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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_I _audit_creation_method 'Jana2006 Version : 05/01/2012' _journal_name_full 'Journal of Solid State Chemistry' _journal_year 2013 _journal_volume 199 _journal_issue ? _journal_page_first 84 _journal_page_last 89 _journal_paper_doi https://doi.org/10.1016/j.jssc.2012.11.029 _publ_section_title ;The composite structure of mixed \t-(Ag, Cu)~x~V~2~O~5~bronzes-Evidence for \T dependant guest-species ordering and mobility ; _publ_contact_author_name 'Lidin, Sven' _publ_contact_author_address ;Centre for Analysis and Synthesis (CAS) PO Box 124 Lund University 221 00 Lund Sweden ; _publ_contact_author_email Sven.Lidin@polymat.lth.se loop_ _publ_author_name _publ_author_address 'Hermes, Wilfred' ;Centre for Analysis and Synthesis (CAS) PO Box 124 Lund University 221 00 Lund Sweden ; 'Dolle, Mickael' ;Centre d'Elaboration de Mat\'eriaux et d'Etudes Structurales (CEMES-CNRS) UPR CNRS 8011, Universit\'e de Toulouse 29 rue J. Marvig BP 94347 31055 Toulouse Cedex France ; 'Rozier, Patrick' ;Centre d'Elaboration de Mat\'eriaux et d'Etudes Structurales (CEMES-CNRS) UPR CNRS 8011, Universit\'e de Toulouse 29 rue J. Marvig BP 94347 31055 Toulouse Cedex France ; 'Lidin, Sven' ;Centre for Analysis and Synthesis (CAS) PO Box 124 Lund University 221 00 Lund Sweden ; _chemical_formula_sum 'Ag0.46 Cu0.46 O5 V2' _chemical_formula_weight 260.7 _space_group_crystal_system monoclinic _space_group_ssg_name X2(0\b0)0 loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,x2,-x3,x4 3 x1+1/2,x2+1/2,x3,x4 4 -x1+1/2,x2+1/2,-x3,x4 5 x1,x2,x3+1/2,x4+1/2 6 -x1,x2,-x3+1/2,x4+1/2 7 x1+1/2,x2+1/2,x3+1/2,x4+1/2 8 -x1+1/2,x2+1/2,-x3+1/2,x4+1/2 _cell_length_a 11.7826(12) _cell_length_b 3.7387(19) _cell_length_c 18.923(2) _cell_angle_alpha 90 _cell_angle_beta 114.621(10) _cell_angle_gamma 90 _cell_volume 757.8(4) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0 0.9207 0 _cell_subsystems_number 2 loop_ _cell_subsystem_code _cell_subsystem_description _cell_subsystem_matrix_W_1_1 _cell_subsystem_matrix_W_1_2 _cell_subsystem_matrix_W_1_3 _cell_subsystem_matrix_W_1_4 _cell_subsystem_matrix_W_2_1 _cell_subsystem_matrix_W_2_2 _cell_subsystem_matrix_W_2_3 _cell_subsystem_matrix_W_2_4 _cell_subsystem_matrix_W_3_1 _cell_subsystem_matrix_W_3_2 _cell_subsystem_matrix_W_3_3 _cell_subsystem_matrix_W_3_4 _cell_subsystem_matrix_W_4_1 _cell_subsystem_matrix_W_4_2 _cell_subsystem_matrix_W_4_3 _cell_subsystem_matrix_W_4_4 1 '1st subsystem' 1 0 0 0 0 1 0 0 0 0 1 0 0 0 0 1 2 '2nd subsystem' 1 0 0 0 0 0 0 1 0 0 1 0 0 1 0 0 _cell_formula_units_Z 8 _cell_measurement_temperature 293 _exptl_crystal_type_of_structure comp _exptl_crystal_density_diffrn 4.5692 _exptl_crystal_F_000 968 _exptl_absorpt_coefficient_mu 9.644 _diffrn_ambient_temperature 293 _diffrn_source 'X-ray tube' _diffrn_radiation_wavelength 0.71069 _diffrn_reflns_number 15274 _diffrn_reflns_theta_min 2.52 _diffrn_reflns_theta_max 31.55 _diffrn_reflns_theta_full 15.44 _diffrn_measured_fraction_theta_max 0.61 _diffrn_measured_fraction_theta_full 0.8 _diffrn_reflns_av_R_equivalents 0.0299 _diffrn_reflns_av_unetI/netI 0.0255 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -5 _diffrn_reflns_limit_k_max 5 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_index_m_1_min -2 _diffrn_reflns_limit_index_m_1_max 2 loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? _diffrn_radiation_probe x-ray _reflns_number_total 3246 _reflns_number_gt 2264 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0446 _refine_ls_wR_factor_gt 0.1085 _refine_ls_R_factor_all 0.0623 _refine_ls_wR_factor_ref 0.1307 _refine_ls_goodness_of_fit_ref 3.09 _refine_ls_goodness_of_fit_gt 3.1 _refine_ls_number_reflns 3246 _refine_ls_number_parameters 110 _refine_ls_number_constraints 1 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(I)+0.0004I^2^) _refine_ls_shift/su_max 0.0492 _refine_ls_shift/su_mean 0.0070 _refine_diff_density_max 2.67 _refine_diff_density_min -2.79 _refine_ls_extinction_method none loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ag -0.8971 1.1015 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Cu 0.3201 1.2651 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.006 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' V 0.3005 0.5294 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_subsystem_code V1 V 0.5104(4) 0.0151(4) 0.16759(3) Uani 0.00561(19) 8 1 d ? ? ? 1 V2 V 0.21236(5) 0.0147(4) 0.16963(3) Uani 0.00607(19) 8 1 d ? ? ? 1 O1 O 0.3861(2) 0.022(2) 0.19628(14) Uiso 0.0075(5) 8 1 d ? ? ? 1 O2 O 0.5537(2) -0.474(2) 0.1813(14) Uiso 0.0065(6) 8 1 d ? ? ? 1 O3 O 0.1993(2) -0.482(2) 0.19351(14) Uiso 0.0065(6) 8 1 d ? ? ? 1 O4 O 0.4388(2) 0.018(2) 0.0711(15) Uiso 0.0114(6) 8 1 d ? ? ? 1 O5 O 0.1627(2) 0.018(3) 0.07398(15) Uiso 0.0114(6) 8 1 d ? ? ? 1 Ag1 Ag 0.7582(5) 0(16) 0.0124(4) Uani 0.0149(3) 8 1 d ? ? ? 2 Cu2 Cu 0.5 0.5(16) 1 Uani 0.0258(9) 4 1 d ? ? ? 2 loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 V1 V 0.0043(2) 0.0055(3) 0.0076(3) -0.0004(8) 0.00298(20) 0.0007(10) V2 V 0.0055(2) 0.0052(3) 0.0086(3) 0.0013(8) 0.0039(2) 0.0018(9) Ag1 Ag 0.0127(3) 0.0156(7) 0.0176(5) 0.0011(9) 0.0076(3) 0.0043(12) Cu2 Cu 0.013(4) 0.047(3) 0.015(5) 0 0.0039(4) 0 loop_ _atom_site_Fourier_wave_vector_seq_id _jana_atom_site_Fourier_wave_vector_q1_coeff 1 1 2 2 loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id V1x1 V1 x 1 V1y1 V1 y 1 V1z1 V1 z 1 V2x1 V2 x 1 V2y1 V2 y 1 V2z1 V2 z 1 O1x1 O1 x 1 O1y1 O1 y 1 O1z1 O1 z 1 O2x1 O2 x 1 O2y1 O2 y 1 O2z1 O2 z 1 O3x1 O3 x 1 O3y1 O3 y 1 O3z1 O3 z 1 O4x1 O4 x 1 O4y1 O4 y 1 O4z1 O4 z 1 O5x1 O5 x 1 O5y1 O5 y 1 O5z1 O5 z 1 Ag1x1 Ag1 x 1 Ag1y1 Ag1 y 1 Ag1z1 Ag1 z 1 Cu2x1 Cu2 x 1 Cu2y1 Cu2 y 1 Cu2z1 Cu2 z 1 Cu2x2 Cu2 x 2 Cu2y2 Cu2 y 2 Cu2z2 Cu2 z 2 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin V1x1 -0.002(6) -0.001(17) V1y1 0.0002(17) 0(2) V1z1 -0.003(14) 0(3) V2x1 -0.002(5) 0(2) V2y1 0(7) 0.01(3) V2z1 -0.0022(7) 0(2) O1x1 -0.005(4) 0(5) O1y1 0.002(5) 0(2) O1z1 -0.006(9) 0(6) O2x1 0(2) 0(2) O2y1 0(2) 0(2) O2z1 0(4) 0(3) O3x1 0.001(14) 0.001(6) O3y1 0(9) -0.0088(19) O3z1 0(5) 0.004(9) O4x1 0.01(4) 0(9) O4y1 0(6) 0.01(2) O4z1 -0.003(13) 0(3) O5x1 -0.01(5) 0.01(6) O5y1 0.02(18) 0.02(18) O5z1 0(6) 0.001(3) Ag1x1 0.002(2) 0.027(5) Ag1y1 0.082(3) -0.309(10) Ag1z1 -0.0016(16) 0.047(4) Cu2x1 0 0 Cu2y1 0.0233(17) 0.0546(10) Cu2z1 0 0 Cu2x2 0 0 Cu2y2 0.0401(17) 0.0001(9) Cu2z2 0 0 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 1 -5 0 0 1992.28 1879.25 89.71 o 3 -5 0 0 6731.20 6006.95 103.97 o 5 -5 0 0 95.77 64.57 57.32 < 0 -4 0 0 51479.90 51640.50 335.16 o 2 -4 0 0 176.79 92.26 26.69 o 4 -4 0 0 11263.20 10781.30 167.17 o 6 -4 0 0 845.67 905.35 68.18 o 8 -4 0 0 377.48 268.50 60.21 o 1 -3 0 0 4658.28 4666.41 85.83 o 3 -3 0 0 17707.40 17947.80 93.15 o 5 -3 0 0 917.18 1056.37 38.73 o 7 -3 0 0 17658.50 17685.60 136.29 o 9 -3 0 0 26.67 35.51 26.02 < 11 -3 0 0 9252.50 9239.29 102.85 o 13 -3 0 0 97.54 53.55 59.83 < 0 -2 0 0 233529.00 190884.00 1070.02 o 2 -2 0 0 1401.68 1442.39 17.62 o 4 -2 0 0 37196.20 37646.70 77.03 o 6 -2 0 0 932.08 903.03 20.43 o 8 -2 0 0 1189.19 1199.59 25.57 o 10 -2 0 0 6852.26 6972.05 59.74 o 12 -2 0 0 594.96 719.09 34.14 o 14 -2 0 0 7088.08 6465.89 115.06 o 1 -1 0 0 13308.40 13976.30 42.64 o 3 -1 0 0 50374.20 51558.20 283.65 o 5 -1 0 0 5881.37 6360.87 36.58 o 7 -1 0 0 40056.40 39577.10 96.44 o 9 -1 0 0 416.59 460.26 19.01 o 11 -1 0 0 19124.10 17905.10 85.08 o 13 -1 0 0 1139.22 1412.01 41.59 o 15 -1 0 0 3288.36 2853.38 116.68 o 2 0 0 0 227.40 244.32 6.88 o 4 0 0 0 146061.00 146569.00 514.71 o 6 0 0 0 4186.39 4569.52 30.08 o 8 0 0 0 14059.40 13440.40 59.36 o 10 0 0 0 12825.40 12712.70 74.11 o 12 0 0 0 394.74 265.86 23.28 o 14 0 0 0 11109.00 10261.30 85.43 o 1 1 0 0 13152.50 15226.50 71.85 o 3 1 0 0 50128.30 51084.40 304.81 o 5 1 0 0 5960.83 6422.68 35.81 o 7 1 0 0 39951.70 39221.20 104.27 o 9 1 0 0 364.69 491.61 20.91 o 11 1 0 0 19031.20 17887.70 93.83 o 13 1 0 0 1175.20 1369.02 36.51 o 15 1 0 0 3231.02 2637.21 81.39 o 2 2 0 0 1411.44 1443.73 26.54 o 4 2 0 0 37024.10 37579.00 112.09 o 6 2 0 0 902.90 900.69 26.12 o 8 2 0 0 1201.53 1165.54 28.56 o 10 2 0 0 6763.80 7102.61 67.66 o 12 2 0 0 641.25 717.52 33.07 o 14 2 0 0 7015.78 6829.61 120.24 o 1 3 0 0 4691.83 4747.75 118.20 o 3 3 0 0 17680.30 18278.70 241.51 o 5 3 0 0 904.85 1061.00 68.28 o 7 3 0 0 17742.70 17821.40 225.91 o 9 3 0 0 9.02 16.32 49.97 < 11 3 0 0 9328.40 9732.85 194.90 o 0 4 0 0 51820.30 52390.90 451.84 o 2 4 0 0 167.25 78.65 103.47 < 4 4 0 0 11184.90 11206.50 260.97 o 6 4 0 0 839.62 908.49 95.05 o 8 4 0 0 336.49 350.58 77.88 o -9 -5 1 1 50.36 60.31 119.69 < -7 -5 1 1 15.16 -49.46 107.64 < -5 -5 1 1 51.10 6.05 98.20 < -3 -5 1 1 156.04 167.13 62.00 < -1 -5 1 1 68.69 77.59 44.60 < 1 -5 1 1 11.52 59.11 55.73 < 3 -5 1 1 140.68 6.05 91.55 < 5 -5 1 1 110.68 85.12 99.29 < 7 -5 1 1 327.11 197.17 116.31 < 9 -5 1 1 100.23 120.83 125.30 < -12 -4 1 1 35.91 39.48 94.22 < -10 -4 1 1 126.60 86.97 76.39 < -8 -4 1 1 17.82 59.65 67.18 < -6 -4 1 1 86.14 65.00 58.56 < -4 -4 1 -1 573.06 707.05 91.88 o -4 -4 1 1 220.90 102.62 83.64 < -2 -4 1 -1 514.76 512.99 113.04 o -2 -4 1 1 269.22 139.86 52.35 < 0 -4 1 -1 257.79 326.18 72.08 o 0 -4 1 1 678.72 563.43 76.56 o 2 -4 1 -1 261.43 215.16 74.65 < 2 -4 1 1 409.06 297.34 68.43 o 4 -4 1 -1 158.63 116.31 122.52 < 4 -4 1 1 360.56 130.59 54.53 < 6 -4 1 1 24.95 52.62 45.91 < 8 -4 1 1 147.59 96.46 51.86 < 10 -4 1 1 11.66 44.71 61.67 < 12 -4 1 1 25.38 9.65 79.23 < -13 -3 1 1 74.18 48.31 59.43 < -11 -3 1 1 165.43 265.71 52.67 o -9 -3 1 -1 513.64 688.84 140.19 o -9 -3 1 1 191.91 169.36 38.66 o -7 -3 1 -1 465.23 533.22 120.83 o -7 -3 1 1 174.76 226.18 34.19 o -5 -3 1 -1 14.73 36.53 95.42 < -5 -3 1 1 30.10 25.08 22.79 < -3 -3 1 -1 21.25 20.83 87.46 < -3 -3 1 1 460.77 463.43 21.43 o -1 -3 1 -1 288.18 305.90 47.82 o -1 -3 1 1 3.95 8.23 23.56 < 1 -3 1 -1 166.86 235.01 57.91 o 1 -3 1 1 34.69 35.17 19.74 < 3 -3 1 -1 594.58 647.78 104.86 o 3 -3 1 1 847.07 907.50 27.59 o 5 -3 1 -1 239.51 292.65 104.91 < 5 -3 1 1 234.53 157.48 25.46 o 7 -3 1 -1 980.06 1098.01 140.13 o 7 -3 1 1 1092.33 1123.53 44.55 o 9 -3 1 -1 324.80 440.85 134.46 o 9 -3 1 1 171.29 153.99 39.64 o 11 -3 1 1 411.16 567.57 60.91 o 13 -3 1 1 211.28 204.26 71.65 < -14 -2 1 1 11.04 93.51 59.49 < -12 -2 1 -1 88.45 92.59 72.58 < -12 -2 1 1 19.12 58.29 40.57 < -10 -2 1 -1 1058.14 788.19 70.99 o -10 -2 1 1 450.17 461.95 39.80 o -8 -2 1 -1 1016.77 1391.64 69.36 o -8 -2 1 1 145.51 232.23 32.33 o -6 -2 1 -1 2693.44 2555.31 94.50 o -6 -2 1 1 972.21 1082.47 35.93 o -4 -2 1 -1 3086.02 3641.87 93.62 o -4 -2 1 1 1461.41 1593.83 26.45 o -2 -2 1 -1 3973.32 4026.83 92.15 o -2 -2 1 1 2501.78 2633.17 27.97 o 0 -2 1 -1 2671.55 3035.69 116.31 o 2 -2 1 -1 2956.47 2585.08 74.05 o 2 -2 1 1 2657.79 2699.04 33.10 o 4 -2 1 -1 1494.46 1587.72 48.47 o 4 -2 1 1 1036.42 947.03 31.90 o 6 -2 1 -1 773.57 620.25 52.67 o 6 -2 1 1 258.37 268.49 27.21 o 8 -2 1 -1 532.84 506.12 58.56 o 8 -2 1 1 234.98 192.86 32.28 o 10 -2 1 -1 8.39 75.63 60.85 < 10 -2 1 1 97.27 53.00 34.68 < 12 -2 1 -1 37.89 51.91 73.72 < 12 -2 1 1 129.76 175.30 53.38 o 14 -2 1 1 216.46 264.13 65.87 o -15 -1 1 1 690.69 1018.79 69.14 o -13 -1 1 -1 1128.86 1161.21 73.28 o -13 -1 1 1 1078.63 1123.75 60.63 o -11 -1 1 -1 2617.16 2827.02 71.32 o -11 -1 1 1 1174.95 1679.38 57.58 o -9 -1 1 -1 1450.99 1484.94 51.15 o -9 -1 1 1 1901.09 1976.01 48.58 o -7 -1 1 -1 3006.25 2939.83 56.22 o -7 -1 1 1 1252.89 1343.28 36.10 o -5 -1 1 -1 136.81 41.06 22.41 < -5 -1 1 1 377.05 337.85 20.94 o -3 -1 1 -1 871.97 684.21 22.74 o -3 -1 1 1 456.01 415.28 17.23 o -1 -1 1 -1 1680.80 1253.69 34.68 o 1 -1 1 -1 340.36 175.25 26.17 o 3 -1 1 -1 4350.74 4209.28 44.28 o 3 -1 1 1 3175.22 3137.50 32.50 o 5 -1 1 -1 1099.27 1028.60 32.17 o 5 -1 1 1 2240.31 2341.40 36.86 o 7 -1 1 -1 5366.26 5863.75 74.97 o 7 -1 1 1 3961.56 4313.43 54.09 o 9 -1 1 -1 1255.01 1205.92 49.89 o 9 -1 1 1 1734.46 1686.36 46.78 o 11 -1 1 -1 3006.56 3620.66 80.97 o 11 -1 1 1 1784.74 2547.89 66.31 o 13 -1 1 -1 982.50 808.97 80.32 o 13 -1 1 1 1251.54 1060.94 62.11 o 15 -1 1 1 523.23 487.96 147.71 o -14 0 1 -1 1318.12 1416.89 80.21 o -14 0 1 1 1348.03 1346.33 69.69 o -12 0 1 -1 79.17 106.38 44.55 < -12 0 1 1 91.84 105.89 43.19 < -10 0 1 -1 8086.83 8135.84 86.10 o -10 0 1 1 8113.27 8433.50 95.75 o -8 0 1 -1 156.63 232.12 31.90 o -8 0 1 1 215.73 220.13 33.59 o -6 0 1 -1 22411.20 23917.60 114.83 o -6 0 1 1 22230.90 23614.70 112.11 o -4 0 1 -1 1640.99 1639.52 29.66 o -4 0 1 1 1723.24 1550.32 29.23 o -2 0 1 -1 43913.20 41108.80 89.53 o -2 0 1 1 43824.20 42530.00 100.39 o 0 0 1 -1 2004.38 1476.92 47.71 o 0 0 1 1 2074.41 1757.47 65.60 o 2 0 1 -1 38885.10 38017.50 104.42 o 2 0 1 1 38822.90 37572.40 122.20 o 4 0 1 -1 357.49 373.46 25.85 o 4 0 1 1 376.83 351.70 24.48 o 6 0 1 -1 13004.10 14126.00 83.64 o 6 0 1 1 12912.40 14070.50 91.06 o 8 0 1 -1 7.12 36.91 30.04 < 8 0 1 1 30.17 67.67 32.93 < 10 0 1 -1 2583.56 3098.07 62.00 o 10 0 1 1 2560.22 3211.71 68.76 o 12 0 1 -1 625.21 845.77 61.83 o 12 0 1 1 660.63 729.47 53.44 o 14 0 1 -1 238.51 275.64 65.71 o 14 0 1 1 253.90 239.48 63.80 o -15 1 1 -1 676.52 971.51 68.60 o -15 1 1 1 1480.17 1967.72 191.23 o -13 1 1 -1 1069.74 1026.37 60.58 o -13 1 1 1 1090.77 1231.55 72.90 o -11 1 1 -1 1207.36 1617.44 56.71 o -11 1 1 1 2621.09 2825.22 79.77 o -9 1 1 -1 1882.30 2032.07 49.51 o -9 1 1 1 1384.19 1370.65 56.22 o -7 1 1 -1 1255.92 1308.38 35.66 o -7 1 1 1 3050.97 2888.58 54.36 o -5 1 1 -1 380.70 313.59 20.56 o -5 1 1 1 123.92 19.96 28.68 < -3 1 1 -1 449.58 414.41 17.01 o -3 1 1 1 899.20 702.69 34.19 o -1 1 1 1 1702.46 1289.68 85.17 o 1 1 1 -1 665.86 1.80 7.31 < 1 1 1 1 291.45 183.76 62.00 < 3 1 1 -1 3176.76 3209.25 32.23 o 3 1 1 1 4451.61 4297.45 62.43 o 5 1 1 -1 2234.53 2343.31 37.51 o 5 1 1 1 1047.29 1004.77 34.90 o 7 1 1 -1 3910.96 4408.25 54.42 o 7 1 1 1 5508.44 5967.57 83.54 o 9 1 1 -1 1743.64 1759.70 52.51 o 9 1 1 1 1183.32 1225.99 56.27 o 11 1 1 -1 1811.69 2417.14 66.25 o 11 1 1 1 3023.39 3595.80 89.81 o 13 1 1 -1 1238.45 1073.75 62.38 o 13 1 1 1 941.36 830.34 71.49 o 15 1 1 -1 538.75 601.22 154.31 o -14 2 1 -1 11.38 31.84 57.91 < -12 2 1 -1 14.66 20.94 44.55 < -12 2 1 1 92.31 177.16 133.76 < -10 2 1 -1 430.87 406.39 42.53 o -10 2 1 1 1057.88 918.29 137.08 o -8 2 1 -1 161.10 285.29 34.62 o -8 2 1 1 1025.69 1185.80 133.15 o -6 2 1 -1 959.88 1104.28 35.12 o -6 2 1 1 2626.38 2312.66 146.62 o -4 2 1 -1 1473.08 1509.20 29.01 o -4 2 1 1 3125.36 3697.54 183.27 o -2 2 1 -1 2470.85 2562.23 36.59 o -2 2 1 1 3936.79 3420.38 135.77 o 0 2 1 -1 3198.91 2908.32 87.19 o 0 2 1 1 2724.41 2987.49 207.97 o 2 2 1 -1 2635.43 2702.64 40.95 o 2 2 1 1 2938.44 2804.44 210.31 o 4 2 1 -1 1038.83 875.33 29.23 o 4 2 1 1 1526.95 1712.92 146.68 o 6 2 1 -1 262.27 259.60 29.55 o 6 2 1 1 750.33 637.59 110.64 o 8 2 1 -1 251.38 190.63 35.82 o 8 2 1 1 545.23 380.00 115.27 o 10 2 1 -1 99.95 16.63 37.51 < 10 2 1 1 8.58 45.20 119.90 < 12 2 1 -1 113.73 233.65 54.31 o 14 2 1 -1 238.97 202.90 65.05 o -13 3 1 -1 78.84 104.64 68.76 < -11 3 1 -1 174.38 181.14 50.06 o -9 3 1 -1 195.66 133.05 42.31 o -9 3 1 1 535.24 748.60 171.16 o -7 3 1 -1 171.86 198.42 44.88 o -7 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