 U13 1 Zn2U231 Zn2 U23 1 Zn2U112 Zn2 U11 2 Zn2U222 Zn2 U22 2 Zn2U332 Zn2 U33 2 Zn2U122 Zn2 U12 2 Zn2U132 Zn2 U13 2 Zn2U232 Zn2 U23 2 Zn2U113 Zn2 U11 3 Zn2U223 Zn2 U22 3 Zn2U333 Zn2 U33 3 Zn2U123 Zn2 U12 3 Zn2U133 Zn2 U13 3 Zn2U233 Zn2 U23 3 Zn1U111 Zn1 U11 1 Zn1U221 Zn1 U22 1 Zn1U331 Zn1 U33 1 Zn1U121 Zn1 U12 1 Zn1U131 Zn1 U13 1 Zn1U231 Zn1 U23 1 Zn1U112 Zn1 U11 2 Zn1U222 Zn1 U22 2 Zn1U332 Zn1 U33 2 Zn1U122 Zn1 U12 2 Zn1U132 Zn1 U13 2 Zn1U232 Zn1 U23 2 Zn1U113 Zn1 U11 3 Zn1U223 Zn1 U22 3 Zn1U333 Zn1 U33 3 Zn1U123 Zn1 U12 3 Zn1U133 Zn1 U13 3 Zn1U233 Zn1 U23 3 Zn3U111 Zn3 U11 1 Zn3U221 Zn3 U22 1 Zn3U331 Zn3 U33 1 Zn3U121 Zn3 U12 1 Zn3U131 Zn3 U13 1 Zn3U231 Zn3 U23 1 Zn3U112 Zn3 U11 2 Zn3U222 Zn3 U22 2 Zn3U332 Zn3 U33 2 Zn3U122 Zn3 U12 2 Zn3U132 Zn3 U13 2 Zn3U232 Zn3 U23 2 Zn3U113 Zn3 U11 3 Zn3U223 Zn3 U22 3 Zn3U333 Zn3 U33 3 Zn3U123 Zn3 U12 3 Zn3U133 Zn3 U13 3 Zn3U233 Zn3 U23 3 loop_ _atom_site_U_Fourier_param_id _atom_site_U_Fourier_param_cos _atom_site_U_Fourier_param_sin Pt1U111 0 0 Pt1U221 0 0 Pt1U331 0 0 Pt1U121 0.0012(2) 0 Pt1U131 0 0 Pt1U231 0 0 Pt1U112 -0.0014(5) 0 Pt1U222 -0.0007(4) 0 Pt1U332 0.0000(4) 0 Pt1U122 0 0 Pt1U132 0 0 Pt1U232 0 0 Pt1U113 0 0 Pt1U223 0 0 Pt1U333 0 0 Pt1U123 0.0005(3) 0 Pt1U133 0 0 Pt1U233 0 0 Pd1U111 0 0 Pd1U221 0 0 Pd1U331 0 0 Pd1U121 0.0012(2) 0 Pd1U131 0 0 Pd1U231 0 0 Pd1U112 -0.0014(5) 0 Pd1U222 -0.0007(4) 0 Pd1U332 0.0000(4) 0 Pd1U122 0 0 Pd1U132 0 0 Pd1U232 0 0 Pd1U113 0 0 Pd1U223 0 0 Pd1U333 0 0 Pd1U123 0.0005(3) 0 Pd1U133 0 0 Pd1U233 0 0 Pm2U111 0 0.0075(5) Pm2U221 0 0.0025(4) Pm2U331 0 0.0013(4) Pm2U121 -0.0018(3) 0 Pm2U131 0.0027(3) 0 Pm2U231 0 -0.0021(3) Pm2U112 -0.0012(5) 0 Pm2U222 0.0035(4) 0 Pm2U332 0.0000(4) 0 Pm2U122 0 -0.0009(3) Pm2U132 0 0.0015(3) Pm2U232 -0.0012(3) 0 Pm2U113 0 0.0012(5) Pm2U223 0 0.0013(4) Pm2U333 0 -0.0013(4) Pm2U123 0.0012(3) 0 Pm2U133 0.0001(3) 0 Pm2U233 0 -0.0006(3) Zn2U111 0 0.0075(5) Zn2U221 0 0.0025(4) Zn2U331 0 0.0013(4) Zn2U121 -0.0018(3) 0 Zn2U131 0.0027(3) 0 Zn2U231 0 -0.0021(3) Zn2U112 -0.0012(5) 0 Zn2U222 0.0035(4) 0 Zn2U332 0.0000(4) 0 Zn2U122 0 -0.0009(3) Zn2U132 0 0.0015(3) Zn2U232 -0.0012(3) 0 Zn2U113 0 0.0012(5) Zn2U223 0 0.0013(4) Zn2U333 0 -0.0013(4) Zn2U123 0.0012(3) 0 Zn2U133 0.0001(3) 0 Zn2U233 0 -0.0006(3) Zn1U111 0 0 Zn1U221 0 0 Zn1U331 0 0 Zn1U121 0.0054(5) 0 Zn1U131 0 0 Zn1U231 0 -0.0063(5) Zn1U112 0.0012(6) 0 Zn1U222 0.0032(7) 0 Zn1U332 -0.0028(6) 0 Zn1U122 0 0 Zn1U132 0 0.0039(5) Zn1U232 0 0 Zn1U113 0 0 Zn1U223 0 0 Zn1U333 0 0 Zn1U123 0.0052(6) 0 Zn1U133 0 0 Zn1U233 0 0.0043(6) Zn3U111 0 0 Zn3U221 0 0 Zn3U331 0 0 Zn3U121 -0.0087(6) 0 Zn3U131 0 0 Zn3U231 0 0 Zn3U112 0.0080(8) 0 Zn3U222 0.0041(6) 0 Zn3U332 -0.0029(6) 0 Zn3U122 0 0 Zn3U132 0 0 Zn3U232 0 0 Zn3U113 0 0 Zn3U223 0 0 Zn3U333 0 0 Zn3U123 0.0007(5) 0 Zn3U133 0 0 Zn3U233 0 0 #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 0 2 1744.09 1921.62 42.78 o 2 0 0 -2 1843.72 2038.72 36.51 o 2 0 0 0 134766.00 144311.00 1337.89 o 2 0 0 2 33121.60 33662.00 441.38 o 4 0 0 -2 1279.10 1640.63 68.73 o 4 0 0 0 97350.30 102996.00 1510.32 o 4 0 0 2 17348.00 17973.70 668.46 o 0 2 0 0 2679.08 2390.70 44.42 o 0 2 0 1 6194.90 6816.25 58.38 o 0 2 0 2 832.58 920.42 20.51 o 0 2 0 3 1063.24 1056.48 30.44 o 2 2 0 -3 728.29 610.47 16.26 o 2 2 0 -2 2514.59 2873.13 34.36 o 2 2 0 -1 12728.80 12377.20 91.53 o 2 2 0 0 27084.50 27098.40 217.88 o 2 2 0 1 30295.80 30006.70 317.21 o 2 2 0 2 16544.20 16603.00 275.03 o 2 2 0 3 2656.37 2731.90 112.64 o 4 2 0 -3 218.18 235.77 18.32 o 4 2 0 -2 2490.95 3106.98 82.04 o 4 2 0 -1 11740.90 11471.10 224.32 o 4 2 0 0 19241.00 18907.50 326.90 o 4 2 0 1 13332.30 14457.50 342.77 o 4 2 0 2 4034.49 4135.43 209.78 o 0 4 0 0 1378.92 1319.73 49.11 o 0 4 0 1 92606.70 97431.70 582.98 o 0 4 0 2 7546.99 7328.81 92.17 o 0 4 0 3 179.01 151.09 14.82 o 2 4 0 -3 410.15 311.75 17.35 o 2 4 0 -2 8266.94 7460.20 95.24 o 2 4 0 -1 30668.90 31758.80 232.88 o 2 4 0 0 36.56 75.82 12.28 o 2 4 0 1 106479.00 103701.00 865.49 o 2 4 0 2 125.11 113.52 22.98 o 2 4 0 3 3111.22 2980.30 136.81 o 4 4 0 -3 3.90 9.64 10.06 < 4 4 0 -2 10349.80 9473.00 149.70 o 4 4 0 -1 5920.88 6686.15 145.49 o 4 4 0 0 5559.72 5725.65 194.67 o 4 4 0 1 43505.00 45320.20 807.43 o 4 4 0 2 3391.17 3432.11 312.70 o 0 6 0 0 119671.00 119631.00 1582.12 o 0 6 0 1 634.43 652.51 44.34 o 0 6 0 2 52.21 102.30 17.58 o 0 6 0 3 157.49 215.27 34.63 o 2 6 0 -3 2672.67 2392.31 81.06 o 2 6 0 -2 4007.81 4011.13 106.34 o 2 6 0 -1 1082.67 1047.41 51.20 o 2 6 0 0 107873.00 106750.00 1084.73 o 2 6 0 1 4520.48 4607.44 124.68 o 2 6 0 2 524.87 470.87 46.68 o 2 6 0 3 1587.13 1741.56 110.23 o 4 6 0 -3 4028.56 4098.77 136.40 o 4 6 0 -2 1928.12 2092.69 84.58 o 4 6 0 -1 38.46 21.39 18.53 < 4 6 0 0 30742.90 30815.10 516.48 o 4 6 0 1 10482.00 9741.17 336.71 o 0 8 0 0 2062.89 2337.70 177.59 o 0 8 0 1 684.19 575.35 59.80 o 0 8 0 2 18433.20 18515.60 321.49 o 0 8 0 3 5398.76 5342.72 162.80 o 2 8 0 -3 3119.11 2927.47 141.40 o 2 8 0 -2 3153.38 2856.05 138.03 o 2 8 0 -1 1674.80 1831.88 93.59 o 2 8 0 0 93.83 74.34 27.53 < 2 8 0 1 462.84 493.35 64.37 o 2 8 0 2 14203.90 13850.70 369.76 o 2 8 0 3 1125.33 1183.05 171.55 o 4 8 0 -3 1714.72 1348.68 87.78 o 4 8 0 -2 937.53 873.54 84.03 o 4 8 0 -1 4790.48 5632.32 268.86 o 4 8 0 0 621.40 508.46 120.26 o 0 10 0 0 6202.59 6261.16 430.15 o 0 10 0 1 33930.20 34896.20 688.06 o 0 10 0 2 608.78 611.34 77.70 o 0 10 0 3 112.32 92.98 38.12 < 2 10 0 -3 210.38 242.91 58.45 o 2 10 0 -2 3087.91 3129.67 172.03 o 2 10 0 -1 32605.30 32584.00 641.46 o 2 10 0 0 1579.86 1577.47 161.76 o 2 10 0 1 25171.20 25495.60 973.31 o 4 10 0 -3 10.07 91.08 52.00 < 4 10 0 -2 1931.17 2041.54 289.82 o 1 1 1 -3 340.02 420.89 8.46 o 1 1 1 -2 117.42 151.13 14.18 o 1 1 1 -1 1719.26 1741.63 24.44 o 1 1 1 0 18261.30 18561.80 81.58 o 1 1 1 1 1778.19 1982.34 24.90 o 1 1 1 2 905.66 916.18 24.85 o 1 1 1 3 1409.67 1510.00 37.22 o 3 1 1 -3 37.61 33.25 3.60 o 3 1 1 -2 21.89 8.37 4.77 < 3 1 1 -1 135.84 283.24 15.25 o 3 1 1 0 7865.36 7828.09 90.89 o 3 1 1 1 4402.00 4773.11 100.30 o 3 1 1 2 274.50 326.75 29.01 o 3 1 1 3 676.72 742.26 53.77 o 5 1 1 -3 60.01 110.98 13.66 o 5 1 1 -2 38.97 95.10 17.90 o 5 1 1 -1 147.18 309.95 29.65 o 5 1 1 0 1975.87 1915.79 93.81 o 1 3 1 -3 7.36 23.19 4.02 o 1 3 1 -2 1325.13 1225.66 20.48 o 1 3 1 -1 534.82 531.04 13.22 o 1 3 1 0 1176.53 1260.46 19.54 o 1 3 1 1 12755.90 12891.70 89.63 o 1 3 1 2 20.15 53.27 7.84 o 1 3 1 3 337.11 334.64 18.53 o 3 3 1 -3 75.27 35.68 4.87 o 3 3 1 -2 834.60 793.55 20.84 o 3 3 1 -1 249.66 156.37 11.33 o 3 3 1 0 572.92 485.71 25.51 o 3 3 1 1 858.61 747.13 37.99 o 3 3 1 2 319.73 359.67 37.16 o 3 3 1 3 1358.42 1398.26 75.44 o 5 3 1 -3 119.62 153.12 15.99 o 5 3 1 -2 598.89 642.52 38.42 o 5 3 1 -1 97.24 77.41 23.30 o 5 3 1 0 427.79 615.66 56.85 o 5 3 1 1 233.00 305.28 129.93 < 1 5 1 -3 239.26 302.26 16.20 o 1 5 1 -2 336.63 282.41 17.36 o 1 5 1 -1 863.09 956.57 28.98 o 1 5 1 0 1073.11 1131.40 30.24 o 1 5 1 1 8925.05 9001.32 105.37 o 1 5 1 2 783.70 804.95 28.57 o 1 5 1 3 321.76 305.55 21.28 o 3 5 1 -3 7.02 44.69 9.00 o 3 5 1 -2 92.96 148.99 13.13 o 3 5 1 -1 608.57 491.41 21.70 o 3 5 1 0 6549.13 6291.47 107.71 o 3 5 1 1 2228.20 2055.11 72.00 o 3 5 1 2 756.74 649.49 54.51 o 3 5 1 3 476.31 489.24 62.57 o 5 5 1 -3 79.55 81.65 14.30 o 5 5 1 -2 117.73 162.23 24.46 o 5 5 1 -1 182.30 152.06 28.48 o 5 5 1 0 3233.18 2785.93 148.60 o 1 7 1 -3 733.22 870.64 39.58 o 1 7 1 -2 371.02 288.37 20.96 o 1 7 1 -1 44.15 29.65 11.23 < 1 7 1 0 51813.70 50575.10 368.61 o 1 7 1 1 3805.48 3673.62 84.64 o 1 7 1 2 1385.70 1334.42 55.53 o 1 7 1 3 23.69 42.57 19.49 < 3 7 1 -3 248.06 342.62 27.32 o 3 7 1 -2 90.75 137.03 18.11 o 3 7 1 -1 324.59 310.11 26.47 o 3 7 1 0 12254.50 12386.00 211.62 o 3 7 1 1 480.19 396.90 41.82 o 3 7 1 2 2838.73 2452.07 117.97 o 5 7 1 -3 123.31 141.26 24.46 o 5 7 1 -2 56.32 78.58 20.86 o 5 7 1 -1 10.31 14.09 27.32 < 1 9 1 -3 233.00 267.04 36.11 o 1 9 1 -2 447.07 410.02 47.85 o 1 9 1 -1 89.20 73.28 26.58 < 1 9 1 0 37.35 48.50 22.56 < 1 9 1 1 20.78 68.20 22.03 o 1 9 1 2 927.58 990.83 73.87 o 1 9 1 3 222.12 232.85 42.57 o 3 9 1 -3 26.44 80.38 27.22 < 3 9 1 -2 8.11 34.84 24.78 < 3 9 1 -1 3417.01 3202.40 145.80 o 3 9 1 0 2126.53 2054.41 123.42 o 3 9 1 1 795.92 948.32 174.34 o 5 9 1 -3 78.08 101.13 35.05 < 5 9 1 -2 13.54 35.27 53.27 < 1 11 1 -3 56.68 56.97 28.91 < 1 11 1 -2 289.77 345.61 57.18 o 1 11 1 -1 9745.49 9722.37 248.74 o 1 11 1 0 3698.94 3730.32 155.20 o 1 11 1 1 13234.70 13978.80 348.29 o 1 11 1 2 160.63 98.16 105.26 < 3 11 1 -3 68.89 83.03 26.90 o 3 11 1 -2 34.26 24.78 43.74 < 3 11 1 -1 1492.12 1395.37 297.00 o 0 0 2 0 2308.32 2390.51 75.14 o 0 0 2 2 3863.75 3959.40 46.96 o 2 0 2 -2 3444.70 3249.75 37.94 o 2 0 2 0 1448.24 1556.00 42.36 o 2 0 2 2 855.83 955.47 52.27 o 4 0 2 -2 3605.12 3280.43 86.87 o 4 0 2 0 1177.23 1534.43 84.64 o 4 0 2 2 1941.11 2189.35 157.49 o 0 2 2 0 22614.40 21173.10 167.02 o 0 2 2 1 2210.44 2216.76 24.42 o 0 2 2 2 759.56 730.92 13.85 o 0 2 2 3 768.18 878.97 22.64 o 2 2 2 -3 36.84 72.64 5.93 o 2 2 2 -2 45.46 107.48 6.14 o 2 2 2 -1 20.91 73.39 5.61 o 2 2 2 0 43705.20 43628.30 251.05 o 2 2 2 1 9652.68 9827.88 109.98 o 2 2 2 2 2930.14 2977.18 71.59 o 2 2 2 3 53.78 173.46 28.38 o 4 2 2 -3 436.00 483.88 19.26 o 4 2 2 -2 97.80 245.67 19.17 o 4 2 2 -1 664.80 789.12 36.20 o 4 2 2 0 16868.90 16329.80 227.99 o 4 2 2 1 9609.70 9664.86 194.48 o 4 2 2 2 99.56 137.24 39.18 o 0 4 2 0 104041.00 98244.50 714.99 o 0 4 2 1 496.13 544.62 18.09 o 0 4 2 2 1248.74 1206.39 26.64 o 0 4 2 3 1735.16 1856.17 37.09 o 2 4 2 -3 740.80 785.39 23.80 o 2 4 2 -2 95.11 124.10 9.64 o 2 4 2 -1 37.76 70.74 7.10 o 2 4 2 0 53692.00 51761.70 285.80 o 2 4 2 1 42.81 65.23 9.11 o 2 4 2 2 2419.76 2524.82 71.54 o 2 4 2 3 29.04 96.79 24.89 o 4 4 2 -3 223.89 241.93 15.25 o 4 4 2 -2 279.12 379.14 20.01 o 4 4 2 -1 789.34 1032.08 47.94 o 4 4 2 0 17021.40 17529.90 259.13 o 4 4 2 1 1488.19 1491.96 82.42 o 4 4 2 2 408.10 410.17 93.81 o 0 6 2 0 5611.47 5363.04 106.86 o 0 6 2 1 955.91 961.80 34.91 o 0 6 2 2 85.35 83.44 12.18 o 0 6 2 3 273.61 256.64 21.70 o 2 6 2 -3 13.83 21.07 8.05 < 2 6 2 -2 1367.62 1392.11 41.87 o 2 6 2 -1 15021.70 13939.90 138.63 o 2 6 2 0 73.83 100.50 15.04 o 2 6 2 1 386.50 388.75 27.31 o 2 6 2 2 5259.65 5213.60 119.29 o 2 6 2 3 387.23 351.72 34.52 o 4 6 2 -3 257.74 238.12 20.22 o 4 6 2 -2 918.24 1077.80 46.46 o 4 6 2 -1 6669.90 6032.57 130.23 o 4 6 2 0 557.23 523.39 45.10 o 4 6 2 1 134.47 150.90 35.69 o 0 8 2 0 1980.57 2086.02 103.07 o 0 8 2 1 24394.90 24607.20 273.99 o 0 8 2 2 1632.62 1752.74 64.41 o 0 8 2 3 210.61 169.84 23.30 o 2 8 2 -3 49.97 123.90 20.54 o 2 8 2 -2 663.63 621.30 41.81 o 2 8 2 -1 2573.93 2732.70 80.42 o 2 8 2 0 624.48 536.46 40.44 o 2 8 2 1 30437.80 29566.70 366.32 o 2 8 2 2 21.02 62.38 29.44 < 2 8 2 3 307.86 326.23 66.92 o 4 8 2 -3 48.55 22.98 16.94 < 4 8 2 -2 1840.99 1686.09 86.09 o 4 8 2 -1 1005.29 1147.55 78.85 o 4 8 2 0 3348.09 3119.88 189.38 o 0 10 2 0 24903.50 24630.70 549.50 o 0 10 2 1 1290.26 1313.71 86.23 o 0 10 2 2 184.51 176.31 34.63 o 0 10 2 3 165.21 231.48 45.11 o 2 10 2 -3 1611.95 1669.04 95.84 o 2 10 2 -2 2627.64 2767.96 125.58 o 2 10 2 -1 25.41 19.06 25.52 < 2 10 2 0 18184.60 18411.80 352.22 o 2 10 2 1 983.81 980.48 124.46 o 2 10 2 2 35.22 31.03 119.78 < 4 10 2 -3 1146.33 1249.57 89.42 o 4 10 2 -2 722.32 730.93 189.59 o 0 12 2 0 1954.66 1610.74 278.72 o 0 12 2 1 781.62 591.29 92.09 o 0 12 2 2 3077.06 3302.06 444.27 o 2 12 2 -3 74.12 38.97 42.47 < 2 12 2 -2 121.62 169.54 59.30 < 1 1 3 -3 958.77 864.65 16.69 o 1 1 3 -2 3414.85 3430.60 38.22 o 1 1 3 -1 9562.29 9955.33 68.10 o 1 1 3 0 956.39 945.91 16.80 o 1 1 3 1 83614.50 89037.20 427.25 o 1 1 3 2 3679.20 3595.00 58.89 o 1 1 3 3 214.13 221.29 18.85 o 3 1 3 -3 5.44 39.08 4.45 o 3 1 3 -2 6982.35 6970.38 64.12 o 3 1 3 -1 129.17 87.78 10.48 o 3 1 3 0 8421.84 8472.72 113.85 o 3 1 3 1 45724.50 46182.00 393.49 o 3 1 3 2 4245.38 4142.68 112.21 o 3 1 3 3 6714.83 6778.08 169.41 o 5 1 3 -3 608.23 689.64 32.60 o 5 1 3 -2 5085.61 5640.61 113.13 o 5 1 3 -1 335.91 229.86 32.08 o 5 1 3 0 10242.90 10297.50 228.76 o 1 3 3 -3 813.90 828.50 19.88 o 1 3 3 -2 76.29 49.13 7.52 o 1 3 3 -1 1221.39 1216.19 25.56 o 1 3 3 0 134094.00 141018.00 596.40 o 1 3 3 1 906.31 936.93 23.80 o 1 3 3 2 6118.05 6220.29 80.40 o 1 3 3 3 51.01 271.74 25.84 o 3 3 3 -3 1724.89 2015.04 34.53 o 3 3 3 -2 11.01 13.13 6.35 < 3 3 3 -1 35.39 102.09 11.54 o 3 3 3 0 111512.00 110691.00 687.68 o 3 3 3 1 4008.44 4348.95 108.61 o 3 3 3 2 14323.90 14516.30 226.43 o 3 3 3 3 1603.00 1980.96 102.09 o 5 3 3 -3 1674.19 2047.87 61.01 o 5 3 3 -2 12.10 11.86 14.93 < 5 3 3 -1 0.17 84.72 24.57 o 5 3 3 0 26391.40 28175.70 411.24 o 1 5 3 -3 1896.99 1833.30 42.68 o 1 5 3 -2 2049.51 2162.33 47.63 o 1 5 3 -1 549.26 493.46 22.65 o 1 5 3 0 2098.81 2218.29 49.11 o 1 5 3 1 419.08 405.52 19.27 o 1 5 3 2 14704.70 14331.20 140.40 o 1 5 3 3 4278.44 4265.85 82.08 o 3 5 3 -3 991.05 807.57 30.89 o 3 5 3 -2 1057.79 1191.60 34.38 o 3 5 3 -1 11563.50 11782.40 131.59 o 3 5 3 0 7975.89 7481.87 112.43 o 3 5 3 1 10702.50 11107.50 183.29 o 3 5 3 2 13690.40 12851.50 221.66 o 3 5 3 3 635.88 598.12 74.00 o 5 5 3 -3 1.84 40.46 12.28 o 5 5 3 -2 503.04 638.58 43.83 o 5 5 3 -1 5264.66 5624.96 144.68 o 5 5 3 0 4123.04 3342.03 191.72 o 1 7 3 -3 9.98 25.63 11.01 < 1 7 3 -2 5082.55 4892.31 104.52 o 1 7 3 -1 61312.70 63082.80 459.50 o 1 7 3 0 1282.28 1260.83 46.44 o 1 7 3 1 58671.90 57100.70 413.76 o 1 7 3 2 427.66 440.20 33.03 o 1 7 3 3 1176.14 1121.91 57.67 o 3 7 3 -3 58.90 24.46 11.23 < 3 7 3 -2 4526.93 3874.51 87.34 o 3 7 3 -1 17313.90 17273.50 213.40 o 3 7 3 0 383.80 328.64 31.97 o 3 7 3 1 47361.40 46904.30 530.69 o 3 7 3 2 847.59 916.43 92.51 o 5 7 3 -3 2.59 42.79 19.91 < 5 7 3 -2 3759.47 3390.09 123.91 o 5 7 3 -1 4063.03 3690.38 244.43 o 1 9 3 -3 542.91 495.32 40.33 o 1 9 3 -2 414.73 522.79 41.50 o 1 9 3 -1 99.76 136.50 21.81 o 1 9 3 0 26777.80 27630.50 320.90 o 1 9 3 1 2785.87 2885.32 102.52 o 1 9 3 2 124.98 154.08 27.74 o 1 9 3 3 2345.77 2423.37 117.90 o 3 9 3 -3 1997.58 1845.04 73.70 o 3 9 3 -2 3269.98 3734.55 125.62 o 3 9 3 -1 2.08 19.06 20.23 < 3 9 3 0 20289.40 20137.20 381.69 o 3 9 3 1 3620.56 3075.37 271.77 o 5 9 3 -3 2092.59 2174.24 129.88 o 5 9 3 -2 1757.19 1902.93 246.91 o 1 11 3 -3 3473.75 3845.28 154.80 o 1 11 3 -2 8836.83 8852.62 232.16 o 1 11 3 -1 1.12 47.97 30.82 < 1 11 3 0 422.98 505.56 59.82 o 1 11 3 1 1035.05 1043.85 130.28 o 1 11 3 2 8468.47 9588.81 984.13 o 3 11 3 -3 1904.98 1777.64 114.24 o 3 11 3 -2 1264.96 1100.00 167.62 o 0 0 4 0 3296.31 3281.22 68.83 o 0 0 4 2 1677.16 1590.31 42.54 o 2 0 4 -2 161.14 117.61 10.90 o 2 0 4 0 2302.87 2403.39 54.88 o 2 0 4 2 1448.65 1474.65 68.00 o 4 0 4 -2 109.60 58.98 13.55 o 4 0 4 0 56.28 54.11 21.39 < 4 0 4 2 736.22 974.18 158.57 o 0 2 4 0 6090.45 6601.47 91.69 o 0 2 4 1 1419.85 1457.23 25.24 o 0 2 4 2 51.31 47.34 7.09 o 0 2 4 3 140.04 150.99 12.71 o 2 2 4 -3 138.45 171.41 11.65 o 2 2 4 -2 56.55 94.03 7.52 o 2 2 4 -1 481.05 555.23 19.89 o 2 2 4 0 1168.55 1357.42 35.42 o 2 2 4 1 237.25 241.19 18.74 o 2 2 4 2 6417.92 6528.53 115.37 o 2 2 4 3 142.32 169.75 24.57 o 4 2 4 -3 51.80 68.62 9.95 o 4 2 4 -2 11.12 28.91 10.27 < 4 2 4 -1 379.71 513.35 34.51 o 4 2 4 0 700.90 621.43 42.76 o 4 2 4 1 115.71 152.60 26.47 o 4 2 4 2 373.24 476.99 130.34 o 0 4 4 0 28064.30 27066.40 295.64 o 0 4 4 1 149.88 150.46 12.71 o 0 4 4 2 1091.51 1108.14 28.13 o 0 4 4 3 437.27 488.18 21.28 o 2 4 4 -3 24.82 46.91 8.47 o 2 4 4 -2 12.97 11.76 6.46 < 2 4 4 -1 1802.60 1616.59 34.76 o 2 4 4 0 4035.27 3888.33 61.04 o 2 4 4 1 318.47 336.78 22.66 o 2 4 4 2 1676.73 1637.60 54.89 o 2 4 4 3 74.91 85.46 21.07 o 4 4 4 -3 1.86 4.66 7.63 < 4 4 4 -2 39.48 102.83 13.87 o 4 4 4 -1 135.90 90.22 16.94 o 4 4 4 0 1942.06 2215.87 88.30 o 4 4 4 1 1782.11 1672.37 82.83 o 0 6 4 0 11.57 44.80 14.51 o 0 6 4 1 6626.42 6404.94 94.73 o 0 6 4 2 1466.45 1451.46 47.27 o 0 6 4 3 366.11 413.95 27.53 o 2 6 4 -3 12.07 17.69 9.32 < 2 6 4 -2 38.92 46.49 11.97 o 2 6 4 -1 5.28 43.63 11.23 o 2 6 4 0 3305.29 3461.70 79.08 o 2 6 4 1 7618.29 7366.86 120.28 o 2 6 4 2 419.67 427.40 32.40 o 2 6 4 3 351.12 319.86 34.41 o 4 6 4 -3 53.17 46.07 13.45 o 4 6 4 -2 12.08 22.45 10.80 < 4 6 4 -1 14.65 32.19 15.99 < 4 6 4 0 1624.88 1505.90 72.99 o 4 6 4 1 693.84 732.01 82.89 o 0 8 4 0 7064.37 7274.54 192.42 o 0 8 4 1 3424.56 3390.80 89.13 o 0 8 4 2 69.38 110.03 21.07 o 0 8 4 3 149.96 86.51 16.31 o 2 8 4 -3 210.02 310.35 29.65 o 2 8 4 -2 510.42 542.11 37.47 o 2 8 4 -1 42.05 55.81 18.32 o 2 8 4 0 2875.90 2584.04 86.55 o 2 8 4 1 4790.88 4482.24 131.61 o 2 8 4 2 124.34 114.58 27.22 o 2 8 4 3 169.50 174.51 62.48 < 4 8 4 -3 55.68 115.43 24.67 o 4 8 4 -2 21.01 15.25 19.06 < 4 8 4 -1 58.32 141.38 33.68 o 4 8 4 0 4339.12 4208.29 353.60 o 0 10 4 0 18822.40 18806.00 407.77 o 0 10 4 1 3.21 38.66 21.50 < 0 10 4 2 656.37 703.64 58.33 o 0 10 4 3 246.60 214.85 35.05 o 2 10 4 -3 39.26 100.50 25.95 o 2 10 4 -2 173.83 188.17 30.81 o 2 10 4 -1 1518.99 1434.17 77.13 o 2 10 4 0 15258.10 14807.80 297.12 o 2 10 4 1 136.98 67.88 59.83 < 4 10 4 -3 2.89 40.67 27.96 < 4 10 4 -2 9.30 -18.32 156.42 < 1 1 5 -3 601.18 662.53 18.83 o 1 1 5 -2 689.23 609.45 18.93 o 1 1 5 -1 0.58 19.70 6.14 o 1 1 5 0 109819.00 108439.00 544.05 o 1 1 5 1 862.46 921.97 26.76 o 1 1 5 2 232.86 215.03 13.98 o 1 1 5 3 2101.40 2116.07 53.58 o 3 1 5 -3 3.93 29.55 6.35 o 3 1 5 -2 559.18 515.97 20.63 o 3 1 5 -1 3230.45 3549.30 63.19 o 3 1 5 0 74466.10 74314.30 531.51 o 3 1 5 1 6969.49 7555.58 143.71 o 3 1 5 2 711.75 807.21 61.92 o 3 1 5 3 140.34 255.31 51.57 o 5 1 5 -3 331.09 293.05 27.63 o 5 1 5 -2 122.82 127.71 21.71 o 5 1 5 -1 1575.48 1804.48 98.27 o 5 1 5 0 22143.90 22097.90 394.48 o 1 3 5 -3 13.94 17.90 7.52 < 1 3 5 -2 3893.52 3672.49 51.66 o 1 3 5 -1 23660.90 23539.30 159.79 o 1 3 5 0 238.17 273.24 15.77 o 1 3 5 1 325.84 380.04 21.81 o 1 3 5 2 548.24 494.38 27.52 o 1 3 5 3 534.64 557.31 30.70 o 3 3 5 -3 239.90 145.57 11.54 o 3 3 5 -2 4586.60 4346.55 72.65 o 3 3 5 -1 13664.70 12817.40 152.95 o 3 3 5 0 1163.26 1348.42 47.08 o 3 3 5 1 2202.31 2407.85 80.03 o 3 3 5 2 1331.59 1435.67 74.06 o 3 3 5 3 695.41 586.13 69.44 o 5 3 5 -3 316.79 422.55 27.95 o 5 3 5 -2 3348.04 3345.36 96.86 o 5 3 5 -1 4104.20 3616.67 119.22 o 5 3 5 0 4932.21 4980.60 283.98 o 1 5 5 -3 240.04 289.25 19.27 o 1 5 5 -2 611.57 650.20 29.63 o 1 5 5 -1 10302.10 10096.40 123.18 o 1 5 5 0 11403.00 11093.00 112.86 o 1 5 5 1 55133.10 53457.00 333.74 o 1 5 5 2 1635.16 1636.58 49.28 o 1 5 5 3 12.80 52.42 12.50 o 3 5 5 -3 173.87 70.20 10.16 o 3 5 5 -2 3453.25 3531.01 66.27 o 3 5 5 -1 2216.56 2394.51 60.03 o 3 5 5 0 17692.60 17598.10 190.88 o 3 5 5 1 32317.80 31616.30 324.96 o 3 5 5 2 650.04 592.49 49.44 o 3 5 5 3 1349.24 1210.53 118.62 o 5 5 5 -3 965.65 988.92 42.65 o 5 5 5 -2 2437.57 2455.02 84.15 o 5 5 5 -1 456.31 566.00 50.40 o 5 5 5 0 8342.43 7456.56 256.02 o 1 7 5 -3 3121.59 3291.03 87.13 o 1 7 5 -2 4865.25 4751.36 99.42 o 1 7 5 -1 1100.70 1257.40 50.47 o 1 7 5 0 70268.40 69137.40 528.41 o 1 7 5 1 269.14 292.12 25.52 o 1 7 5 2 170.69 159.26 22.24 o 1 7 5 3 335.36 394.51 35.47 o 3 7 5 -3 2478.18 2521.24 76.51 o 3 7 5 -2 902.24 724.69 40.21 o 3 7 5 -1 248.84 269.69 28.91 o 3 7 5 0 18379.10 18617.90 253.84 o 3 7 5 1 199.89 189.33 30.28 o 3 7 5 2 576.87 518.43 101.74 o 5 7 5 -3 1499.38 1359.34 68.24 o 5 7 5 -2 280.93 286.31 43.31 o 5 7 5 -1 635.39 702.40 178.17 o 1 9 5 -3 86.39 88.53 20.65 o 1 9 5 -2 1357.68 1420.86 63.90 o 1 9 5 -1 5053.94 5019.48 126.82 o 1 9 5 0 6559.75 6656.70 156.94 o 1 9 5 1 1938.81 1990.72 79.64 o 1 9 5 2 8832.85 8277.92 176.33 o 1 9 5 3 898.78 912.47 79.06 o 3 9 5 -3 243.21 143.16 22.45 o 3 9 5 -2 1555.78 1756.21 78.92 o 3 9 5 -1 11252.70 10615.60 208.74 o 3 9 5 0 154.15 213.80 50.41 o 3 9 5 1 10.84 91.40 93.62 < 5 9 5 -3 14.73 37.70 44.48 < 1 11 5 -3 630.01 493.42 70.19 o 1 11 5 -2 1958.41 1824.03 122.06 o 1 11 5 -1 16321.00 15958.50 426.49 o 1 11 5 0 29.38 16.94 36.85 < 1 11 5 1 24009.60 21201.90 673.13 o 1 11 5 2 142.05 81.12 104.10 < 3 11 5 -3 98.95 124.64 46.17 < 3 11 5 -2 1276.72 1035.98 110.37 o 0 0 6 0 133679.00 126924.00 1358.97 o 0 0 6 2 133.34 105.99 13.13 o 2 0 6 -2 43.29 13.87 8.05 < 2 0 6 0 119818.00 119942.00 904.92 o 2 0 6 2 14973.60 14918.10 293.89 o 4 0 6 -2 84.72 158.00 22.56 o 4 0 6 0 35123.80 37129.60 575.95 o 4 0 6 2 8101.55 8272.08 704.57 o 0 2 6 0 10126.40 9862.42 127.24 o 0 2 6 1 16429.90 16182.80 138.78 o 0 2 6 2 1789.81 1748.63 40.46 o 0 2 6 3 1095.81 1016.61 33.74 o 2 2 6 -3 1004.57 929.27 26.43 o 2 2 6 -2 2668.33 2728.44 49.15 o 2 2 6 -1 537.33 478.13 22.01 o 2 2 6 0 600.38 662.07 31.54 o 2 2 6 1 35712.50 34993.10 300.02 o 2 2 6 2 16354.40 16242.30 207.85 o 2 2 6 3 2363.87 2255.23 82.67 o 4 2 6 -3 0.32 8.58 8.68 < 4 2 6 -2 1972.90 2284.10 63.84 o 4 2 6 -1 2238.18 2023.31 68.60 o 4 2 6 0 2342.37 2008.92 83.41 o 4 2 6 1 15625.10 16281.50 331.88 o 0 4 6 0 303.96 295.89 21.07 o 0 4 6 1 40779.50 40882.30 259.78 o 0 4 6 2 3534.03 3312.06 58.11 o 0 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10 -2 780.45 642.48 49.01 o 4 4 10 -1 1722.73 1881.65 101.44 o 4 4 10 0 2192.88 2008.33 177.88 o 0 6 10 0 7625.06 8350.34 207.71 o 0 6 10 1 51.25 43.84 15.25 < 0 6 10 2 157.93 227.24 26.47 o 0 6 10 3 186.17 225.12 29.97 o 2 6 10 -3 55.86 66.19 15.46 o 2 6 10 -2 347.15 402.44 33.03 o 2 6 10 -1 722.78 661.13 43.82 o 2 6 10 0 12075.90 12278.20 215.03 o 2 6 10 1 0.03 -17.47 17.37 < 2 6 10 2 162.43 212.21 50.93 o 4 6 10 -3 188.75 182.34 29.33 o 4 6 10 -2 295.75 379.06 41.51 o 4 6 10 -1 292.00 145.59 48.81 < 0 8 10 0 3126.21 3243.93 158.31 o 0 8 10 1 2486.34 2492.92 91.66 o 0 8 10 2 2491.58 2674.84 92.41 o 0 8 10 3 655.17 566.88 46.68 o 2 8 10 -3 49.46 24.36 21.60 < 2 8 10 -2 170.13 225.45 27.74 o 2 8 10 -1 402.87 449.55 42.24 o 2 8 10 0 894.94 726.19 52.18 o 2 8 10 1 1934.42 1664.18 167.76 o 4 8 10 -3 46.16 13.56 24.46 < 4 8 10 -2 122.99 126.02 63.64 < 1 1 11 -3 956.05 1016.87 50.68 o 1 1 11 -2 279.49 269.14 23.50 o 1 1 11 -1 817.59 816.23 42.33 o 1 1 11 0 78201.20 74754.40 672.55 o 1 1 11 1 588.46 634.05 37.58 o 1 1 11 2 133.12 122.41 20.97 o 1 1 11 3 2116.16 1986.69 82.80 o 3 1 11 -3 180.23 187.21 22.77 o 3 1 11 -2 221.61 220.13 22.34 o 3 1 11 -1 574.00 703.53 44.67 o 3 1 11 0 41610.50 41300.30 481.89 o 3 1 11 1 8972.56 9582.66 219.49 o 3 1 11 2 134.16 164.24 44.37 o 5 1 11 -3 52.25 84.61 23.51 o 5 1 11 -2 183.43 216.34 33.46 o 5 1 11 -1 521.80 691.54 96.77 o 1 3 11 -3 201.52 170.37 21.07 o 1 3 11 -2 4655.01 4787.80 104.53 o 1 3 11 -1 6520.19 6884.05 122.05 o 1 3 11 0 1381.09 1497.24 63.05 o 1 3 11 1 46.23 146.78 20.65 o 1 3 11 2 2129.30 2086.38 78.98 o 1 3 11 3 16.46 51.05 21.82 < 3 3 11 -3 28.33 49.14 15.46 o 3 3 11 -2 5049.31 4955.97 118.46 o 3 3 11 -1 4050.46 3860.70 108.02 o 3 3 11 0 7.98 25.31 19.38 < 3 3 11 1 329.63 452.75 52.94 o 3 3 11 2 2927.56 2770.31 400.02 o 5 3 11 -3 7.24 31.03 22.56 < 5 3 11 -2 3728.87 3571.95 174.43 o 1 5 11 -3 4.85 22.24 15.99 < 1 5 11 -2 169.43 195.58 22.24 o 1 5 11 -1 3832.41 4010.29 102.42 o 1 5 11 0 11487.80 12585.90 198.93 o 1 5 11 1 30608.10 31013.50 380.34 o 1 5 11 2 365.06 383.38 41.40 o 1 5 11 3 64.43 135.66 27.85 o 3 5 11 -3 373.60 352.77 32.50 o 3 5 11 -2 1684.98 1930.83 83.99 o 3 5 11 -1 268.74 320.83 39.71 o 3 5 11 0 14574.80 14491.10 324.84 o 3 5 11 1 21659.20 19180.10 1013.74 o 5 5 11 -3 1078.31 1092.70 81.07 o 5 5 11 -2 1511.65 1687.49 283.45 o 1 7 11 -3 3019.64 3570.60 105.16 o 1 7 11 -2 1804.79 1916.70 78.80 o 1 7 11 -1 22.68 62.38 18.96 o 1 7 11 0 56408.60 60638.20 533.94 o 1 7 11 1 1682.79 1853.70 83.68 o 1 7 11 2 14.18 40.77 23.09 < 1 7 11 3 866.13 1033.71 131.15 o 3 7 11 -3 2260.19 2757.23 92.52 o 3 7 11 -2 210.08 259.64 33.46 o 3 7 11 -1 56.71 26.90 25.73 < 3 7 11 0 17646.70 17822.80 574.38 o 1 9 11 -3 84.75 -13.56 42.47 < 1 9 11 -2 667.05 640.88 98.03 o 1 9 11 -1 3581.16 3594.21 226.65 o 1 9 11 0 3737.58 3459.32 222.94 o 3 9 11 -3 165.82 216.55 67.14 o 0 0 12 0 61854.90 57419.00 1164.69 o 0 0 12 2 80.00 113.42 30.18 o 2 0 12 -2 17.10 6.14 25.31 < 2 0 12 0 21500.20 20805.30 406.73 o 2 0 12 2 5405.91 5385.45 239.64 o 4 0 12 -2 84.76 101.45 38.34 < 4 0 12 0 4960.61 5420.33 495.78 o 0 2 12 0 10083.60 9703.71 236.60 o 0 2 12 1 9446.16 9540.93 160.57 o 0 2 12 2 122.92 131.20 21.39 o 0 2 12 3 119.92 105.47 20.12 o 2 2 12 -3 250.97 255.49 26.47 o 2 2 12 -2 133.72 177.58 25.52 o 2 2 12 -1 375.18 422.65 33.77 o 2 2 12 0 438.87 394.47 32.61 o 2 2 12 1 15335.70 14686.90 246.09 o 2 2 12 2 5728.08 5787.99 165.64 o 2 2 12 3 519.65 409.82 79.08 o 4 2 12 -3 31.99 47.23 13.98 o 4 2 12 -2 72.67 114.48 23.83 o 4 2 12 -1 40.63 85.04 27.75 o 4 2 12 0 49.77 83.87 46.38 < 0 4 12 0 17.18 61.64 22.35 < 0 4 12 1 7780.80 8440.31 166.76 o 0 4 12 2 321.17 287.46 30.81 o 0 4 12 3 64.09 107.59 23.62 o 2 4 12 -3 366.54 385.28 36.53 o 2 4 12 -2 8.05 13.45 15.14 < 2 4 12 -1 298.88 319.44 33.25 o 2 4 12 0 553.24 578.23 47.53 o 2 4 12 1 11101.40 11055.90 236.72 o 2 4 12 2 40.38 69.58 56.23 < 4 4 12 -3 169.65 154.50 27.96 o 4 4 12 -2 73.60 57.72 27.75 < 4 4 12 -1 4.62 36.96 54.22 < 0 6 12 0 26081.20 27784.30 503.54 o 0 6 12 1 1432.35 1524.79 70.57 o 0 6 12 2 1164.35 1280.86 67.83 o 0 6 12 3 74.59 130.79 28.38 o 2 6 12 -3 3.37 46.92 19.17 < 2 6 12 -2 8.70 20.86 15.36 < 2 6 12 -1 70.73 127.71 23.83 o 2 6 12 0 24736.10 26151.00 370.01 o 2 6 12 1 794.11 776.53 72.08 o 4 6 12 -3 1.72 19.80 24.04 < 4 6 12 -2 33.56 36.85 21.71 < 0 8 12 0 438.90 627.41 97.40 o 0 8 12 1 331.26 383.93 59.51 o 0 8 12 2 1711.81 1881.70 146.10 o 2 8 12 -3 32.68 6.57 21.92 < 2 8 12 -2 80.46 146.25 44.27 o 2 8 12 -1 97.49 163.19 63.01 < 1 1 13 -3 67.04 55.60 23.19 < 1 1 13 -2 220.70 218.34 28.91 o 1 1 13 -1 362.86 356.38 37.48 o 1 1 13 0 5948.67 5671.47 152.23 o 1 1 13 1 10781.70 10400.40 206.88 o 1 1 13 2 189.78 206.70 30.28 o 1 1 13 3 24.38 15.04 19.91 < 3 1 13 -3 45.42 56.76 19.59 < 3 1 13 -2 612.54 662.25 48.69 o 3 1 13 -1 10.52 56.87 21.29 < 3 1 13 0 7137.22 6756.93 194.27 o 3 1 13 1 3670.51 3503.20 240.06 o 5 1 13 -3 215.63 241.43 37.70 o 5 1 13 -2 524.83 515.91 130.43 o 1 3 13 -3 41.73 102.19 26.58 o 1 3 13 -2 131.04 127.71 25.63 o 1 3 13 -1 961.48 1073.95 66.78 o 1 3 13 0 56486.00 55647.90 676.76 o 1 3 13 1 55.23 108.34 25.31 o 1 3 13 2 1171.22 1103.18 69.74 o 1 3 13 3 143.73 103.35 38.76 < 3 3 13 -3 177.98 306.34 38.65 o 3 3 13 -2 154.63 149.31 25.41 o 3 3 13 -1 183.93 147.29 29.23 o 3 3 13 0 25671.00 25124.10 822.62 o 5 3 13 -3 277.80 294.36 103.87 < 1 5 13 -3 64.24 53.27 20.44 < 1 5 13 -2 149.92 166.25 26.79 o 1 5 13 -1 1747.72 1808.68 80.39 o 1 5 13 0 3814.53 4011.17 126.54 o 1 5 13 1 2775.60 3035.55 117.13 o 1 5 13 2 2193.51 2213.88 120.56 o 1 5 13 3 755.95 809.68 176.25 o 3 5 13 -3 3.46 30.08 19.27 < 3 5 13 -2 112.50 223.76 35.37 o 3 5 13 -1 3825.14 3986.95 156.99 o 3 5 13 0 5546.94 5259.67 272.61 o 1 7 13 -3 6.77 -12.18 31.77 < 1 7 13 -2 2303.95 2603.31 154.18 o 1 7 13 -1 14814.00 16751.70 412.12 o 1 7 13 0 642.82 561.91 80.35 o 1 7 13 1 9901.60 10102.90 356.36 o 3 7 13 -3 4.54 1.16 29.97 < 3 7 13 -2 1589.78 1412.32 133.20 o 0 0 14 0 3609.13 3577.45 234.07 o 0 0 14 2 4722.64 4369.10 200.76 o 2 0 14 -2 4176.38 3745.34 204.73 o 2 0 14 0 5252.23 5464.25 281.23 o 4 0 14 -2 4205.16 3639.69 231.41 o 0 2 14 0 12604.40 11983.40 395.33 o 0 2 14 1 2442.85 2220.25 99.17 o 0 2 14 2 12.97 14.09 17.90 < 0 2 14 3 317.01 253.59 32.08 o 2 2 14 -3 28.06 47.44 25.20 < 2 2 14 -2 574.91 614.63 53.14 o 2 2 14 -1 3.68 47.45 15.89 < 2 2 14 0 18983.30 18663.40 294.42 o 2 2 14 1 8526.86 7965.57 269.42 o 4 2 14 -3 150.80 179.60 31.87 o 4 2 14 -2 582.45 483.80 103.85 o 0 4 14 0 57153.10 57310.90 939.09 o 0 4 14 1 1752.42 1893.23 92.03 o 0 4 14 2 850.80 846.12 63.82 o 0 4 14 3 2084.01 2220.89 108.09 o 2 4 14 -3 1292.08 1426.76 77.56 o 2 4 14 -2 132.72 96.36 24.67 o 2 4 14 -1 924.06 946.00 66.89 o 2 4 14 0 27098.50 28429.20 548.87 o 2 4 14 1 3228.38 3378.19 366.32 o 4 4 14 -3 534.12 679.78 101.00 o 4 4 14 -2 11.80 15.04 56.23 < 0 6 14 0 4934.51 5719.41 376.99 o 0 6 14 1 119.47 155.99 43.42 o 0 6 14 2 583.16 568.29 94.75 o 0 6 14 3 21.54 84.83 91.18 < 2 6 14 -3 169.14 188.07 54.22 o 2 6 14 -2 1059.60 1078.23 130.81 o 2 6 14 -1 3547.13 4143.35 255.61 o 2 6 14 0 440.15 283.64 118.69 < 4 6 14 -3 4.08 71.06 86.63 < 1 1 15 -3 235.49 235.71 34.41 o 1 1 15 -2 192.97 187.64 35.26 o 1 1 15 -1 1254.73 1103.11 74.39 o 1 1 15 0 125.22 146.98 28.38 o 1 1 15 1 11803.10 11222.10 241.05 o 1 1 15 2 50.04 72.54 33.46 < 1 1 15 3 0.74 -48.93 56.34 < 3 1 15 -3 279.62 388.17 46.17 o 3 1 15 -2 177.56 138.93 32.40 o 3 1 15 -1 165.74 229.58 53.69 o 1 3 15 -3 57.22 85.78 32.72 < 1 3 15 -2 8.92 26.37 23.09 < 1 3 15 -1 539.72 569.14 59.18 o 1 3 15 0 21044.70 20386.60 331.88 o 1 3 15 1 374.39 350.88 62.36 o 1 3 15 2 872.27 742.62 180.47 o 3 3 15 -3 125.00 113.63 30.39 o 3 3 15 -2 19.53 -5.19 24.68 < 3 3 15 -1 219.63 175.57 86.51 < 1 5 15 -3 2.67 132.70 74.77 < 1 5 15 -2 92.25 197.18 93.08 < 1 5 15 -1 433.47 514.03 107.99 o 1 5 15 0 381.76 496.04 105.46 o 1 5 15 1 355.69 344.64 134.05 < 3 5 15 -3 8.90 9.43 40.56 < 3 5 15 -2 167.09 152.70 88.63 < 0 0 16 0 78338.30 72581.70 2192.35 o 0 0 16 2 48.02 58.46 38.34 < 2 0 16 -2 122.55 116.91 40.77 < 2 0 16 0 42854.40 42030.80 1702.64 o 0 2 16 0 1980.35 1582.95 148.50 o 0 2 16 1 86.71 114.05 43.84 < 0 2 16 2 245.22 326.45 66.50 o 0 2 16 3 276.68 239.09 66.18 o 2 2 16 -3 87.52 63.96 25.31 < 2 2 16 -2 631.43 626.28 78.97 o 2 2 16 -1 921.97 945.18 101.29 o 2 2 16 0 6569.53 5991.33 381.81 o 4 2 16 -3 23.30 11.54 63.22 < 0 4 16 0 2275.39 2117.50 217.85 o 0 4 16 1 9883.16 11876.00 772.41 o 0 4 16 2 1356.15 1864.15 314.27 o 2 4 16 -3 3.50 -37.91 33.57 < 2 4 16 -2 1361.55 1583.20 274.38 o 1 1 17 -3 443.01 354.79 75.70 o 1 1 17 -1 1611.65 1594.59 257.30 o 1 1 17 0 12917.80 11323.20 503.30 o 3 1 17 -3 156.30 159.79 70.53 <