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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_CdNi _audit_creation_method 'Jana2006 Version : 08/11/2010' _journal_date_recd_electronic 2005-03-17 _journal_date_accepted 2005-04-21 _journal_name_full 'Acta Crystallographica, Section B' _journal_year 2005 _journal_volume 61 _journal_issue 3 _journal_page_first 280 _journal_page_last 286 _journal_paper_category FA _journal_paper_doi https://doi.org/10.1107/S0108768105012632 _publ_contact_author_name 'Petricek, Vaclav' _publ_contact_author_address ;Institute of Physics Academy of Sciences of the Czech Republic Na Slovance 2 182 21 Praha Czech Republic ; _publ_contact_author_email petricek@fzu.cz _publ_section_title ;Modulated one-dimensional structure of [Cd(NH~3~)~3~Ni(CN)~4~] ; _publ_section_title_footnote ? loop_ _publ_author_name _publ_author_address 'Petricek, Vaclav' ;Institute of Physics Academy of Sciences of the Czech Republic Na Slovance 2 182 21 Praha Czech Republic ; 'Dusek, Michal' ;Institute of Physics Academy of Sciences of the Czech Republic Na Slovance 2 182 21 Praha Czech Republic ; 'Cernak, Juraj' ;Institute of Chemistry P.J. Safarik University Moyzesova 11 04154 Kosice Slovakia ; _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'C4 H9 Cd1 N7 Ni1' _chemical_formula_weight 326.3 _space_group_crystal_system monoclinic _space_group_ssg_name C2/c(\a0\g)0s loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,x2,-x3+1/2,-x4+1/2 3 -x1,-x2,-x3,-x4 4 x1,-x2,x3+1/2,x4+1/2 5 x1+1/2,x2+1/2,x3,x4 6 -x1+1/2,x2+1/2,-x3+1/2,-x4+1/2 7 -x1+1/2,-x2+1/2,-x3,-x4 8 x1+1/2,-x2+1/2,x3+1/2,x4+1/2 _cell_length_a 8.4867(14) _cell_length_b 15.951(3) _cell_length_c 7.604(3) _cell_angle_alpha 90 _cell_angle_beta 90.48(2) _cell_angle_gamma 90 _cell_volume 1029.3(4) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.4365 0 0.1307 _cell_formula_units_Z 4 _cell_measurement_reflns_used 30 _cell_measurement_theta_min 9.08 _cell_measurement_theta_max 16.29 _cell_measurement_temperature 260.0(10) _cell_special_details ? _exptl_crystal_type_of_structure mod _exptl_crystal_density_diffrn 2.1047 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 620 _exptl_absorpt_coefficient_mu 3.862 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details '(Jana2000; Petricek, Dusek & Palatinus, 2000)' _exptl_absorpt_correction_T_min 0.660 _exptl_absorpt_correction_T_max 0.807 _exptl_crystal_description ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_size_rad ? _exptl_crystal_colour ? _exptl_special_details ? _diffrn_ambient_temperature 293 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71069 _diffrn_source ? _diffrn_radiation_monochromator ? _diffrn_measurement_device_type 'Oxford Diffraction point detector' _diffrn_measurement_method '\q/2\q' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 15484 _diffrn_reflns_av_R_equivalents 0.0862 _diffrn_reflns_av_unetI/netI 0.0928 _diffrn_reflns_theta_min 1.49 _diffrn_reflns_theta_max 27.10 _diffrn_reflns_theta_full 27.10 _diffrn_measured_fraction_theta_max ? _diffrn_measured_fraction_theta_full 1.00 _diffrn_reflns_limit_h_min 0 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_reduction_process ? _diffrn_standards_number 3 _diffrn_standards_interval_count 100 _diffrn_standards_interval_time ? _diffrn_standards_decay_% 1.4 loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l 6 0 0 0 0 8 0 0 0 0 6 0 _refine_special_details ? _reflns_number_total 7894 _reflns_number_gt 3496 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef F _refine_ls_R_factor_gt 0.0371 _refine_ls_wR_factor_gt 0.0425 _refine_ls_R_factor_all 0.0371 _refine_ls_wR_factor_ref 0.0425 _refine_ls_goodness_of_fit_ref 1.78 _refine_ls_restrained_S_gt ? _refine_ls_number_reflns 3496 _refine_ls_number_parameters 275 _refine_ls_number_restraints ? _refine_ls_number_constraints ? _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(F)+0.0001F^2^) _refine_ls_hydrogen_treatment constr _refine_ls_shift/su_max 0.0000 _refine_ls_shift/su_mean 0.0000 _refine_diff_density_max 0.95 _refine_diff_density_min -0.99 _refine_ls_extinction_method none _refine_ls_extinction_coef ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cd -0.808 1.202 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Ni 0.339 1.112 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' N 0.006 0.003 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' C 0.003 0.002 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0 0 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.011 0.006 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction 'Jana2000 (Petricek & Dusek, 2000)' _computing_structure_solution 'SIR97 (Altomare et al., 1997)' _computing_structure_refinement 'Jana2000 (Petricek & Dusek, 2000)' _computing_molecular_graphics 'Diamond (Brandenburg, 1999)' _computing_publication_material 'Jana2000 (Petricek & Dusek, 2000)' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_type_symbol Cd1 1 0.20155(4) 0.25 0.0247(2) Uani d . 1 . . Cd Cd2 1 0.14519(4) 0.25 0.0367(2) Uani d . 1 . . Cd Ni 0.5 -0.01073(3) 0.25 0.02530(17) Uani d . 1 . . Ni C1 0.6550(4) 0.07102(18) 0.2481(4) 0.0282(9) Uani d . 1 . . C N1 0.7525(3) 0.12053(17) 0.2469(4) 0.0371(9) Uani d . 1 . . N C2 0.6550(4) -0.09278(19) 0.2478(4) 0.0311(10) Uani d . 1 . . C N2 0.7485(4) -0.1440(2) 0.2471(4) 0.0455(11) Uani d . 1 . . N N4 0.9962(6) 0.0300(3) 0.4583(7) 0.0480(16) Uani d . 1 . . N N3 0.9982(4) 0.23658(17) -0.0019(4) 0.0381(9) Uani d . 1 . . N H31 0.921(4) 0.209(3) -0.036(7) 0.149(16) Uiso d . 1 . . H H32 1.081(4) 0.217(3) -0.046(7) 0.149(16) Uiso d . 1 . . H H33 0.987(7) 0.2854(14) -0.032(7) 0.149(16) Uiso d . 1 . . H loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 _atom_site_aniso_type_symbol Cd1 0.0283(6) 0.0237(3) 0.0221(3) 0 0.0006(3) 0 Cd Cd2 0.0253(3) 0.0415(4) 0.0434(4) 0 -0.0008(2) 0 Cd Ni 0.0195(3) 0.0215(3) 0.0350(3) 0 0.0007(2) 0 Ni C1 0.0249(14) 0.0247(15) 0.0350(17) 0.0026(12) -0.0009(13) -0.0001(12) C N1 0.0316(14) 0.0337(16) 0.0461(18) -0.0038(12) 0.0002(12) 0.0000(12) N C2 0.0272(17) 0.0325(17) 0.0337(18) -0.0003(13) 0.0004(13) -0.0006(12) C N2 0.0404(17) 0.045(2) 0.0507(19) 0.0115(15) 0.0001(14) 0.0012(15) N N4 0.050(3) 0.047(2) 0.047(3) -0.0017(19) 0.001(2) 0.0165(19) N N3 0.0392(17) 0.0393(15) 0.0358(16) 0.0007(12) 0.0003(13) 0.0026(12) N loop_ _atom_site_Fourier_wave_vector_seq_id _atom_site_Fourier_wave_vector_x _atom_site_Fourier_wave_vector_y _atom_site_Fourier_wave_vector_z 1 0.4365 0 0.1307 2 0.873 0 0.2614 3 1.3095 0 0.3921 loop_ _atom_site_occ_special_func_atom_site_label _atom_site_occ_special_func_crenel_c _atom_site_occ_special_func_crenel_w Cd1 0.25 0.4365 Cd2 0.75 0.5635 N4 0.7438(16) 0.5 loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Nix1 Ni x 1 Niy1 Ni y 1 Niz1 Ni z 1 Nix2 Ni x 2 Niy2 Ni y 2 Niz2 Ni z 2 C1x1 C1 x 1 C1y1 C1 y 1 C1z1 C1 z 1 C1x2 C1 x 2 C1y2 C1 y 2 C1z2 C1 z 2 N1x1 N1 x 1 N1y1 N1 y 1 N1z1 N1 z 1 N1x2 N1 x 2 N1y2 N1 y 2 N1z2 N1 z 2 C2x1 C2 x 1 C2y1 C2 y 1 C2z1 C2 z 1 C2x2 C2 x 2 C2y2 C2 y 2 C2z2 C2 z 2 C2x3 C2 x 3 C2y3 C2 y 3 C2z3 C2 z 3 N2x1 N2 x 1 N2y1 N2 y 1 N2z1 N2 z 1 N2x2 N2 x 2 N2y2 N2 y 2 N2z2 N2 z 2 N2x3 N2 x 3 N2y3 N2 y 3 N2z3 N2 z 3 N3x1 N3 x 1 N3y1 N3 y 1 N3z1 N3 z 1 N3x2 N3 x 2 N3y2 N3 y 2 N3z2 N3 z 2 N3x3 N3 x 3 N3y3 N3 y 3 N3z3 N3 z 3 H31x1 H31 x 1 H31y1 H31 y 1 H31z1 H31 z 1 H31x2 H31 x 2 H31y2 H31 y 2 H31z2 H31 z 2 H31x3 H31 x 3 H31y3 H31 y 3 H31z3 H31 z 3 H32x1 H32 x 1 H32y1 H32 y 1 H32z1 H32 z 1 H32x2 H32 x 2 H32y2 H32 y 2 H32z2 H32 z 2 H32x3 H32 x 3 H32y3 H32 y 3 H32z3 H32 z 3 H33x1 H33 x 1 H33y1 H33 y 1 H33z1 H33 z 1 H33x2 H33 x 2 H33y2 H33 y 2 H33z2 H33 z 2 H33x3 H33 x 3 H33y3 H33 y 3 H33z3 H33 z 3 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Nix1 0.0077(3) 0 Niy1 0 -0.0095(5) Niz1 -0.0006(5) 0 Nix2 0 -0.0073(2) Niy2 0.0009(9) 0 Niz2 0 -0.0002(3) C1x1 0.0081(14) 0.003(8) C1y1 0.0006(8) -0.0111(4) C1z1 -0.003(2) 0.0001(11) C1x2 0.0082(9) -0.0056(9) C1y2 0.0005(5) 0.001(5) C1z2 0.0004(14) -0.0019(14) N1x1 0.0085(11) 0.0087(10) N1y1 0.0033(6) -0.011(5) N1z1 -0.0064(16) -0.0004(13) N1x2 0.0133(10) 0.0001(7) N1y2 -0.001(5) -0.0003(4) N1z2 0.0004(14) -0.0037(10) C2x1 0.0173(5) 0.0025(5) C2y1 -0.0021(3) -0.0132(3) C2z1 0.0034(6) 0.0017(6) C2x2 -0.0013(8) 0.0021(9) C2y2 0.0029(4) -0.0008(4) C2z2 -0.0015(11) 0.0021(12) C2x3 0.0017(11) -0.0057(10) C2y3 0.0023(5) 0.002(5) C2z3 0.0029(14) 0.0006(13) N2x1 0.0135(5) -0.0085(5) N2y1 0.0008(3) -0.0206(3) N2z1 0.0006(6) 0.0017(6) N2x2 0.0059(7) 0.0012(8) N2y2 0.0047(4) 0.0002(5) N2z2 -0.0019(9) 0.0007(11) N2x3 0.0022(9) 0.0036(9) N2y3 0.0002(5) 0.0065(5) N2z3 0.0009(11) 0.0008(11) N3x1 0.0048(4) -0.0016(5) N3y1 0.0047(2) -0.0022(3) N3z1 -0.0151(5) -0.0309(5) N3x2 -0.0036(7) -0.0043(7) N3y2 0(4) 0.0003(4) N3z2 0.0007(9) -0.0026(8) N3x3 0(9) -0.0027(8) N3y3 0.0025(4) -0.0004(4) N3z3 -0.006(10) -0.007(10) H31x1 -0.002(4) 0.001(4) H31y1 0.013(3) -0.01(3) H31z1 -0.035(8) -0.017(7) H31x2 -0.002(2) -0.004(2) H31y2 -0.005(2) 0.002(2) H31z2 0.006(4) -0.008(4) H31x3 -0.0023(12) -0.0015(12) H31y3 0.0005(11) -0.001(10) H31z3 -0.0079(16) 0.0002(16) H32x1 0.001(3) 0.001(4) H32y1 0.003(3) -0.008(3) H32z1 -0.014(7) -0.018(7) H32x2 0.0004(16) -0.0053(16) H32y2 0.001(15) 0.0012(15) H32z2 0.002(2) -0.004(2) H32x3 0.0015(11) -0.0016(11) H32y3 0.0025(7) 0.0015(7) H32z3 -0.001(12) -0.0087(12) H33x1 0.022(7) 0(7) H33y1 0.0078(13) -0.0042(10) H33z1 0.001(9) -0.059(8) H33x2 -0.014(4) -0.005(4) H33y2 -0.0011(10) 0.0016(10) H33z2 -0.01(4) -0.001(4) H33x3 -0.002(19) -0.0029(19) H33y3 0.0029(7) -0.0014(6) H33z3 -0.0082(18) -0.007(18) loop_ _jana_atom_site_displace_Legendre_atom_site_label _jana_atom_site_displace_Legendre_axis _jana_atom_site_displace_Legendre_param_order _jana_atom_site_displace_Legendre_param_coeff Cd1 x 1 -0.01989(18) Cd1 y 1 0 Cd1 z 1 0.015(2) Cd1 x 2 0 Cd1 y 2 0.0011(2) Cd1 z 2 0 Cd1 x 3 0.0094(8) Cd1 y 3 0 Cd1 z 3 0.0073(8) Cd1 x 4 0 Cd1 y 4 0.0017(7) Cd1 z 4 0 Cd2 x 1 0.02793(17) Cd2 y 1 0 Cd2 z 1 -0.0246(2) Cd2 x 2 0 Cd2 y 2 0.00773(18) Cd2 z 2 0 Cd2 x 3 0.0047(4) Cd2 y 3 0 Cd2 z 3 -0.0124(5) Cd2 x 4 0 Cd2 y 4 -0.0035(3) Cd2 z 4 0 N4 x 1 0.0085(12) N4 y 1 -0.001(6) N4 z 1 0.0042(13) N4 x 2 -0.007(2) N4 y 2 -0.0031(11) N4 z 2 -0.007(3) loop_ _atom_site_displace_special_func_atom_site_label _atom_site_displace_special_func_sawtooth_ax _atom_site_displace_special_func_sawtooth_ay _atom_site_displace_special_func_sawtooth_az _atom_site_displace_special_func_sawtooth_c _atom_site_displace_special_func_sawtooth_w Ni 0.0352(4) 0 0.0078(8) 0.75 1 C1 0.051(2) -0.0031(13) 0.008(3) 0.81745(17) 1 N1 0.056(2) -0.0072(11) 0.01(3) 0.86005(16) 1 loop_ _atom_site_U_Fourier_id _atom_site_U_Fourier_atom_site_label _atom_site_U_Fourier_tens_elem _atom_site_U_Fourier_wave_vector_seq_id NiU111 Ni U11 1 NiU221 Ni U22 1 NiU331 Ni U33 1 NiU121 Ni U12 1 NiU131 Ni U13 1 NiU231 Ni U23 1 loop_ _atom_site_U_Fourier_param_id _atom_site_U_Fourier_param_cos _atom_site_U_Fourier_param_sin NiU111 0 -0.0029(6) NiU221 0 -0.0008(4) NiU331 0 -0.0001(5) NiU121 -0.0022(3) 0 NiU131 0 -0.0004(5) NiU231 0.0017(3) 0 loop_ _jana_atom_site_U_Legendre_atom_site_label _jana_atom_site_U_Legendre_tens_elem _jana_atom_site_U_Legendre_param_order _jana_atom_site_U_Legendre_param_coeff Cd1 U11 1 0 Cd1 U22 1 0 Cd1 U33 1 0 Cd1 U12 1 0.005(7) Cd1 U13 1 0 Cd1 U23 1 -0.0051(7) Cd1 U11 2 -0.002(2) Cd1 U22 2 -0.0058(16) Cd1 U33 2 -0.0069(18) Cd1 U12 2 0 Cd1 U13 2 -0.006(16) Cd1 U23 2 0 Cd1 U11 3 0 Cd1 U22 3 0 Cd1 U33 3 0 Cd1 U12 3 0.015(2) Cd1 U13 3 0 Cd1 U23 3 -0.012(2) Cd1 U11 4 0.057(5) Cd1 U22 4 -0.013(5) Cd1 U33 4 0.006(6) Cd1 U12 4 0 Cd1 U13 4 -0.002(4) Cd1 U23 4 0 Cd2 U11 1 0 Cd2 U22 1 0 Cd2 U33 1 0 Cd2 U12 1 0.0059(6) Cd2 U13 1 0 Cd2 U23 1 -0.0337(9) Cd2 U11 2 0.0033(12) Cd2 U22 2 0.0242(16) Cd2 U33 2 0.0299(16) Cd2 U12 2 0 Cd2 U13 2 -0.0017(11) Cd2 U23 2 0 Cd2 U11 3 0 Cd2 U22 3 0 Cd2 U33 3 0 Cd2 U12 3 0.0041(12) Cd2 U13 3 0 Cd2 U23 3 -0.018(16) Cd2 U11 4 0.008(3) Cd2 U22 4 -0.052(4) Cd2 U33 4 -0.011(3) Cd2 U12 4 0 Cd2 U13 4 0.006(2) Cd2 U23 4 0 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 2 0 0 0 51546.3 51223.7 319.19 o 4 0 0 0 57302.5 54244.8 452.78 o 4 0 0 2 101.85 137.76 18.94 o 6 0 0 0 17747.5 15216.1 311.37 o 6 0 0 2 200.98 212.11 24.81 o 8 0 0 0 6111.62 5680.46 238.62 o 8 0 0 2 155.38 164.8 30.24 o 10 0 0 0 1119.96 1261.56 45.18 o 1 1 0 0 1004.51 864.46 25.61 o 1 1 0 1 1008.35 1030.51 26.24 o 3 1 0 -1 955.83 984.44 24.46 o 3 1 0 0 2341.44 2620.87 72.66 o 3 1 0 1 684.18 685.7 18.32 o 5 1 0 -2 38.56 40.47 12.63 o 5 1 0 -1 380.74 398.17 14.59 o 5 1 0 1 1551.76 1598.9 41.53 o 7 1 0 -1 992.91 945.75 28.28 o 7 1 0 1 680.11 663.29 22.86 o 9 1 0 -1 470.84 408.22 23.3 o 9 1 0 0 189.45 166.84 22.06 o 9 1 0 1 518.43 441.04 25.44 o 11 1 0 -1 490.15 470.92 28.64 o 0 2 0 0 37.76 314.66 11.38 o 0 2 0 1 938.08 779.97 20.28 o 2 2 0 -3 84.45 53.72 8.72 o 2 2 0 -1 1505.71 1597.65 44.74 o 2 2 0 0 609.55 553.36 14.67 o 2 2 0 1 421.79 451.35 13.79 o 4 2 0 -3 219.76 228.03 12.36 o 4 2 0 -1 2221.37 2330.04 62.08 o 4 2 0 0 741.93 857.88 23.21 o 6 2 0 -1 1236.33 1274.1 34.06 o 8 2 0 -1 1299.29 1335.11 38.6 o 8 2 0 0 224.97 194.06 20.28 o 8 2 0 1 77.51 85.65 19.83 o 10 2 0 -1 350.63 348.27 24.99 o 10 2 0 1 127.73 86.62 25.35 o 1 3 0 -3 186.06 72.75 9.69 o 1 3 0 -1 2657.41 2479.9 55.5 o 1 3 0 0 55383.6 55185.9 218.43 o 1 3 0 1 1949.88 1998.22 54.87 o 1 3 0 3 132.01 87.87 11.74 o 3 3 0 -1 3686.73 3467.81 80.31 o 3 3 0 0 34324.6 32838.5 229.72 o 3 3 0 1 1590.69 1628.78 39.58 o 3 3 0 2 55.8 40.47 11.92 o 5 3 0 -3 207.93 195.75 13.16 o 5 3 0 -1 1176.28 1134.65 31.22 o 5 3 0 0 14377.5 13370 187.03 o 5 3 0 1 485.95 497.33 17.43 o 7 3 0 -3 79.82 85.91 15.03 o 7 3 0 -1 722.43 707.93 20.81 o 7 3 0 0 5297.82 5307.64 151.28 o 7 3 0 1 335.25 373.36 20.19 o 7 3 0 2 118.9 91.96 19.21 o 9 3 0 -3 88.9 82.44 18.68 o 9 3 0 -1 281.47 237.1 22.41 o 9 3 0 0 1318.97 1325.42 39.84 o 11 3 0 -1 186.07 199.75 27.3 o 0 4 0 1 822.9 859.57 22.32 o 0 4 0 2 165.96 88.76 10.58 o 2 4 0 -1 2055.86 2058.17 56.74 o 2 4 0 0 24145.2 26486.3 189.79 o 2 4 0 1 5942.05 5843.3 100.5 o 2 4 0 2 132.66 120.33 12.18 o 4 4 0 -3 151.19 208.56 12.27 o 4 4 0 0 897.17 1016.45 29.17 o 4 4 0 1 2293.52 2195.4 63.14 o 4 4 0 2 227.61 211.85 14.94 o 6 4 0 -3 52.51 83.51 14.14 o 6 4 0 -2 223.24 227.86 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