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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_(BaMnF4_10K) _audit_creation_method 'Jana2006 Version : 31/03/2009' _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ? _journal_techeditor_code ? _journal_paper_category ? _journal_techeditor_notes ? _journal_coden_ASTM ? _journal_name_full 'Acta Crystallographica Section B' _journal_year 2009 _journal_volume 65 _journal_issue ? _journal_page_first 576 _journal_page_last 586 _journal_paper_doi https://doi.org/10.1107/s0108768109027177 _journal_suppl_publ_number ? _journal_suppl_publ_pages ? _publ_contact_author_name 'Posse, Jose Maria' _publ_contact_author_address ;Departamento Fisica Materia Condensada Universidad del Pais Vasco Apdo. 644 48080 Bilbao Spain ; _publ_contact_author_email josemaria@wm.lc.ehu.es _publ_contact_author_fax '+34 946013500' _publ_contact_author_phone '+34 94 6015481' _publ_requested_journal 'Acta Crystallographica Section B' _publ_requested_category ? _publ_contact_letter ? _publ_section_title 'Ternary fluorides BaMF~4~ (M=Zn, Mg and Mn) at low temperatures' loop_ _publ_author_name _publ_author_address 'Posse, Jose Maria' ;Departamento Fisica Materia Condensada Universidad del Pais Vasco Apdo. 644 48080 Bilbao Spain ; 'Grzechnik, Andrzej' ;Departamento Fisica Materia Condensada Universidad del Pais Vasco Apdo. 644 48080 Bilbao Spain ; 'Friese, Karen' ;Departamento Fisica Materia Condensada Universidad del Pais Vasco Apdo. 644 48080 Bilbao Spain ; _publ_section_references ; Petricek, V., Dusek, M. &; Palatinus L. (2006). Jana2006. Structure Determination Software Programs. Institute of Physics, Praha, Czech Republic. CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.15 (release 10-01-2008 CrysAlis171 .NET) CrysAlis CCD, Oxford Diffraction Ltd., Version 1.171.32.15 (release 10-01-2008 CrysAlis171 .NET) ; _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Ba1 F4 Mn1' _chemical_formula_weight 268.3 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration ? _space_group_crystal_system monoclinic _space_group_ssg_name X21(1/21/2\g)0 loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,-x2,x3+1/2,-x1-x2+x4 3 x1+1/2,x2+1/2,x3,x4+1/2 4 -x1+1/2,-x2+1/2,x3+1/2,-x1-x2+x4+1/2 _cell_length_a 4.198368(14) _cell_length_b 15.05560(10) _cell_length_c 6.00025(2) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90.0853(2) _cell_volume 379.269(3) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.50000 0.50000 0.39487 _cell_formula_units_Z 4 _cell_measurement_reflns_used 3614 _cell_measurement_theta_min 2.6751 _cell_measurement_theta_max 36.7821 _cell_measurement_temperature 10 _cell_special_details ? _exptl_crystal_type_of_structure mod _exptl_crystal_density_diffrn 4.69670 #(3) _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 468 _exptl_crystal_description irregular _exptl_crystal_colour colourless _exptl_crystal_size_max 0.1826 _exptl_crystal_size_mid 0.1350 _exptl_crystal_size_min 0.1241 _exptl_absorpt_coefficient_mu 13.406 _exptl_absorpt_correction_T_min 0.218 _exptl_absorpt_correction_T_max 0.338 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.32.15 (release 10-01-2008 CrysAlis171 .NET) (compiled Jan 10 2008,16:37:18) Numerical absorption correction based on gaussian integration over a multifaceted crystal model ; _exptl_special_details 'Low temperature measurement; Helijet Oxford diffraction' _diffrn_ambient_temperature 10 _diffrn_radiation_type 'Mo K\a' _diffrn_source 'X-ray tube' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-cycle diffractometer' _diffrn_measurement_device_type 'Oxford Diffraction CCD' _diffrn_detector_area_resol_mean 8.3504 _diffrn_measurement_method '\w and \f scans' _diffrn_reflns_number 19876 _diffrn_reflns_theta_min 2.68 _diffrn_reflns_theta_max 36.78 _diffrn_reflns_theta_full 18.01 _diffrn_measured_fraction_theta_max ? _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0407 _diffrn_reflns_av_unetI/netI 0.034 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_h_max 3 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_index_m_1_min -2 _diffrn_reflns_limit_index_m_1_max 2 _diffrn_reflns_reduction_process Poisson _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? _reflns_odcompleteness_completeness 88.85 _reflns_odcompleteness_theta 26.32 _reflns_odcompleteness_iscentric ? _refine_special_details ; Refined in four dimensional space, non-standard setting Twinned crystal: Twin matrix (1 0 0, 0 -1 0, 0 0 1) Crenel function for Ba-atom Inversion twinning tested---Flack parameter 0 ; _reflns_number_total 6397 _reflns_number_gt 5653 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef F _refine_ls_R_factor_gt 0.0416 _refine_ls_wR_factor_gt 0.0488 _refine_ls_R_factor_all 0.0485 _refine_ls_wR_factor_ref 0.0496 _refine_ls_goodness_of_fit_ref 1.76 _refine_ls_goodness_of_fit_gt 1.84 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 6397 _refine_ls_number_parameters 89 _refine_ls_number_restraints ? _refine_ls_number_constraints 4 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(F)+0.0001F^2^) _refine_ls_shift/su_max 0.0134 _refine_ls_shift/su_mean 0.0035 _refine_diff_density_max 5.19 _refine_diff_density_min -5.71 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 20(17) _refine_ls_abs_structure_details 'Inversion twin tested' _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ba -0.324 2.282 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Mn 0.337 0.728 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' F 0.017 0.010 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection 'CRYSALIS CCD' _computing_cell_refinement Jana2006 _computing_data_reduction ; CRYSALIS RED Jana2006 (Petricek, Dusek & Palatinus, 2006) ; _computing_structure_solution ? _computing_structure_refinement 'Jana2006 (Petricek, Dusek & Palatinus, 2006)' _computing_molecular_graphics ? _computing_publication_material '-2 9 9 -1 19.95 18.49 1.43 o' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Ba1 Ba 0.5036(5) 0.33738(4) 0.44756(15) Uani 0.00334(6) 4 0.644(3) d ? ? ? Ba2 Ba 0.5036(5) 0.3538(2) 0.48008(18) Uani 0.00334(6) 4 0.356(3) d ? ? ? Mn Mn 0.0037(5) 0.41624(5) 0 Uiso 0.00329(13) 4 1 d ? ? ? F1 F -0.0002(11) 0.33707(18) 0.7195(5) Uiso 0.0071(6) 4 1 d ? ? ? F2 F -0.0012(9) 0.2997(2) 0.1958(4) Uiso 0.0057(5) 4 1 d ? ? ? F3 F -0.0042(7) 0.4639(2) 0.3368(4) Uiso 0.0078(5) 4 1 d ? ? ? F4 F 0.5021(9) 0.42167(18) 0.0197(4) Uiso 0.0071(5) 4 1 d ? ? ? loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ba1 Ba 0.00274(12) 0.00334(12) 0.00395(9) 0.00047(13) 0.00036(15) 0.00085(9) Ba2 Ba 0.00274(12) 0.00334(12) 0.00395(9) 0.00047(13) 0.00036(15) 0.00085(9) loop_ _atom_site_Fourier_wave_vector_seq_id _atom_site_Fourier_wave_vector_x _atom_site_Fourier_wave_vector_y _atom_site_Fourier_wave_vector_z 1 0.50000 0.50000 0.39487 2 1.00000 1.00000 0.78974 loop_ _atom_site_occ_special_func_atom_site_label _atom_site_occ_special_func_crenel_c _atom_site_occ_special_func_crenel_w Ba1 0.4311(11) 0.644(3) Ba2 0.9524(11) 0.356(3) loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Ba1x1 Ba1 x 1 Ba1y1 Ba1 y 1 Ba1z1 Ba1 z 1 Ba1x2 Ba1 x 2 Ba1y2 Ba1 y 2 Ba1z2 Ba1 z 2 Ba2x1 Ba2 x 1 Ba2y1 Ba2 y 1 Ba2z1 Ba2 z 1 Ba2x2 Ba2 x 2 Ba2y2 Ba2 y 2 Ba2z2 Ba2 z 2 Mnx1 Mn x 1 Mny1 Mn y 1 Mnz1 Mn z 1 Mnx2 Mn x 2 Mny2 Mn y 2 Mnz2 Mn z 2 F1x1 F1 x 1 F1y1 F1 y 1 F1z1 F1 z 1 F1x2 F1 x 2 F1y2 F1 y 2 F1z2 F1 z 2 F2x1 F2 x 1 F2y1 F2 y 1 F2z1 F2 z 1 F2x2 F2 x 2 F2y2 F2 y 2 F2z2 F2 z 2 F3x1 F3 x 1 F3y1 F3 y 1 F3z1 F3 z 1 F3x2 F3 x 2 F3y2 F3 y 2 F3z2 F3 z 2 F4x1 F4 x 1 F4y1 F4 y 1 F4z1 F4 z 1 F4x2 F4 x 2 F4y2 F4 y 2 F4z2 F4 z 2 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Ba1x1 0.0056(6) -0.0044(5) Ba1y1 0 -0.00091(9) Ba1z1 0.01414(18) -0.00612(17) Ba1x2 0 -0.0112(6) Ba1y2 -0.00380(7) 0 Ba1z2 0 0 Ba2x1 0 0 Ba2y1 0 -0.0123(3) Ba2z1 0 0.0316(14) Ba2x2 -0.0088(7) 0.0071(7) Ba2y2 0.0059(3) 0 Ba2z2 0 -0.0271(10) Mnx1 -0.0078(2) 0.00296(18) Mny1 0 0.00121(5) Mnz1 0.00298(11) 0 Mnx2 0 0 Mny2 0.00068(11) -0.00443(7) Mnz2 0.00418(13) 0 F1x1 -0.0121(8) 0.0260(7) F1y1 -0.0081(2) -0.0054(2) F1z1 0.0097(4) 0.0047(5) F1x2 0 0 F1y2 -0.0018(2) 0.0046(2) F1z2 -0.0054(5) -0.0080(5) F2x1 -0.0417(8) -0.0225(8) F2y1 0 0.0031(2) F2z1 0 0.0047(5) F2x2 0 0 F2y2 0.0024(2) -0.0034(2) F2z2 0.0093(5) 0.0039(5) F3x1 0.0470(8) 0.0341(8) F3y1 -0.0034(2) 0 F3z1 0.0074(5) 0.0053(5) F3x2 0 0 F3y2 0.0045(2) 0.0035(2) F3z2 -0.0055(5) 0 F4x1 0.0024(7) 0 F4y1 0.0120(3) -0.0217(3) F4z1 -0.0133(6) -0.0344(5) F4x2 0 0 F4y2 0 0.0048(3) F4z2 0 -0.0039(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance_av _geom_bond_distance_min _geom_bond_distance_max _geom_bond_publ_flag Ba1 F1 ? ? 2.640(7) 2.555(7) 2.697(7) yes Ba1 F1 ? 1_655 2.643(7) 2.584(7) 2.690(7) yes Ba1 F1 ? 4_554 2.863(7) 2.789(7) 3.027(8) yes Ba1 F2 ? ? 2.701(6) 2.643(7) 2.738(6) yes Ba1 F2 ? 1_655 2.711(6) 2.621(7) 2.804(7) yes Ba1 F2 ? 4_555 2.614(6) 2.561(7) 2.659(5) yes Ba1 F3 ? ? 2.844(6) 2.752(7) 3.166(7) yes Ba1 F3 ? 1_655 2.842(6) 2.752(6) 3.003(7) yes Ba1 F4 ? ? 2.832(6) 2.670(6) 3.051(5) yes Ba1 F4 ? 1_556 3.839(6) 3.450(7) 4.079(4) yes Ba1 F4 ? 2_665 3.738(7) 3.288(7) 4.050(9) yes Ba2 F1 ? ? 2.649(8) 2.580(9) 2.727(7) yes Ba2 F1 ? 1_655 2.673(8) 2.550(9) 2.723(7) yes Ba2 F1 ? 4_554 3.478(9) 3.203(10) 3.632(8) yes Ba2 F2 ? ? 2.725(7) 2.705(6) 2.802(9) yes Ba2 F2 ? 1_655 2.700(7) 2.657(8) 2.731(8) yes Ba2 F2 ? 4_555 2.656(9) 2.586(8) 2.783(10) yes Ba2 F3 ? ? 2.916(7) 2.812(6) 3.041(8) yes Ba2 F3 ? 1_655 2.853(7) 2.776(6) 2.925(7) yes Ba2 F4 ? ? 2.887(9) 2.690(12) 3.099(11) yes Ba2 F4 ? 1_556 3.167(9) 3.043(7) 3.423(10) yes Ba2 F4 ? 2_665 3.181(9) 3.005(10) 3.676(8) yes Mn Mn ? 1_455 4.199(3) 4.129(3) 4.268(3) yes Mn Mn ? 1_655 4.198(3) 4.129(3) 4.268(3) yes Mn Mn ? 2_564 3.9199(19) 3.903(2) 3.935(2) yes Mn Mn ? 2_565 3.9201(19) 3.903(2) 3.935(2) yes Mn F1 ? 1_554 2.068(7) 2.021(7) 2.104(7) yes Mn F2 ? ? 2.116(6) 2.099(7) 2.137(5) yes Mn F3 ? ? 2.154(5) 2.119(6) 2.181(6) yes Mn F3 ? 2_564 2.062(6) 2.037(7) 2.087(6) yes Mn F4 ? 1_455 2.132(5) 2.111(5) 2.159(4) yes Mn F4 ? ? 2.121(5) 2.080(5) 2.146(4) yes F1 F2 ? ? 3.201(9) 3.102(8) 3.310(9) yes F1 F2 ? 1_556 2.918(9) 2.841(9) 3.022(9) yes F1 F2 ? 4_455 2.947(9) 2.843(9) 3.030(8) yes F1 F2 ? 4_555 2.956(9) 2.881(9) 3.034(8) yes F1 F3 ? ? 2.989(9) 2.902(9) 3.063(10) yes F1 F3 ? 2_565 3.087(10) 2.978(9) 3.223(9) yes F1 F4 ? 1_456 3.060(8) 2.876(7) 3.249(9) yes F1 F4 ? 1_556 3.064(8) 2.879(7) 3.248(8) yes F2 F3 ? ? 2.631(8) 2.586(8) 2.657(8) yes F2 F4 ? 1_455 2.994(8) 2.927(8) 3.035(8) yes F2 F4 ? ? 3.009(8) 2.894(8) 3.103(8) yes F2 F4 ? 4_555 3.866(9) 3.460(8) 4.312(8) yes F3 F3 ? 2_564 3.198(8) 3.106(7) 3.309(9) yes F3 F3 ? 2_565 3.198(8) 3.106(7) 3.309(9) yes F3 F4 ? 1_455 2.904(7) 2.835(6) 2.960(7) yes F3 F4 ? ? 2.946(7) 2.890(7) 3.042(7) yes F3 F4 ? 2_565 2.943(8) 2.915(8) 2.969(8) yes F3 F4 ? 2_665 2.958(8) 2.902(8) 3.002(9) yes F4 F4 ? 2_664 3.831(9) 3.306(7) 4.412(7) yes F4 F4 ? 2_665 3.826(9) 3.306(7) 4.412(7) yes loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_av _geom_angle_min _geom_angle_max _geom_angle_publ_flag F1 Ba1 F1 ? ? 1_655 101.8(2) 96.1(2) 108.2(2) yes F1 Ba1 F1 ? ? 4_554 105.9(2) 105.2(2) 106.7(2) yes F1 Ba1 F2 ? ? ? 73.5(2) 71.8(2) 76.5(2) yes F1 Ba1 F2 ? ? 1_655 165.5(2) 163.9(2) 168.6(2) yes F1 Ba1 F2 ? ? 4_555 68.2(2) 66.9(2) 70.2(2) yes F1 Ba1 F3 ? ? ? 65.83(19) 59.61(18) 68.78(18) yes F1 Ba1 F3 ? ? 1_655 134.05(19) 130.62(19) 138.49(18) yes F1 Ba1 F4 ? ? ? 126.1(2) 117.3(2) 129.1(2) yes F1 Ba1 F4 ? ? 1_556 54.19(16) 52.26(16) 57.03(16) yes F1 Ba1 F4 ? ? 2_665 85.45(19) 80.83(19) 91.87(19) yes F1 Ba1 F1 1_655 ? 4_554 106.6(2) 103.9(2) 110.3(2) yes F1 Ba1 F2 1_655 ? ? 166.2(2) 163.6(2) 170.8(2) yes F1 Ba1 F2 1_655 ? 1_655 73.6(2) 72.2(2) 75.5(2) yes F1 Ba1 F2 1_655 ? 4_555 67.4(2) 65.6(2) 70.5(2) yes F1 Ba1 F3 1_655 ? ? 133.09(19) 127.43(19) 141.07(19) yes F1 Ba1 F3 1_655 ? 1_655 65.97(19) 62.8(2) 67.67(19) yes F1 Ba1 F4 1_655 ? ? 125.0(2) 118.4(2) 129.2(2) yes F1 Ba1 F4 1_655 ? 1_556 54.03(16) 51.44(16) 57.67(16) yes F1 Ba1 F4 1_655 ? 2_665 84.60(19) 82.21(19) 88.10(19) yes F1 Ba1 F2 4_554 ? ? 64.41(19) 60.65(19) 66.58(19) yes F1 Ba1 F2 4_554 ? 1_655 64.06(19) 60.19(19) 66.34(19) yes F1 Ba1 F2 4_554 ? 4_555 63.3(2) 62.2(2) 64.7(2) yes F1 Ba1 F3 4_554 ? ? 120.06(18) 113.70(16) 122.82(17) yes F1 Ba1 F3 4_554 ? 1_655 119.96(18) 115.98(19) 122.7(2) yes F1 Ba1 F4 4_554 ? ? 86.2(2) 81.9(2) 91.6(2) yes F1 Ba1 F4 4_554 ? 1_556 137.58(19) 131.3(2) 140.67(19) yes F1 Ba1 F4 4_554 ? 2_665 161.29(18) 154.92(17) 165.21(19) yes F2 Ba1 F2 ? ? 1_655 108.09(18) 99.00(19) 115.09(17) yes F2 Ba1 F2 ? ? 4_555 100.0(2) 95.78(19) 103.1(2) yes F2 Ba1 F3 ? ? ? 56.31(17) 53.23(15) 58.28(18) yes F2 Ba1 F3 ? ? 1_655 125.68(16) 122.38(17) 128.53(16) yes F2 Ba1 F4 ? ? ? 65.37(16) 65.08(16) 65.70(15) yes F2 Ba1 F4 ? ? 1_556 125.91(17) 121.53(16) 131.6(2) yes F2 Ba1 F4 ? ? 2_665 106.34(17) 104.39(15) 108.8(2) yes F2 Ba1 F2 1_655 ? 4_555 98.0(2) 96.3(2) 102.9(2) yes F2 Ba1 F3 1_655 ? ? 126.86(16) 122.94(17) 129.86(15) yes F2 Ba1 F3 1_655 ? 1_655 56.78(17) 55.30(18) 58.46(17) yes F2 Ba1 F4 1_655 ? ? 65.01(16) 63.84(17) 66.30(17) yes F2 Ba1 F4 1_655 ? 1_556 125.88(17) 123.32(16) 130.60(16) yes F2 Ba1 F4 1_655 ? 2_665 106.79(17) 103.33(19) 110.42(17) yes F2 Ba1 F3 4_555 ? ? 132.6(2) 125.50(17) 137.56(19) yes F2 Ba1 F3 4_555 ? 1_655 131.6(2) 129.4(2) 134.36(17) yes F2 Ba1 F4 4_555 ? ? 149.4(2) 146.0(2) 154.2(2) yes F2 Ba1 F4 4_555 ? 1_556 74.33(17) 68.91(17) 77.44(17) yes F2 Ba1 F4 4_555 ? 2_665 135.23(16) 132.41(16) 142.40(15) yes F3 Ba1 F3 ? ? 1_655 90.04(15) 84.26(16) 96.89(16) yes F3 Ba1 F4 ? ? ? 63.08(16) 58.23(16) 66.72(19) yes F3 Ba1 F4 ? ? 1_556 87.92(15) 83.63(16) 94.65(15) yes F3 Ba1 F4 ? ? 2_665 50.78(13) 47.66(13) 54.95(15) yes F3 Ba1 F4 1_655 ? ? 61.74(16) 56.90(14) 65.13(19) yes F3 Ba1 F4 1_655 ? 1_556 88.37(15) 84.89(16) 94.02(15) yes F3 Ba1 F4 1_655 ? 2_665 50.59(14) 46.84(14) 56.03(15) yes F4 Ba1 F4 ? ? 1_556 136.14(19) 128.3(2) 139.4(2) yes F4 Ba1 F4 ? ? 2_665 75.12(17) 63.41(14) 80.9(2) yes F4 Ba1 F4 1_556 ? 2_665 61.02(15) 55.03(16) 73.20(17) yes F1 Ba2 F1 ? ? 1_655 111.2(3) 108.4(4) 113.2(4) yes F1 Ba2 F1 ? ? 4_554 99.6(2) 98.7(2) 101.3(2) yes F1 Ba2 F2 ? ? ? 73.3(2) 70.9(2) 74.3(2) yes F1 Ba2 F2 ? ? 1_655 154.1(3) 151.2(3) 158.4(3) yes F1 Ba2 F2 ? ? 4_555 68.1(2) 66.1(3) 69.8(3) yes F1 Ba2 F3 ? ? ? 64.86(19) 61.77(19) 66.79(19) yes F1 Ba2 F3 ? ? 1_655 149.7(3) 144.9(3) 152.8(3) yes F1 Ba2 F4 ? ? ? 123.0(2) 120.6(3) 125.2(2) yes F1 Ba2 F4 ? ? 1_556 59.6(2) 57.6(2) 61.5(2) yes F1 Ba2 F4 ? ? 2_665 93.9(2) 86.5(3) 97.3(2) yes F1 Ba2 F1 1_655 ? 4_554 97.7(2) 95.8(2) 102.6(2) yes F1 Ba2 F2 1_655 ? ? 152.0(3) 148.5(3) 161.1(3) yes F1 Ba2 F2 1_655 ? 1_655 73.0(2) 71.9(2) 74.8(2) yes F1 Ba2 F2 1_655 ? 4_555 68.6(2) 67.4(3) 70.5(3) yes F1 Ba2 F3 1_655 ? ? 151.8(3) 143.0(3) 155.3(3) yes F1 Ba2 F3 1_655 ? 1_655 65.44(19) 64.70(19) 67.4(2) yes F1 Ba2 F4 1_655 ? ? 123.7(2) 121.0(3) 128.3(3) yes F1 Ba2 F4 1_655 ? 1_556 59.6(2) 58.21(18) 61.0(3) yes F1 Ba2 F4 1_655 ? 2_665 96.1(2) 92.2(2) 97.9(2) yes F1 Ba2 F2 4_554 ? ? 54.8(2) 52.97(18) 58.5(2) yes F1 Ba2 F2 4_554 ? 1_655 54.8(2) 52.81(18) 58.3(2) yes F1 Ba2 F2 4_554 ? 4_555 56.3(2) 54.7(2) 59.3(2) yes F1 Ba2 F3 4_554 ? ? 110.4(2) 108.5(2) 113.9(3) yes F1 Ba2 F3 4_554 ? 1_655 110.6(2) 108.05(17) 115.1(3) yes F1 Ba2 F4 4_554 ? ? 87.5(3) 86.4(3) 88.6(2) yes F1 Ba2 F4 4_554 ? 1_556 131.7(3) 128.2(2) 135.3(3) yes F1 Ba2 F4 4_554 ? 2_665 155.6(3) 152.0(4) 163.8(4) yes F2 Ba2 F2 ? ? 1_655 91.4(3) 89.01(19) 96.6(3) yes F2 Ba2 F2 ? ? 4_555 89.3(2) 86.9(2) 96.4(2) yes F2 Ba2 F3 ? ? ? 55.84(17) 54.49(17) 56.88(16) yes F2 Ba2 F3 ? ? 1_655 124.6(3) 120.3(4) 128.8(4) yes F2 Ba2 F4 ? ? ? 65.5(2) 63.2(3) 66.31(17) yes F2 Ba2 F4 ? ? 1_556 132.9(2) 129.6(2) 134.7(2) yes F2 Ba2 F4 ? ? 2_665 111.2(2) 105.4(2) 112.7(3) yes F2 Ba2 F2 1_655 ? 4_555 91.5(2) 88.5(2) 95.4(3) yes F2 Ba2 F3 1_655 ? ? 123.5(3) 120.6(4) 126.9(4) yes F2 Ba2 F3 1_655 ? 1_655 55.97(17) 55.07(16) 56.89(18) yes F2 Ba2 F4 1_655 ? ? 65.0(2) 62.9(3) 66.7(3) yes F2 Ba2 F4 1_655 ? 1_556 132.3(2) 131.44(18) 133.5(3) yes F2 Ba2 F4 1_655 ? 2_665 111.3(2) 105.7(2) 116.2(3) yes F2 Ba2 F3 4_555 ? ? 127.3(2) 123.3(2) 133.3(2) yes F2 Ba2 F3 4_555 ? 1_655 129.4(2) 127.0(2) 132.4(2) yes F2 Ba2 F4 4_555 ? ? 143.7(3) 141.4(3) 147.0(4) yes F2 Ba2 F4 4_555 ? 1_556 75.5(3) 71.6(3) 78.6(3) yes F2 Ba2 F4 4_555 ? 2_665 148.0(3) 137.7(4) 151.5(2) yes F3 Ba2 F3 ? ? 1_655 103.1(2) 93.8(2) 105.7(2) yes F3 Ba2 F4 ? ? ? 59.88(18) 58.00(19) 60.9(2) yes F3 Ba2 F4 ? ? 1_556 99.3(2) 94.2(3) 101.7(2) yes F3 Ba2 F4 ? ? 2_665 57.78(16) 52.44(15) 59.29(15) yes F3 Ba2 F4 1_655 ? ? 60.47(19) 57.2(2) 63.5(2) yes F3 Ba2 F4 1_655 ? 1_556 97.9(2) 93.9(3) 99.6(2) yes F3 Ba2 F4 1_655 ? 2_665 58.12(16) 51.75(15) 60.7(2) yes F4 Ba2 F4 ? ? 1_556 140.7(3) 137.1(3) 143.5(3) yes F4 Ba2 F4 ? ? 2_665 68.2(2) 64.31(18) 75.8(3) yes F4 Ba2 F4 1_556 ? 2_665 72.6(2) 61.6(2) 77.88(19) yes Mn Mn Mn 1_455 ? 1_655 179.02(5) 179.01(8) 179.02(4) yes Mn Mn Mn 1_455 ? 2_564 89.48(5) 89.15(5) 89.82(5) yes Mn Mn Mn 1_455 ? 2_565 89.50(5) 88.41(5) 90.57(5) yes Mn Mn Mn 1_655 ? 2_564 90.52(5) 89.48(5) 91.55(5) yes Mn Mn Mn 1_655 ? 2_565 90.51(5) 90.38(5) 90.63(5) yes Mn Mn Mn 2_564 ? 2_565 99.89(5) 98.82(5) 100.92(5) yes F1 Mn F2 1_554 ? ? 88.4(3) 85.0(3) 93.7(3) yes F1 Mn F3 1_554 ? ? 163.9(3) 160.6(2) 170.0(3) yes F1 Mn F3 1_554 ? 2_564 96.8(2) 93.1(2) 101.7(2) yes F1 Mn F4 1_554 ? 1_455 93.7(3) 85.7(3) 100.1(3) yes F1 Mn F4 1_554 ? ? 94.1(3) 85.7(3) 101.6(3) yes F2 Mn F3 ? ? ? 76.0(2) 74.21(19) 77.46(18) yes F2 Mn F3 ? ? 2_564 174.4(2) 172.4(2) 177.71(19) yes F2 Mn F4 ? ? 1_455 89.6(3) 87.0(3) 91.8(3) yes F2 Mn F4 ? ? ? 90.5(3) 87.4(3) 93.8(3) yes F3 Mn F3 ? ? 2_564 98.7(2) 95.9(2) 103.14(19) yes F3 Mn F4 ? ? 1_455 85.3(2) 83.0(2) 86.9(2) yes F3 Mn F4 ? ? ? 87.1(2) 84.2(2) 89.5(2) yes F3 Mn F4 2_564 ? 1_455 89.7(3) 88.2(3) 90.5(3) yes F3 Mn F4 2_564 ? ? 89.4(3) 88.7(3) 90.3(3) yes F4 Mn F4 1_455 ? ? 172.1(3) 169.7(3) 174.5(2) yes F2 F1 F2 ? ? 1_556 158.4(3) 150.9(3) 162.9(3) yes F2 F1 F2 ? ? 4_455 79.9(2) 74.1(2) 83.6(2) yes F2 F1 F2 ? ? 4_555 80.2(2) 73.0(2) 84.6(2) yes F2 F1 F3 ? ? ? 50.16(17) 48.89(18) 52.11(17) yes F2 F1 F3 ? ? 2_565 113.1(3) 109.1(2) 120.3(3) yes F2 F1 F4 ? ? 1_456 130.4(2) 119.6(2) 140.3(3) yes F2 F1 F4 ? ? 1_556 130.6(2) 120.5(2) 137.5(3) yes F2 F1 F4 ? ? 4_555 62.50(19) 58.84(19) 66.6(2) yes F2 F1 F2 1_556 ? 4_455 84.8(2) 78.0(2) 90.3(2) yes F2 F1 F2 1_556 ? 4_555 85.0(2) 76.0(2) 90.7(2) yes F2 F1 F3 1_556 ? ? 151.3(3) 147.7(3) 157.0(3) yes F2 F1 F3 1_556 ? 2_565 88.0(2) 86.6(2) 89.0(2) yes F2 F1 F4 1_556 ? 1_456 60.0(2) 58.0(2) 63.4(2) yes F2 F1 F4 1_556 ? 1_556 60.4(2) 58.3(2) 63.7(2) yes F2 F1 F4 1_556 ? 4_555 96.2(2) 85.3(2) 104.0(3) yes F2 F1 F2 4_455 ? 4_555 90.8(3) 80.5(2) 99.2(3) yes F2 F1 F3 4_455 ? ? 114.0(2) 110.5(2) 116.9(2) yes F2 F1 F3 4_455 ? 2_565 133.9(2) 127.0(2) 141.9(3) yes F2 F1 F4 4_455 ? 1_456 79.9(2) 72.3(2) 90.1(2) yes F2 F1 F4 4_455 ? 1_556 143.6(3) 138.2(3) 148.5(3) yes F2 F1 F4 4_455 ? 4_555 46.73(16) 41.34(15) 52.22(16) yes F2 F1 F3 4_555 ? ? 114.4(2) 109.9(2) 122.1(2) yes F2 F1 F3 4_555 ? 2_565 133.3(2) 124.0(2) 142.5(3) yes F2 F1 F4 4_555 ? 1_456 143.4(3) 131.3(3) 150.4(3) yes F2 F1 F4 4_555 ? 1_556 79.9(2) 71.7(2) 89.2(2) yes F2 F1 F4 4_555 ? 4_555 47.08(16) 42.12(14) 52.26(16) yes F3 F1 F3 ? ? 2_565 63.5(2) 60.61(19) 68.3(2) yes F3 F1 F4 ? ? 1_456 100.6(3) 96.6(3) 106.5(3) yes F3 F1 F4 ? ? 1_556 101.1(3) 96.9(3) 104.9(3) yes F3 F1 F4 ? ? 4_555 112.4(2) 107.7(2) 117.9(2) yes F3 F1 F4 2_565 ? 1_456 57.5(2) 55.9(2) 60.3(2) yes F3 F1 F4 2_565 ? 1_556 57.2(2) 54.2(2) 59.5(2) yes F3 F1 F4 2_565 ? 4_555 171.7(2) 166.4(2) 177.9(2) yes F4 F1 F4 1_456 ? 1_556 87.6(2) 85.8(2) 89.0(2) yes F4 F1 F4 1_456 ? 4_555 124.5(2) 112.5(2) 136.5(2) yes F4 F1 F4 1_556 ? 4_555 124.8(2) 118.5(2) 133.1(2) yes F1 F2 F1 1_554 ? ? 158.0(3) 154.7(3) 160.8(3) yes F1 F2 F1 1_554 ? 4_454 100.4(2) 97.0(2) 104.5(3) yes F1 F2 F1 1_554 ? 4_554 100.3(2) 95.7(2) 107.5(3) yes F1 F2 F3 1_554 ? ? 97.7(2) 94.6(3) 100.8(3) yes F1 F2 F4 1_554 ? 1_455 62.4(2) 58.09(19) 66.7(2) yes F1 F2 F4 1_554 ? ? 62.2(2) 57.93(19) 66.7(2) yes F1 F2 F4 1_554 ? 4_555 131.3(3) 127.0(2) 137.2(3) yes F1 F2 F1 ? ? 4_454 94.3(2) 87.7(2) 101.5(2) yes F1 F2 F1 ? ? 4_554 94.2(2) 89.3(2) 103.2(2) yes F1 F2 F3 ? ? ? 60.73(19) 59.6(2) 62.11(19) yes F1 F2 F4 ? ? 1_455 103.7(2) 100.4(2) 105.5(2) yes F1 F2 F4 ? ? ? 103.4(2) 99.3(2) 107.5(2) yes F1 F2 F4 ? ? 4_555 69.8(2) 65.8(2) 74.39(19) yes F1 F2 F1 4_454 ? 4_554 90.8(2) 87.2(3) 96.2(3) yes F1 F2 F3 4_454 ? ? 130.0(3) 118.3(2) 144.8(3) yes F1 F2 F4 4_454 ? 1_455 87.3(2) 74.7(2) 98.9(2) yes F1 F2 F4 4_454 ? ? 159.6(3) 148.1(3) 166.7(3) yes F1 F2 F4 4_454 ? 4_555 51.05(17) 48.42(18) 53.29(17) yes F1 F2 F3 4_554 ? ? 130.4(3) 118.5(2) 145.8(2) yes F1 F2 F4 4_554 ? 1_455 160.2(3) 149.0(2) 168.9(3) yes F1 F2 F4 4_554 ? ? 86.6(2) 74.7(2) 97.4(2) yes F1 F2 F4 4_554 ? 4_555 51.06(17) 48.86(17) 52.95(16) yes F3 F2 F4 ? ? 1_455 61.8(2) 59.7(2) 63.4(2) yes F3 F2 F4 ? ? ? 62.6(2) 59.8(2) 65.8(2) yes F3 F2 F4 ? ? 4_555 130.1(2) 127.4(2) 134.35(19) yes F4 F2 F4 1_455 ? ? 89.9(2) 88.9(2) 90.9(2) yes F4 F2 F4 1_455 ? 4_555 135.1(2) 125.5(2) 143.8(2) yes F4 F2 F4 ? ? 4_555 134.9(2) 125.3(2) 144.1(2) yes F1 F3 F1 ? ? 2_564 142.4(3) 138.4(3) 147.4(3) yes F1 F3 F2 ? ? ? 69.1(2) 67.3(3) 70.7(2) yes F1 F3 F3 ? ? 2_564 159.3(3) 157.1(3) 161.9(2) yes F1 F3 F3 ? ? 2_565 59.72(19) 56.71(19) 62.45(18) yes F1 F3 F4 ? ? 1_455 111.7(3) 106.4(3) 117.8(3) yes F1 F3 F4 ? ? ? 110.5(3) 104.3(3) 117.5(3) yes F1 F3 F4 ? ? 2_565 95.2(2) 86.9(2) 102.7(2) yes F1 F3 F4 ? ? 2_665 94.5(2) 82.1(2) 105.6(3) yes F1 F3 F2 2_564 ? ? 146.4(3) 141.3(3) 150.0(3) yes F1 F3 F3 2_564 ? 2_564 56.74(18) 54.85(17) 59.09(19) yes F1 F3 F3 2_564 ? 2_565 83.3(2) 81.94(19) 85.1(2) yes F1 F3 F4 2_564 ? 1_455 93.6(3) 81.8(2) 104.6(2) yes F1 F3 F4 2_564 ? ? 93.0(2) 85.9(2) 98.4(2) yes F1 F3 F4 2_564 ? 2_565 60.9(2) 57.4(2) 64.9(2) yes F1 F3 F4 2_564 ? 2_665 60.9(2) 55.6(2) 65.2(2) yes F2 F3 F3 ? ? 2_564 90.9(2) 88.5(2) 92.74(19) yes F2 F3 F3 ? ? 2_565 128.0(2) 123.6(2) 130.3(3) yes F2 F3 F4 ? ? 1_455 65.3(2) 63.2(2) 67.6(2) yes F2 F3 F4 ? ? ? 65.0(2) 62.4(2) 68.0(2) yes F2 F3 F4 ? ? 2_565 132.9(3) 117.3(2) 148.1(3) yes F2 F3 F4 ? ? 2_665 132.0(3) 115.0(2) 148.9(3) yes F3 F3 F3 2_564 ? 2_565 140.0(2) 138.2(2) 141.7(3) yes F3 F3 F4 2_564 ? 1_455 57.75(19) 56.24(17) 59.3(2) yes F3 F3 F4 2_564 ? ? 57.07(18) 55.19(19) 58.36(19) yes F3 F3 F4 2_564 ? 2_565 99.0(2) 96.9(2) 100.2(2) yes F3 F3 F4 2_564 ? 2_665 98.1(2) 93.5(2) 101.8(2) yes F3 F3 F4 2_565 ? 1_455 134.4(2) 123.1(2) 145.5(2) yes F3 F3 F4 2_565 ? ? 132.6(2) 120.6(2) 145.0(2) yes F3 F3 F4 2_565 ? 2_565 57.16(18) 55.90(17) 58.18(18) yes F3 F3 F4 2_565 ? 2_665 56.14(18) 54.18(16) 57.49(19) yes F4 F3 F4 1_455 ? ? 93.0(2) 91.63(17) 94.1(2) yes F4 F3 F4 1_455 ? 2_565 82.0(2) 68.71(18) 96.92(19) yes F4 F3 F4 1_455 ? 2_665 151.5(3) 142.0(3) 161.0(3) yes F4 F3 F4 ? ? 2_565 151.3(3) 145.2(3) 156.9(3) yes F4 F3 F4 ? ? 2_665 81.0(2) 68.72(18) 94.59(19) yes F4 F3 F4 2_565 ? 2_665 92.0(2) 90.9(2) 93.4(2) yes F1 F4 F1 1_554 ? 1_654 87.4(2) 75.44(18) 100.9(2) yes F1 F4 F1 1_554 ? 4_554 77.1(2) 67.35(18) 83.6(2) yes F1 F4 F2 1_554 ? ? 57.4(2) 54.9(2) 59.0(2) yes F1 F4 F2 1_554 ? 1_655 116.0(3) 102.1(2) 130.8(3) yes F1 F4 F2 1_554 ? 4_554 49.14(18) 41.93(15) 55.5(2) yes F1 F4 F3 1_554 ? ? 88.11(18) 84.91(17) 90.64(18) yes F1 F4 F3 1_554 ? 1_655 164.6(3) 154.4(2) 175.6(3) yes F1 F4 F3 1_554 ? 2_564 61.86(19) 58.42(18) 64.32(19) yes F1 F4 F3 1_554 ? 2_664 120.4(2) 114.56(19) 128.2(3) yes F1 F4 F4 1_554 ? 1_455 46.20(16) 42.26(15) 49.60(17) yes F1 F4 F4 1_554 ? 1_655 133.5(2) 117.68(19) 149.9(2) yes F1 F4 F4 1_554 ? 2_664 77.5(2) 73.4(2) 79.63(19) yes F1 F4 F4 1_554 ? 2_665 135.41(19) 128.44(18) 141.12(17) yes F1 F4 F1 1_654 ? 4_554 77.3(2) 66.16(19) 89.0(3) yes F1 F4 F2 1_654 ? ? 116.2(3) 100.3(3) 133.9(3) yes F1 F4 F2 1_654 ? 1_655 57.7(2) 54.8(2) 61.5(2) yes F1 F4 F2 1_654 ? 4_554 48.94(18) 41.41(15) 55.13(18) yes F1 F4 F3 1_654 ? ? 163.7(3) 152.7(3) 178.1(3) yes F1 F4 F3 1_654 ? 1_655 88.90(18) 86.21(17) 91.12(19) yes F1 F4 F3 1_654 ? 2_564 120.1(2) 111.4(2) 131.5(3) yes F1 F4 F3 1_654 ? 2_664 61.67(18) 58.89(17) 66.13(19) yes F1 F4 F4 1_654 ? 1_455 132.7(2) 117.40(19) 149.4(2) yes F1 F4 F4 1_654 ? 1_655 46.21(16) 42.37(15) 49.42(17) yes F1 F4 F4 1_654 ? 2_664 77.8(2) 73.16(18) 82.6(2) yes F1 F4 F4 1_654 ? 2_665 136.2(2) 128.92(19) 142.32(18) yes F2 F4 F2 ? ? 1_655 89.3(2) 77.3(2) 102.0(3) yes F2 F4 F2 ? ? 4_554 69.56(19) 59.68(19) 80.8(2) yes F2 F4 F3 ? ? ? 52.39(16) 51.03(14) 53.78(17) yes F2 F4 F3 ? ? 1_655 113.2(2) 109.0(2) 120.0(2) yes F2 F4 F3 ? ? 2_564 89.02(18) 87.49(17) 91.18(19) yes F2 F4 F3 ? ? 2_664 166.8(3) 159.2(3) 174.4(3) yes F2 F4 F4 ? ? 1_455 44.89(16) 43.48(16) 46.38(17) yes F2 F4 F4 ? ? 1_655 133.7(2) 120.4(3) 147.1(3) yes F2 F4 F4 ? ? 2_664 129.76(19) 127.9(2) 131.9(2) yes F2 F4 F4 ? ? 2_665 95.2(2) 90.10(16) 100.5(2) yes F2 F4 F2 1_655 ? 4_554 69.18(19) 62.43(15) 79.34(17) yes F2 F4 F3 1_655 ? ? 113.6(2) 106.6(2) 122.9(2) yes F2 F4 F3 1_655 ? 1_655 52.96(17) 51.93(17) 53.90(18) yes F2 F4 F3 1_655 ? 2_564 167.7(3) 162.1(3) 172.5(3) yes F2 F4 F3 1_655 ? 2_664 89.06(18) 87.64(18) 91.1(2) yes F2 F4 F4 1_655 ? 1_455 133.4(2) 120.6(3) 146.8(3) yes F2 F4 F4 1_655 ? 1_655 45.22(16) 43.48(17) 47.11(18) yes F2 F4 F4 1_655 ? 2_664 130.75(19) 128.45(19) 133.7(2) yes F2 F4 F4 1_655 ? 2_665 95.7(2) 90.84(15) 99.8(2) yes F2 F4 F3 4_554 ? ? 121.0(2) 110.7(2) 131.8(2) yes F2 F4 F3 4_554 ? 1_655 121.3(2) 113.14(17) 131.91(19) yes F2 F4 F3 4_554 ? 2_564 108.42(19) 100.60(17) 113.76(18) yes F2 F4 F3 4_554 ? 2_664 108.47(19) 98.57(16) 116.8(2) yes F2 F4 F4 4_554 ? 1_455 90.05(17) 78.33(17) 101.92(18) yes F2 F4 F4 4_554 ? 1_655 89.89(17) 79.22(15) 100.83(16) yes F2 F4 F4 4_554 ? 2_664 97.55(19) 92.48(19) 100.89(17) yes F2 F4 F4 4_554 ? 2_665 158.0(2) 152.7(2) 164.6(2) yes F3 F4 F3 ? ? 1_655 92.3(2) 77.04(16) 107.08(19) yes F3 F4 F3 ? ? 2_564 65.78(17) 64.36(17) 67.15(18) yes F3 F4 F3 ? ? 2_664 129.3(3) 112.7(2) 148.1(3) yes F3 F4 F4 ? ? 1_455 43.11(15) 42.38(14) 43.61(14) yes F3 F4 F4 ? ? 1_655 135.5(2) 119.67(17) 151.67(19) yes F3 F4 F4 ? ? 2_664 111.6(2) 104.9(2) 119.5(2) yes F3 F4 F4 ? ? 2_665 49.71(15) 41.98(12) 56.42(15) yes F3 F4 F3 1_655 ? 2_564 128.9(3) 113.6(2) 145.6(3) yes F3 F4 F3 1_655 ? 2_664 66.12(17) 63.54(15) 68.78(17) yes F3 F4 F4 1_655 ? 1_455 134.7(2) 119.43(18) 149.4(2) yes F3 F4 F4 1_655 ? 1_655 43.89(15) 42.43(15) 45.38(14) yes F3 F4 F4 1_655 ? 2_664 112.5(2) 105.5(2) 120.5(2) yes F3 F4 F4 1_655 ? 2_665 49.42(15) 41.49(13) 56.28(15) yes F3 F4 F3 2_564 ? 2_664 91.0(2) 77.4(2) 104.4(3) yes F3 F4 F4 2_564 ? 1_455 44.17(16) 43.08(15) 44.82(16) yes F3 F4 F4 2_564 ? 1_655 134.3(2) 121.1(3) 148.3(2) yes F3 F4 F4 2_564 ? 2_664 48.41(15) 41.52(13) 55.02(15) yes F3 F4 F4 2_564 ? 2_665 86.0(2) 76.72(17) 96.0(2) yes F3 F4 F4 2_664 ? 1_455 134.1(2) 120.7(3) 147.6(2) yes F3 F4 F4 2_664 ? 1_655 43.88(16) 43.44(16) 44.35(16) yes F3 F4 F4 2_664 ? 2_664 49.21(15) 43.30(13) 54.86(15) yes F3 F4 F4 2_664 ? 2_665 86.5(2) 75.27(17) 98.8(2) yes F4 F4 F4 2_664 ? 2_665 104.3(2) 95.56(19) 113.7(2) yes loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_meas _refln_F_calc _refln_F_sigma _refln_include_status -1 -1 -10 2 13.07 14.46 1.48 o 1 -1 -10 2 13.32 13.91 0.80 o -2 0 -10 2 12.24 10.77 1.00 o -1 0 -10 1 25.50 23.50 0.88 o 0 0 -10 0 7.89 6.87 2.78 < 0 0 -10 2 9.60 10.89 1.25 o 1 0 -10 1 23.13 23.57 0.87 o -3 1 -10 2 6.19 6.68 2.13 < -2 1 -10 1 7.25 4.97 2.72 < -1 1 -10 0 32.48 33.50 1.22 o -1 1 -10 2 12.14 6.96 1.09 o 0 1 -10 1 0.71 4.37 19.87 < 1 1 -10 2 8.70 6.47 1.15 o -2 2 -10 2 13.44 14.59 1.47 o 0 2 -10 0 19.37 18.73 1.39 o 0 2 -10 2 14.66 14.56 0.96 o 1 2 -10 1 17.56 16.58 0.92 o -3 3 -10 2 12.79 12.45 1.55 o -2 3 -10 1 22.33 22.59 1.29 o -1 3 -10 2 13.48 13.13 1.49 o 0 3 -10 1 25.27 22.71 1.15 o 1 3 -10 2 11.77 12.74 0.91 o -2 4 -10 2 6.88 4.38 2.66 < 0 4 -10 2 8.88 4.31 1.43 o 1 4 -10 1 13.75 10.79 1.46 o -3 5 -10 2 13.28 12.99 1.43 o 0 5 -10 1 11.70 10.81 1.88 o 1 5 -10 2 13.28 12.92 1.59 o -2 6 -10 2 14.45 13.67 1.48 o 0 6 -10 2 14.66 13.75 0.98 o 0 7 -10 1 12.35 13.07 1.97 o -2 8 -10 2 13.71 11.40 1.64 o 0 8 -10 2 12.30 11.38 1.23 o 1 -1 -9 2 0.00 1.63 19.24 < -4 0 -9 2 10.45 10.85 1.17 o -3 0 -9 1 9.96 10.93 0.94 o -2 0 -9 2 12.60 11.95 0.78 o -1 0 -9 1 12.89 12.55 0.72 o 0 0 -9 2 12.88 11.81 0.73 o 1 0 -9 1 12.86 12.84 0.80 o 2 0 -9 0 0.00 0.75 21.45 < 2 0 -9 2 10.89 10.52 0.89 o -3 1 -9 2 16.66 16.90 0.69 o -2 1 -9 1 25.31 23.86 0.68 o -1 1 -9 0 23.37 23.14 0.83 o -1 1 -9 2 18.71 17.97 0.57 o 0 1 -9 -1 14.17 11.58 1.53 o 0 1 -9 1 24.03 23.52 0.66 o 1 1 -9 0 22.65 23.08 0.84 o 1 1 -9 2 16.58 17.07 0.72 o 2 1 -9 -1 12.41 11.87 0.94 o 2 1 -9 1 21.76 21.15 0.70 o -4 2 -9 2 9.14 10.38 1.41 o -3 2 -9 1 17.21 17.11 0.98 o -2 2 -9 0 50.41 50.17 0.92 o -2 2 -9 2 11.15 10.70 0.78 o -1 2 -9 -1 28.47 26.03 0.71 o -1 2 -9 1 18.59 18.47 0.84 o 0 2 -9 -2 17.34 16.41 0.92 o 0 2 -9 0 52.64 52.98 0.89 o 0 2 -9 2 11.66 10.73 0.69 o 1 2 -9 -1 28.43 26.14 0.83 o 1 2 -9 1 18.43 17.65 0.71 o 2 2 -9 -2 15.85 16.38 0.98 o 2 2 -9 0 49.17 50.27 0.78 o 2 2 -9 2 8.07 10.49 1.13 o -3 3 -9 2 7.28 8.29 1.52 < -2 3 -9 1 6.52 8.28 1.65 < -1 3 -9 0 29.47 28.56 1.15 o -1 3 -9 2 7.75 8.24 1.36 < 0 3 -9 1 8.11 7.16 1.07 o 1 3 -9 -2 13.02 15.23 1.13 o 1 3 -9 0 28.75 28.51 0.82 o 1 3 -9 2 6.53 8.06 1.27 < 2 3 -9 -1 19.39 16.56 0.92 o 2 3 -9 1 5.67 5.32 1.62 < -4 4 -9 2 14.34 14.19 1.02 o -3 4 -9 1 21.08 20.62 0.94 o -2 4 -9 0 5.96 6.06 2.11 < -2 4 -9 2 15.99 15.80 1.21 o -1 4 -9 -1 5.07 6.40 3.58 < -1 4 -9 1 24.85 23.58 1.15 o 0 4 -9 -2 7.41 6.76 2.90 < 0 4 -9 0 7.71 6.55 2.46 < 0 4 -9 2 15.27 15.90 0.69 o 1 4 -9 -1 7.96 6.32 1.66 < 1 4 -9 1 24.19 24.39 0.70 o 2 4 -9 0 7.92 6.20 1.29 o 2 4 -9 2 13.19 14.45 0.86 o -3 5 -9 2 13.24 13.21 1.56 o -2 5 -9 1 18.68 17.87 1.31 o -1 5 -9 0 54.12 52.78 1.19 o -1 5 -9 2 19.13 13.71 1.04 o 0 5 -9 1 18.56 18.91 0.87 o 1 5 -9 -2 11.38 13.74 2.02 < 1 5 -9 0 52.77 52.72 0.91 o 1 5 -9 2 14.85 13.38 0.75 o 2 5 -9 -1 22.55 21.84 0.89 o 2 5 -9 1 17.92 17.89 0.77 o -4 6 -9 2 11.41 10.96 1.73 o -3 6 -9 1 5.26 4.97 3.40 < -2 6 -9 0 19.55 19.40 1.27 o -2 6 -9 2 13.48 13.01 1.40 o -1 6 -9 -1 19.09 19.14 1.36 o -1 6 -9 1 0.00 3.57 29.03 < 0 6 -9 -2 17.91 20.48 1.39 o 0 6 -9 2 12.11 13.00 1.01 o 1 6 -9 -1 19.09 19.52 0.94 o 1 6 -9 1 3.92 1.79 2.37 < 2 6 -9 0 18.74 19.29 0.74 o 2 6 -9 2 10.19 10.91 1.02 o -3 7 -9 2 12.75 10.98 1.62 o -2 7 -9 1 18.14 17.93 1.33 o -1 7 -9 0 42.03 41.44 1.17 o -1 7 -9 2 10.69 11.69 1.47 o 0 7 -9 1 18.57 17.01 0.90 o 1 7 -9 0 40.96 41.51 0.87 o 1 7 -9 2 9.62 11.00 1.02 o 2 7 -9 1 14.43 14.66 0.80 o -2 8 -9 2 12.41 11.66 1.58 o -1 8 -9 1 20.76 19.82 1.16 o 0 8 -9 2 12.89 11.78 1.01 o 1 8 -9 -1 18.69 17.92 0.92 o 1 8 -9 1 20.91 20.50 0.75 o 2 8 -9 0 14.00 14.70 1.55 o 2 8 -9 2 9.01 12.00 2.15 < -3 9 -9 2 16.79 16.12 1.41 o -2 9 -9 1 7.40 7.89 2.64 < -1 9 -9 0 27.08 28.09 1.25 o -1 9 -9 2 17.33 17.10 1.30 o 0 9 -9 1 6.53 6.70 2.67 < 1 9 -9 0 26.93 28.13 0.86 o 1 9 -9 2 16.41 16.14 0.79 o 0 10 -9 2 8.20 3.33 1.64 < 1 10 -9 1 4.89 6.90 2.83 < -1 11 -9 2 8.46 9.88 2.26 < 0 11 -9 1 14.38 14.73 1.54 o 1 11 -9 2 10.19 9.88 1.38 o 0 12 -9 2 18.62 16.31 1.36 o -1 13 -9 2 10.58 10.08 1.94 < -1 -1 -8 2 14.96 16.18 0.71 o 1 -1 -8 2 13.13 14.75 0.65 o 3 -1 -8 2 11.46 11.77 1.22 o -4 0 -8 2 8.68 10.88 1.23 o -3 0 -8 1 22.39 21.88 0.65 o -2 0 -8 2 10.99 11.61 0.69 o -1 0 -8 1 26.70 25.86 0.55 o 0 0 -8 0 46.32 45.41 0.80 o 0 0 -8 2 11.34 11.78 0.69 o 1 0 -8 1 26.21 27.10 0.62 o 2 0 -8 0 41.23 41.23 0.70 o 2 0 -8 2 10.15 11.30 0.77 o 3 0 -8 1 25.45 24.86 0.86 o 4 0 -8 0 32.51 32.08 0.91 o -5 1 -8 2 5.87 7.94 2.04 < -4 1 -8 1 8.54 7.76 1.40 o -3 1 -8 0 36.29 37.44 0.86 o -3 1 -8 2 7.34 8.12 0.90 o -2 1 -8 -1 21.88 22.16 0.71 o -2 1 -8 1 6.38 6.88 1.04 o -1 1 -8 0 39.51 40.72 0.67 o -1 1 -8 2 15.68 8.10 0.55 o 0 1 -8 -1 23.93 24.30 0.67 o 0 1 -8 1 6.12 4.15 0.96 o 1 1 -8 0 39.78 40.69 0.68 o 1 1 -8 2 7.64 7.93 0.93 o 2 1 -8 -1 23.45 23.91 0.67 o 2 1 -8 1 1.76 1.29 4.26 < 3 1 -8 -2 18.28 19.23 0.73 o 3 1 -8 0 36.64 37.35 0.70 o 3 1 -8 2 7.05 7.61 1.60 < 4 1 -8 -1 20.42 21.33 0.95 o -4 2 -8 0 30.73 30.65 0.89 o -4 2 -8 2 10.36 10.76 1.08 o -3 2 -8 -1 0.00 3.71 25.40 < -3 2 -8 1 19.57 18.97 0.85 o -2 2 -8 -2 8.50 11.14 1.55 < -2 2 -8 0 34.65 35.76 0.68 o -2 2 -8 2 13.19 12.92 0.67 o -1 2 -8 -1 5.84 5.03 1.30 < -1 2 -8 1 20.57 19.48 0.62 o 0 2 -8 -2 11.52 12.00 1.07 o 0 2 -8 0 37.74 37.88 0.61 o 0 2 -8 2 13.27 12.88 0.58 o 1 2 -8 -1 7.16 6.21 1.34 < 1 2 -8 1 17.31 17.34 0.65 o 2 2 -8 -2 10.18 12.04 1.12 o 2 2 -8 0 33.96 35.53 0.67 o 2 2 -8 2 10.48 10.68 0.79 o 3 2 -8 -1 4.53 6.34 1.86 < 3 2 -8 1 14.47 14.06 0.77 o 4 2 -8 -2 7.44 11.21 1.33 < 4 2 -8 0 31.31 30.29 0.91 o -5 3 -8 2 11.57 11.52 1.13 o -4 3 -8 1 23.08 22.77 0.91 o -3 3 -8 0 38.36 38.44 0.88 o -3 3 -8 2 11.87 12.20 0.97 o -2 3 -8 -1 18.85 17.88 0.95 o -2 3 -8 1 27.21 26.77 0.77 o -1 3 -8 -2 8.09 5.56 1.41 < -1 3 -8 0 42.63 42.85 0.69 o -1 3 -8 2 13.65 12.40 0.55 o 0 3 -8 -1 22.92 21.63 0.78 o 0 3 -8 1 28.71 28.64 0.64 o 1 3 -8 -2 10.96 4.99 1.62 o 1 3 -8 0 42.79 42.95 0.65 o 1 3 -8 2 11.45 12.38 0.71 o 2 3 -8 -1 24.63 23.35 0.66 o 2 3 -8 1 26.58 26.92 0.65 o 3 3 -8 -2 5.81 5.74 1.52 < 3 3 -8 0 37.75 38.69 0.71 o 3 3 -8 2 10.24 11.82 0.85 o 4 3 -8 -1 22.80 22.04 0.70 o -4 4 -8 2 5.39 6.60 2.00 < -3 4 -8 -1 25.47 23.28 1.26 o -3 4 -8 1 10.32 10.64 1.11 o -2 4 -8 -2 16.48 16.38 1.06 o -2 4 -8 0 23.08 24.61 0.83 o -2 4 -8 2 10.28 7.38 0.97 o -1 4 -8 -1 27.25 25.75 0.82 o -1 4 -8 1 10.65 11.82 1.34 o 0 4 -8 -2 18.20 18.16 0.88 o 0 4 -8 0 25.46 25.68 0.57 o 0 4 -8 2 9.84 7.48 0.78 o 1 4 -8 -1 25.83 25.50 0.78 o 1 4 -8 1 11.91 11.56 0.74 o 2 4 -8 0 24.13 24.67 0.67 o 2 4 -8 2 7.94 6.80 1.12 o 3 4 -8 -1 22.92 22.81 0.71 o 3 4 -8 1 10.86 10.30 0.90 o 4 4 -8 -2 15.24 16.37 0.99 o 4 4 -8 0 20.82 22.03 0.87 o -5 5 -8 2 10.47 10.83 1.24 o -4 5 -8 1 9.90 10.60 1.26 o -3 5 -8 0 9.64 9.19 1.36 o -3 5 -8 2 10.44 12.88 1.02 o -2 5 -8 -1 8.39 9.51 1.44 < -2 5 -8 1 12.37 12.74 1.44 o -1 5 -8 -2 14.77 14.06 0.97 o -1 5 -8 0 9.72 11.93 1.50 o -1 5 -8 2 12.75 13.77 0.71 o 0 5 -8 1 13.26 13.47 0.83 o 1 5 -8 -2 14.03 14.91 1.35 o 1 5 -8 0 12.47 11.97 0.75 o 1 5 -8 2 11.72 12.85 0.72 o 2 5 -8 -1 8.91 8.91 0.95 o 2 5 -8 1 12.69 12.59 0.81 o 3 5 -8 -2 12.21 14.19 0.86 o 3 5 -8 0 10.12 9.29 0.91 o 3 5 -8 2 9.95 10.80 0.95 o -4 6 -8 2 11.37 11.53 1.58 o -3 6 -8 1 19.75 19.59 1.28 o -2 6 -8 0 72.35 71.24 1.27 o -2 6 -8 2 12.87 12.56 1.25 o -1 6 -8 -1 14.81 15.16 1.47 o -1 6 -8 1 21.35 20.88 1.07 o 0 6 -8 -2 8.86 2.81 1.94 < 0 6 -8 0 78.25 75.94 1.22 o 0 6 -8 2 13.63 12.62 0.70 o 1 6 -8 -1 16.38 14.78 0.89 o 1 6 -8 1 19.29 19.99 0.67 o 2 6 -8 -2 7.33 2.77 1.50 < 2 6 -8 0 70.87 71.36 0.91 o 2 6 -8 2 10.77 11.70 0.84 o 3 6 -8 -1 13.19 12.79 0.83 o 3 6 -8 1 17.64 17.24 0.74 o -5 7 -8 2 12.77 11.02 1.62 o -4 7 -8 1 13.91 12.96 1.48 o -3 7 -8 0 25.39 25.71 1.27 o -3 7 -8 2 12.77 12.14 1.38 o -2 7 -8 -1 21.00 19.85 1.32 o -2 7 -8 1 15.45 14.96 1.31 o -1 7 -8 -2 16.48 16.02 1.43 o -1 7 -8 0 28.90 28.80 1.11 o -1 7 -8 2 15.10 12.62 0.83 o 0 7 -8 1 17.16 15.63 0.87 o 1 7 -8 0 28.23 28.79 0.66 o 1 7 -8 2 12.94 12.21 0.77 o 2 7 -8 -1 23.58 21.94 0.69 o 2 7 -8 1 13.21 14.70 0.82 o 3 7 -8 -2 15.34 16.06 0.77 o 3 7 -8 0 24.44 25.68 0.72 o 3 7 -8 2 11.65 11.12 0.84 o -4 8 -8 2 14.00 13.56 1.40 o -3 8 -8 1 9.31 8.62 1.91 < -2 8 -8 0 15.34 16.07 1.34 o -2 8 -8 2 15.08 15.14 1.20 o -1 8 -8 -1 17.47 14.39 1.33 o -1 8 -8 1 10.83 9.29 1.39 o 0 8 -8 -2 11.68 13.40 1.89 o 0 8 -8 0 18.49 16.88 1.15 o 0 8 -8 2 14.16 15.11 0.90 o 1 8 -8 -1 16.25 15.00 0.92 o 1 8 -8 1 8.82 8.70 0.97 o 2 8 -8 -2 12.32 13.46 1.49 o 2 8 -8 0 15.74 16.07 0.76 o 2 8 -8 2 14.09 13.49 0.79 o 3 8 -8 -1 14.77 13.80 0.82 o 3 8 -8 1 7.24 7.37 1.33 < -3 9 -8 0 41.18 40.99 1.24 o -3 9 -8 2 9.56 10.19 1.75 < -2 9 -8 -1 8.15 8.84 2.34 < -2 9 -8 1 17.01 16.19 1.20 o -1 9 -8 -2 10.28 8.42 1.89 < -1 9 -8 0 46.90 45.75 1.14 o -1 9 -8 2 11.65 10.41 1.37 o 0 9 -8 -1 13.05 10.66 1.44 o 0 9 -8 1 15.40 16.18 1.18 o 1 9 -8 0 47.66 45.75 0.87 o 1 9 -8 2 9.68 10.11 0.91 o 2 9 -8 -1 11.09 11.27 0.91 o 2 9 -8 1 14.05 14.54 0.86 o 3 9 -8 -2 7.35 8.72 1.44 < 3 9 -8 0 41.82 40.96 0.76 o -4 10 -8 2 14.40 16.95 1.59 o -3 10 -8 1 12.81 11.83 1.63 o -2 10 -8 0 44.29 41.83 1.23 o -2 10 -8 2 17.27 18.38 1.20 o -1 10 -8 -1 19.83 19.62 1.40 o 0 10 -8 -2 12.16 13.40 1.60 o 0 10 -8 0 45.56 43.95 1.11 o 0 10 -8 2 17.79 18.43 0.69 o 1 10 -8 -1 21.63 20.77 1.26 o 1 10 -8 1 13.30 13.88 0.82 o 2 10 -8 -2 13.90 13.42 1.06 o 2 10 -8 0 41.16 41.94 0.75 o 2 10 -8 2 15.68 17.06 0.81 o 3 10 -8 -1 18.95 20.09 0.89 o -1 11 -8 2 15.68 13.57 1.15 o 0 11 -8 1 0.00 4.85 26.69 < 1 11 -8 0 45.31 44.50 0.88 o 1 11 -8 2 12.98 12.52 0.85 o 2 11 -8 -1 13.53 12.27 0.89 o 2 11 -8 1 5.27 5.12 1.94 < 3 11 -8 -2 17.89 18.57 1.34 o -1 12 -8 1 12.88 11.78 1.27 o 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11.76 10.59 0.68 o 5 9 -2 0 57.21 56.88 0.86 o -2 10 -2 2 25.77 24.78 0.93 o -1 10 -2 -1 18.73 17.48 0.99 o -1 10 -2 1 19.83 20.79 0.97 o 0 10 -2 -2 16.67 16.67 0.70 o 0 10 -2 0 81.03 79.72 1.00 o 0 10 -2 2 25.30 24.58 0.66 o 1 10 -2 -1 18.23 18.53 0.43 o 1 10 -2 1 17.01 17.64 0.58 o 2 10 -2 -2 16.43 16.75 0.45 o 2 10 -2 0 70.16 70.72 0.87 o 2 10 -2 2 20.13 20.43 0.54 o 3 10 -2 -1 15.86 16.50 0.52 o 3 10 -2 1 12.24 13.11 0.71 o 4 10 -2 -2 12.61 13.54 0.58 o 4 10 -2 0 53.31 54.16 0.78 o 5 10 -2 -1 13.92 13.14 0.70 o 5 10 -2 1 11.62 9.32 0.90 o 6 10 -2 -2 16.45 10.04 0.82 o -1 11 -2 2 22.82 21.57 0.87 o 0 11 -2 1 35.86 34.92 0.61 o 1 11 -2 -2 11.84 11.90 0.69 o 1 11 -2 0 63.15 61.85 0.95 o 1 11 -2 2 19.33 19.95 0.64 o 2 11 -2 -1 19.99 21.18 0.59 o 2 11 -2 1 26.41 27.77 0.64 o 3 11 -2 -2 10.87 11.81 0.59 o 3 11 -2 0 48.34 49.79 0.67 o 3 11 -2 2 16.19 16.36 0.72 o 4 11 -2 -1 14.51 15.75 0.59 o 4 11 -2 1 21.04 20.48 0.88 o 5 11 -2 -2 11.30 11.07 0.79 o 5 11 -2 0 37.71 37.40 0.86 o 0 12 -2 2 6.77 6.49 1.41 < 1 12 -2 -1 36.06 35.18 0.64 o 1 12 -2 1 14.84 14.83 0.66 o 2 12 -2 -2 16.24 17.21 0.62 o 2 12 -2 0 84.59 86.34 1.01 o 2 12 -2 2 7.20 8.58 0.82 o 3 12 -2 -1 29.57 29.86 0.56 o 3 12 -2 1 14.02 14.03 0.76 o 4 12 -2 -2 14.10 13.91 0.59 o 4 12 -2 0 65.90 66.96 0.90 o 4 12 -2 2 7.60 9.21 1.49 < 5 12 -2 -1 21.99 22.66 0.73 o 5 12 -2 1 12.71 10.89 1.10 o 1 13 -2 -2 20.83 21.37 0.82 o 1 13 -2 0 50.87 51.40 0.75 o 1 13 -2 2 7.01 8.03 0.96 o 2 13 -2 -1 20.64 20.64 0.64 o 2 13 -2 1 8.50 9.42 0.94 o 3 13 -2 -2 18.96 20.44 0.56 o 3 13 -2 0 43.61 43.76 0.67 o 3 13 -2 2 10.11 8.68 0.87 o 4 13 -2 -1 18.32 19.06 0.71 o 4 13 -2 1 11.83 7.66 1.11 o 5 13 -2 -2 16.72 17.82 0.74 o 5 13 -2 0 35.55 34.06 0.94 o 6 13 -2 -1 17.99 15.74 0.97 o 1 14 -2 -1 13.74 14.11 0.92 o 1 14 -2 1 30.46 30.80 0.69 o 2 14 -2 -2 13.92 14.62 0.71 o 2 14 -2 0 43.38 44.79 0.75 o 2 14 -2 2 24.69 25.23 0.74 o 3 14 -2 -1 10.45 11.43 0.69 o 3 14 -2 1 24.29 26.20 0.76 o 4 14 -2 -2 10.74 12.02 0.73 o 4 14 -2 0 35.66 34.91 0.77 o 4 14 -2 2 31.55 18.32 1.02 o 5 14 -2 -1 10.47 8.95 0.99 o 6 14 -2 -2 10.42 9.20 1.12 o 1 15 -2 -2 8.14 9.21 1.31 o 1 15 -2 2 17.84 19.42 0.79 o 2 15 -2 -1 31.06 32.13 0.70 o 2 15 -2 1 22.45 22.70 0.75 o 3 15 -2 -2 6.81 8.93 0.90 o 3 15 -2 0 29.60 29.80 0.63 o 3 15 -2 2 17.44 17.01 0.89 o 4 15 -2 -1 26.83 28.63 0.76 o 4 15 -2 1 17.09 17.67 0.84 o 5 15 -2 -2 6.29 8.17 1.57 < 5 15 -2 0 26.51 25.82 1.03 o 1 16 -2 -1 31.79 32.49 0.93 o 1 16 -2 1 6.01 6.90 1.79 < 2 16 -2 -2 27.48 30.18 0.96 o 2 16 -2 0 61.40 61.38 0.89 o 2 16 -2 2 2.57 4.79 3.56 < 3 16 -2 -1 25.54 26.40 0.62 o 3 16 -2 1 8.60 7.54 1.17 o 4 16 -2 -2 24.21 26.17 0.63 o 4 16 -2 0 50.33 50.80 0.88 o 5 16 -2 -1 20.77 19.89 0.85 o 1 17 -2 -2 19.57 19.19 0.97 o 1 17 -2 0 8.43 5.43 1.46 < 1 17 -2 2 18.88 21.91 1.22 o 2 17 -2 -1 7.01 8.06 1.80 < 2 17 -2 1 20.77 21.19 0.81 o 3 17 -2 -2 17.99 17.64 0.78 o 3 17 -2 0 9.58 6.14 0.89 o 3 17 -2 2 20.54 17.96 0.88 o 4 17 -2 -1 10.02 7.22 1.10 o 4 17 -2 1 14.42 15.64 1.02 o 5 17 -2 -2 15.69 14.30 0.89 o 1 18 -2 -1 24.13 24.29 1.05 o 1 18 -2 1 26.77 27.67 1.08 o 2 18 -2 -2 6.25 8.83 1.90 < 2 18 -2 0 26.92 28.64 1.10 o 2 18 -2 2 20.99 21.31 0.87 o 3 18 -2 -1 21.70 22.18 0.69 o 3 18 -2 1 26.23 25.50 0.85 o 4 18 -2 -2 8.14 9.71 1.09 o 4 18 -2 0 25.70 25.40 0.85 o 5 18 -2 -1 19.11 18.43 0.88 o 1 19 -2 -2 12.76 15.05 1.26 o 1 19 -2 0 57.30 59.70 1.14 o 1 19 -2 2 12.04 12.62 1.45 o 2 19 -2 -1 24.20 24.62 1.08 o 2 19 -2 1 7.33 8.29 1.56 < 3 19 -2 -2 11.28 14.54 1.45 o 3 19 -2 0 53.06 52.13 0.81 o 3 19 -2 2 17.97 11.57 0.99 o 4 19 -2 -1 19.78 20.53 0.89 o 5 19 -2 -2 16.27 13.26 0.96 o 1 20 -2 -1 9.61 10.03 1.52 o 1 20 -2 1 17.67 17.31 1.25 o 2 20 -2 -2 23.80 25.96 1.10 o 2 20 -2 0 3.42 3.11 4.06 < 2 20 -2 2 8.41 10.37 1.70 < 3 20 -2 -1 10.27 10.96 1.04 o 3 20 -2 1 14.13 15.04 1.09 o 4 20 -2 -2 21.62 23.35 0.89 o 1 21 -2 -2 8.80 6.65 1.68 < 1 21 -2 0 24.54 24.08 1.19 o 1 21 -2 2 18.72 21.83 1.39 o 2 21 -2 -1 17.12 17.32 1.26 o 2 21 -2 1 24.06 24.48 1.28 o 3 21 -2 -2 7.09 6.74 2.25 < 3 21 -2 0 23.40 21.94 0.92 o 4 21 -2 -1 18.88 16.15 1.37 o 1 22 -2 -1 23.67 24.94 1.21 o 1 22 -2 1 12.32 11.17 1.62 o 2 22 -2 -2 3.56 5.65 3.89 < 2 22 -2 0 16.83 18.17 1.42 o 3 22 -2 -1 21.51 23.22 0.92 o 4 22 -2 -2 0.00 5.35 26.88 < 0 23 -2 -1 12.94 12.26 1.36 o 1 23 -2 -2 30.72 32.00 1.17 o 1 23 -2 0 27.84 27.19 1.22 o 2 23 -2 -1 11.55 10.87 1.74 o 3 23 -2 -2 28.02 30.21 0.91 o 0 24 -2 0 31.26 33.12 1.24 o 1 24 -2 -1 12.40 12.35 1.64 o 2 24 -2 -2 13.40 12.20 1.72 o 0 25 -2 -1 19.43 18.86 1.37 o 1 25 -2 -2 4.07 4.80 5.03 < 1 -1 -1 2 3.05 3.37 0.36 o -4 0 -1 2 2.39 2.11 2.03 < -3 0 -1 1 3.18 3.23 0.38 o -2 0 -1 2 1.92 1.57 0.47 < -1 0 -1 1 2.93 2.96 0.22 o 0 0 -1 2 2.00 1.55 0.45 < 1 0 -1 1 7.31 7.18 0.21 o 2 0 -1 0 5.21 5.66 0.26 o 2 0 -1 2 2.81 2.12 1.87 < -4 1 -1 1 12.47 12.16 1.03 o -3 1 -1 0 130.87 124.53 1.36 o -3 1 -1 2 1.92 2.03 0.52 < -2 1 -1 -1 5.39 5.14 0.27 o -2 1 -1 1 14.20 14.26 0.23 o -1 1 -1 0 176.77 173.51 1.77 o -1 1 -1 2 1.79 1.71 0.48 < 0 1 -1 -1 6.11 6.83 0.27 o 0 1 -1 1 6.61 6.80 0.18 o 1 1 -1 0 178.18 173.64 1.79 o 1 1 -1 2 1.92 1.97 0.65 < 2 1 -1 -1 6.75 7.09 0.25 o 2 1 -1 1 2.21 1.17 0.61 < 3 1 -1 -2 4.31 4.45 0.35 o 3 1 -1 0 129.49 124.77 1.34 o 4 1 -1 -1 4.60 4.96 1.53 < -4 2 -1 2 7.74 8.88 0.48 o -3 2 -1 -1 10.50 10.53 0.80 o -3 2 -1 1 6.71 7.06 0.28 o -2 2 -1 -2 5.85 5.23 0.77 o -2 2 -1 0 77.88 77.46 0.81 o -2 2 -1 2 8.72 9.40 0.22 o -1 2 -1 -1 13.89 14.51 0.24 o -1 2 -1 1 11.74 11.78 0.22 o 0 2 -1 -2 7.10 6.85 0.26 o 0 2 -1 0 94.84 93.58 0.96 o 0 2 -1 2 8.84 9.16 0.26 o 1 2 -1 -1 13.20 14.03 0.23 o 1 2 -1 1 12.96 13.84 0.25 o 2 2 -1 -2 7.15 6.74 0.26 o 2 2 -1 0 78.30 77.24 0.81 o 2 2 -1 2 7.68 8.39 0.47 o 3 2 -1 -1 9.72 9.75 0.25 o 3 2 -1 1 9.82 10.02 0.39 o 4 2 -1 -2 5.01 5.04 0.48 o -3 3 -1 0 62.24 59.13 0.69 o -3 3 -1 2 10.13 9.81 0.31 o -2 3 -1 -1 10.78 10.63 0.23 o -2 3 -1 1 20.33 20.64 0.28 o -1 3 -1 -2 4.83 5.40 0.31 o -1 3 -1 0 74.70 75.28 0.77 o -1 3 -1 2 12.52 12.62 0.27 o 0 3 -1 -1 10.48 10.61 0.27 o 0 3 -1 1 17.77 17.55 0.27 o 1 3 -1 -2 5.31 5.69 0.33 o 1 3 -1 0 75.64 75.41 0.78 o 1 3 -1 2 10.32 9.68 0.29 o 2 3 -1 -1 5.98 6.30 0.28 o 2 3 -1 1 9.36 9.61 0.27 o 3 3 -1 -2 5.01 5.56 0.30 o 3 3 -1 0 60.60 59.38 0.71 o 3 3 -1 2 6.29 6.93 0.69 o 4 3 -1 -1 4.82 3.84 0.78 o 5 3 -1 -2 5.09 5.30 1.60 < -4 4 -1 2 0.00 2.42 19.49 < -3 4 -1 1 4.25 3.91 0.40 o -2 4 -1 -2 7.07 8.23 0.75 o -2 4 -1 0 155.13 150.86 1.56 o -2 4 -1 2 0.45 1.11 4.02 < -1 4 -1 -1 18.57 17.23 0.29 o -1 4 -1 1 6.75 6.50 0.33 o 0 4 -1 -2 7.63 8.41 0.30 o 0 4 -1 0 179.70 185.52 1.81 o 0 4 -1 2 1.26 1.13 1.70 < 1 4 -1 -1 12.37 12.58 0.26 o 1 4 -1 1 8.91 9.06 0.31 o 2 4 -1 -2 7.17 8.09 0.29 o 2 4 -1 0 153.71 150.51 1.55 o 2 4 -1 2 2.76 2.49 1.45 < 3 4 -1 -1 12.02 11.78 0.28 o 3 4 -1 1 6.05 6.63 0.70 o 4 4 -1 -2 7.68 7.77 0.54 o 4 4 -1 0 104.51 105.41 1.13 o -3 5 -1 0 110.34 107.25 1.16 o -3 5 -1 2 9.62 9.99 0.28 o -2 5 -1 -1 4.17 4.46 0.56 o -2 5 -1 1 12.45 12.24 0.27 o -1 5 -1 -2 9.99 10.03 0.23 o -1 5 -1 0 154.14 152.09 1.56 o -1 5 -1 2 9.79 9.38 0.32 o 0 5 -1 -1 7.51 8.07 0.30 o 0 5 -1 1 17.01 16.62 0.32 o 1 5 -1 -2 11.04 12.09 0.26 o 1 5 -1 0 153.61 152.12 1.55 o 1 5 -1 2 9.62 9.61 0.30 o 2 5 -1 -1 15.86 16.23 0.26 o 2 5 -1 1 14.30 14.11 0.34 o 3 5 -1 -2 9.33 10.00 0.26 o 3 5 -1 0 108.99 107.49 1.15 o 3 5 -1 2 9.22 9.49 0.79 o 4 5 -1 -1 15.84 16.02 0.53 o 4 5 -1 1 8.65 9.45 0.67 o 5 5 -1 -2 7.25 7.38 1.44 < -3 6 -1 1 31.93 29.80 0.73 o -2 6 -1 -2 3.33 4.04 1.43 < -2 6 -1 0 55.99 54.61 0.62 o -2 6 -1 2 23.49 22.72 0.35 o -1 6 -1 -1 19.37 19.60 0.32 o -1 6 -1 1 35.28 33.87 0.44 o 0 6 -1 -2 2.14 3.66 0.86 < 0 6 -1 0 68.74 68.01 0.72 o 0 6 -1 2 23.54 22.57 0.39 o 1 6 -1 -1 23.05 22.72 0.32 o 1 6 -1 1 25.63 24.89 0.37 o 2 6 -1 -2 1.79 3.71 0.92 < 2 6 -1 0 54.93 54.28 0.60 o 2 6 -1 2 17.09 15.66 0.52 o 3 6 -1 -1 17.50 17.48 0.35 o 3 6 -1 1 15.65 16.34 0.54 o 4 6 -1 -2 2.55 4.16 1.35 < 4 6 -1 0 37.82 38.97 0.68 o 4 6 -1 2 21.32 10.36 0.61 o 5 6 -1 -1 12.31 12.01 0.57 o -3 7 -1 2 6.54 6.81 0.42 o -2 7 -1 -1 27.35 26.83 0.56 o -2 7 -1 1 16.74 16.24 0.34 o -1 7 -1 -2 5.49 5.78 0.62 o -1 7 -1 0 30.86 30.63 0.41 o -1 7 -1 2 7.09 6.92 0.39 o 0 7 -1 -1 33.43 32.91 0.42 o 0 7 -1 1 23.77 23.57 0.39 o 1 7 -1 -2 6.90 7.75 0.36 o 1 7 -1 0 30.81 30.49 0.41 o 1 7 -1 2 6.21 7.01 1.18 < 2 7 -1 -1 29.47 28.66 0.38 o 2 7 -1 1 22.51 22.27 0.44 o 3 7 -1 -2 4.94 5.94 0.53 o 3 7 -1 0 31.41 30.58 0.57 o 3 7 -1 2 3.08 7.07 2.16 < 4 7 -1 -1 19.67 20.36 0.56 o 4 7 -1 1 15.62 16.24 0.73 o 5 7 -1 -2 5.48 5.36 1.70 < -2 8 -1 -2 18.39 19.14 0.81 o -2 8 -1 0 168.00 169.80 1.81 o -2 8 -1 2 11.59 11.35 0.43 o -1 8 -1 -1 25.47 25.98 0.42 o -1 8 -1 1 8.60 8.79 0.37 o 0 8 -1 -2 23.00 23.12 0.39 o 0 8 -1 0 199.23 201.59 2.02 o 0 8 -1 2 11.11 11.16 0.40 o 1 8 -1 -1 27.61 26.97 0.38 o 1 8 -1 1 14.93 15.38 0.44 o 2 8 -1 -2 23.10 23.10 0.33 o 2 8 -1 0 170.58 169.83 1.75 o 2 8 -1 2 9.18 9.85 0.75 o 3 8 -1 -1 19.85 20.65 0.46 o 3 8 -1 1 13.73 14.31 0.62 o 4 8 -1 -2 19.25 19.10 0.47 o 4 8 -1 0 118.63 121.03 1.35 o 4 8 -1 2 10.55 8.62 0.96 o 5 8 -1 -1 17.30 13.91 0.67 o -2 9 -1 1 34.12 32.99 0.63 o -1 9 -1 -2 8.91 8.70 0.69 o -1 9 -1 0 20.70 20.09 0.40 o -1 9 -1 2 20.37 20.36 0.42 o 0 9 -1 -1 13.92 14.44 0.38 o 0 9 -1 1 30.03 29.81 0.45 o 1 9 -1 -2 10.17 10.49 0.34 o 1 9 -1 0 20.33 20.13 0.47 o 1 9 -1 2 18.92 18.02 0.79 o 2 9 -1 -1 8.22 9.40 0.49 o 2 9 -1 1 21.29 21.60 0.58 o 3 9 -1 -2 7.91 8.82 0.54 o 3 9 -1 0 16.67 18.77 0.60 o 3 9 -1 2 14.57 14.06 0.91 o 4 9 -1 -1 6.16 6.80 0.89 o 4 9 -1 1 14.07 15.38 0.88 o 5 9 -1 -2 5.00 6.49 1.14 < 5 9 -1 0 16.25 16.53 0.79 o -2 10 -1 2 21.58 21.94 0.49 o -1 10 -1 -1 30.49 28.88 0.64 o -1 10 -1 1 26.71 27.66 0.56 o 0 10 -1 -2 4.86 5.39 0.95 < 0 10 -1 0 26.45 26.47 0.51 o 0 10 -1 2 21.78 22.07 0.65 o 1 10 -1 -1 31.54 30.48 0.55 o 1 10 -1 1 28.15 26.96 0.69 o 2 10 -1 -2 3.02 5.33 1.26 < 2 10 -1 0 20.39 20.19 0.57 o 2 10 -1 2 17.25 19.00 0.64 o 3 10 -1 -1 25.82 26.05 0.50 o 3 10 -1 1 20.40 21.66 0.65 o 4 10 -1 -2 4.15 5.71 1.03 < 4 10 -1 0 12.45 13.10 0.71 o 4 10 -1 2 15.26 15.15 0.96 o 5 10 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-1 5.79 6.04 0.22 o 2 1 0 1 2.70 3.02 0.52 < 3 1 0 -2 3.24 3.59 0.33 o 3 1 0 0 20.45 19.66 0.43 o -4 2 0 2 4.30 5.63 0.90 < -3 2 0 1 4.87 4.65 0.47 o -2 2 0 -2 3.79 4.50 1.44 < -2 2 0 0 20.94 20.88 0.29 o -2 2 0 2 6.77 7.52 0.25 o -1 2 0 -1 14.71 14.73 0.23 o -1 2 0 1 12.26 12.10 0.21 o 0 2 0 -2 2.76 3.17 0.36 o 0 2 0 0 20.30 22.69 0.25 o 0 2 0 2 6.97 7.52 0.25 o 1 2 0 -1 8.62 8.43 0.19 o 1 2 0 1 19.12 19.13 0.27 o 2 2 0 -2 3.21 3.13 0.41 o 2 2 0 0 21.64 21.04 0.27 o 2 2 0 2 4.45 5.62 0.93 < 3 2 0 -1 2.47 2.53 0.57 < 3 2 0 1 14.06 13.67 0.46 o -3 3 0 0 109.00 106.60 1.17 o -3 3 0 2 8.53 8.96 0.35 o -2 3 0 -1 4.17 3.99 0.41 o -2 3 0 1 11.79 11.52 0.30 o -1 3 0 -2 5.44 5.70 0.30 o -1 3 0 0 142.68 139.66 1.43 o -1 3 0 2 9.25 9.52 0.25 o 0 3 0 -1 12.54 12.15 0.22 o 0 3 0 1 6.33 6.04 0.28 o 1 3 0 -2 5.23 5.06 0.24 o 1 3 0 0 140.72 139.45 1.42 o 1 3 0 2 8.23 8.58 0.29 o 2 3 0 -1 18.89 19.39 0.28 o 2 3 0 1 2.90 2.37 0.74 < 3 3 0 -2 6.07 5.57 0.28 o 3 3 0 0 109.48 106.16 1.15 o 3 3 0 2 6.28 7.60 0.90 o -4 4 0 2 8.29 8.18 0.76 o -3 4 0 1 13.46 13.79 0.50 o -2 4 0 -2 5.73 5.76 0.67 o -2 4 0 0 143.89 138.84 1.46 o -2 4 0 2 9.27 9.55 0.24 o -1 4 0 -1 11.16 11.22 0.23 o -1 4 0 1 17.95 17.82 0.27 o 0 4 0 -2 6.70 7.53 0.27 o 0 4 0 0 168.23 171.26 1.70 o 0 4 0 2 9.36 9.40 0.28 o 1 4 0 -1 5.82 5.88 0.34 o 1 4 0 1 18.44 17.91 0.27 o 2 4 0 -2 7.01 7.53 0.27 o 2 4 0 0 142.69 139.31 1.44 o 2 4 0 2 7.64 7.99 0.72 o 3 4 0 -1 1.10 2.74 1.87 < 3 4 0 1 13.43 13.99 0.61 o 4 4 0 -2 4.59 5.77 0.82 < 4 4 0 0 97.75 99.55 1.07 o -3 5 0 0 34.38 33.31 0.50 o -3 5 0 2 12.87 13.62 0.30 o -2 5 0 -1 13.84 13.80 0.36 o -2 5 0 1 19.23 19.16 0.27 o -1 5 0 -2 8.57 9.04 0.29 o -1 5 0 0 26.94 28.39 0.35 o -1 5 0 2 17.30 17.02 0.28 o 0 5 0 -1 17.77 17.56 0.29 o 0 5 0 1 19.00 18.67 0.29 o 1 5 0 -2 9.25 9.54 0.26 o 1 5 0 0 27.24 28.35 0.37 o 1 5 0 2 13.46 13.81 0.29 o 2 5 0 -1 18.02 17.55 0.30 o 2 5 0 1 13.87 13.39 0.37 o 3 5 0 -2 7.90 8.67 0.30 o 3 5 0 0 35.19 33.24 0.47 o 3 5 0 2 8.65 9.68 0.84 o 4 5 0 -1 12.82 13.76 0.61 o 4 5 0 1 8.92 9.32 0.71 o -3 6 0 1 10.59 10.59 0.45 o -2 6 0 -2 6.92 7.94 0.91 o -2 6 0 0 70.64 70.05 0.74 o -2 6 0 2 1.52 2.48 1.15 < -1 6 0 -1 19.05 18.91 0.29 o -1 6 0 1 11.53 11.29 0.28 o 0 6 0 -2 9.45 9.50 0.30 o 0 6 0 0 86.48 84.94 0.90 o 0 6 0 2 2.24 2.45 0.87 < 1 6 0 -1 18.68 18.26 0.33 o 1 6 0 1 6.84 6.59 0.31 o 2 6 0 -2 9.62 9.35 0.30 o 2 6 0 0 71.06 70.04 0.75 o 2 6 0 2 0.00 4.51 18.97 < 3 6 0 -1 12.99 12.97 0.34 o 3 6 0 1 2.30 2.95 2.58 < 4 6 0 -2 8.64 7.74 0.53 o 4 6 0 0 50.78 52.06 0.77 o 4 6 0 2 2.26 5.44 2.86 < 5 6 0 -1 9.07 8.96 0.64 o -3 7 0 2 24.73 22.66 0.85 o -2 7 0 -1 10.12 10.30 0.60 o -2 7 0 1 24.87 24.16 0.34 o -1 7 0 -2 12.89 13.26 0.31 o -1 7 0 0 163.14 162.06 1.65 o -1 7 0 2 27.19 25.95 0.37 o 0 7 0 -1 10.88 11.08 0.38 o 0 7 0 1 24.00 23.45 0.34 o 1 7 0 -2 16.60 16.56 0.31 o 1 7 0 0 162.99 161.86 1.65 o 1 7 0 2 21.97 22.32 0.76 o 2 7 0 -1 6.83 6.55 0.38 o 2 7 0 1 17.98 18.30 0.52 o 3 7 0 -2 13.18 13.46 0.31 o 3 7 0 0 124.56 123.30 1.32 o 3 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9 0 0 68.45 68.56 0.85 o 3 9 0 2 5.09 7.94 1.85 < 4 9 0 -1 18.69 18.88 0.58 o 4 9 0 1 8.74 8.31 1.08 o 5 9 0 -2 17.10 17.13 0.77 o 5 9 0 0 52.04 53.33 0.85 o -2 10 0 2 15.95 15.86 0.46 o -1 10 0 -1 4.21 1.25 0.94 < -1 10 0 1 18.97 18.87 0.42 o 0 10 0 -2 13.21 12.56 0.40 o 0 10 0 0 76.94 75.87 0.85 o 0 10 0 2 15.45 15.61 0.67 o 1 10 0 -1 3.44 4.42 0.95 < 1 10 0 1 21.20 21.39 0.56 o 2 10 0 -2 12.82 12.62 0.47 o 2 10 0 0 69.22 68.33 0.98 o 2 10 0 2 13.28 13.90 0.71 o 3 10 0 -1 7.98 8.14 0.74 o 3 10 0 1 18.57 18.46 0.87 o 4 10 0 -2 11.55 11.19 0.65 o 4 10 0 0 53.53 54.38 0.92 o 4 10 0 2 15.35 11.79 1.02 o 5 10 0 -1 6.53 7.97 1.26 < 5 10 0 1 11.76 13.91 0.98 o 6 10 0 -2 12.32 9.11 0.87 o -1 11 0 0 61.43 59.79 0.72 o 0 11 0 -1 19.60 19.20 0.55 o 0 11 0 1 38.03 36.44 0.71 o 1 11 0 -2 9.86 10.91 0.49 o 1 11 0 0 60.29 59.95 0.84 o 1 11 0 2 23.77 23.92 0.88 o 2 11 0 -1 21.78 21.98 0.70 o 2 11 0 1 31.18 31.43 0.85 o 3 11 0 -2 8.85 9.79 0.70 o 3 11 0 0 47.77 49.18 0.73 o 3 11 0 2 17.26 17.71 0.98 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1.04 o 4 17 0 1 19.17 19.85 1.23 o 5 17 0 -2 14.06 13.74 0.92 o 5 17 0 0 11.28 8.62 1.44 o 2 18 0 2 25.22 26.38 0.86 o 3 18 0 -1 22.46 23.17 0.78 o 3 18 0 1 28.01 26.47 0.84 o 4 18 0 -2 7.95 6.52 1.20 o 4 18 0 0 5.22 5.28 2.79 < 5 18 0 -1 21.02 19.53 1.21 o 3 19 0 0 50.81 51.14 0.90 o 3 19 0 2 12.17 9.42 1.64 o 4 19 0 -1 26.51 26.64 0.82 o 5 19 0 -2 18.81 14.74 0.93 o 2 20 0 2 0.00 7.22 30.86 < 3 20 0 -1 6.82 6.54 2.05 < 3 20 0 1 16.50 15.88 0.95 o 4 20 0 -2 24.44 25.79 0.84 o 4 20 0 0 6.62 3.41 2.83 < 2 21 0 1 20.75 22.59 1.23 o 3 21 0 -2 9.48 8.73 1.66 < 3 21 0 0 21.12 17.74 0.93 o 4 21 0 -1 16.39 15.77 1.02 o 5 21 0 -2 8.76 9.11 1.67 < 3 22 0 -1 22.39 22.35 1.28 o 4 22 0 -2 6.20 7.12 2.27 < 3 23 0 -2 24.14 27.07 1.28 o 1 -1 1 2 3.41 4.41 0.47 o -4 0 1 2 5.64 5.39 1.04 < -3 0 1 1 5.16 5.41 0.32 o -2 0 1 2 6.95 6.87 0.29 o -1 0 1 1 6.91 6.89 0.28 o 0 0 1 2 6.86 6.75 0.29 o 1 0 1 1 6.63 7.00 0.28 o 2 0 1 0 5.68 5.57 0.23 o 2 0 1 2 5.83 5.19 1.02 < 3 0 1 1 4.44 4.90 0.57 o -3 1 1 0 127.50 124.61 1.35 o -3 1 1 2 5.10 5.27 0.32 o -2 1 1 -1 3.54 3.49 0.47 o -2 1 1 1 14.46 14.54 0.25 o -1 1 1 0 178.00 173.98 1.79 o -1 1 1 2 5.61 5.69 0.33 o 0 1 1 -1 3.19 2.97 0.25 o 0 1 1 1 14.39 14.09 0.24 o 1 1 1 0 177.02 174.10 1.78 o 1 1 1 2 4.92 5.43 0.38 o 2 1 1 -1 7.36 7.08 0.21 o 2 1 1 1 10.11 9.77 0.28 o 3 1 1 -2 3.65 3.38 0.29 o 3 1 1 0 130.50 124.84 1.36 o 3 1 1 2 4.38 5.05 0.98 < -4 2 1 2 5.98 8.03 1.41 < -3 2 1 1 10.81 10.67 0.23 o -2 2 1 -2 4.11 2.13 1.72 < -2 2 1 0 75.07 75.69 0.78 o -2 2 1 2 7.13 8.00 0.28 o -1 2 1 -1 13.92 14.10 0.26 o -1 2 1 1 10.55 10.57 0.24 o 0 2 1 -2 2.12 1.55 0.50 < 0 2 1 0 91.43 91.16 0.93 o 0 2 1 2 6.86 7.68 0.29 o 1 2 1 -1 6.62 6.74 0.17 o 1 2 1 1 5.42 6.02 0.28 o 2 2 1 -2 1.67 1.53 0.54 < 2 2 1 0 77.05 75.48 0.80 o 2 2 1 2 5.50 7.59 0.88 o 3 2 1 -1 2.35 1.42 0.66 < 3 2 1 1 3.24 3.49 1.23 < 4 2 1 -2 1.92 2.11 1.48 < 4 2 1 0 54.98 59.52 0.63 o -3 3 1 0 60.57 58.56 0.71 o -3 3 1 2 9.73 10.18 0.33 o -2 3 1 -1 6.45 7.02 0.39 o -2 3 1 1 15.48 16.35 0.27 o -1 3 1 -2 2.21 2.09 0.88 < -1 3 1 0 74.37 74.48 0.77 o -1 3 1 2 11.83 12.30 0.27 o 0 3 1 -1 12.03 11.84 0.24 o 0 3 1 1 12.63 12.68 0.24 o 1 3 1 -2 1.82 1.69 0.41 < 1 3 1 0 74.09 74.60 0.76 o 1 3 1 2 9.92 10.14 0.27 o 2 3 1 -1 14.14 13.84 0.26 o 2 3 1 1 12.78 12.61 0.34 o 3 3 1 -2 1.70 2.02 0.70 < 3 3 1 0 60.79 58.81 0.70 o 3 3 1 2 8.52 7.42 0.84 o 4 3 1 -1 9.95 9.92 0.53 o 4 3 1 1 9.50 10.33 0.56 o -3 4 1 1 4.59 5.61 0.86 < -2 4 1 -2 6.60 8.97 1.10 o -2 4 1 0 154.57 152.51 1.57 o -2 4 1 2 2.19 3.42 0.91 < -1 4 1 -1 20.55 20.25 0.33 o -1 4 1 1 7.99 8.29 0.27 o 0 4 1 -2 8.63 9.40 0.19 o 0 4 1 0 181.25 187.53 1.82 o 0 4 1 2 2.35 3.48 0.79 < 1 4 1 -1 17.82 17.53 0.26 o 1 4 1 1 16.15 15.91 0.26 o 2 4 1 -2 8.99 9.16 0.27 o 2 4 1 0 155.78 152.15 1.57 o 2 4 1 2 0.77 3.97 7.62 < 3 4 1 -1 10.10 9.94 0.32 o 3 4 1 1 15.32 15.71 0.70 o 4 4 1 -2 7.94 8.48 0.62 o 4 4 1 0 106.92 106.41 1.19 o 4 4 1 2 1.58 3.97 3.54 < -3 5 1 0 108.76 105.58 1.20 o -3 5 1 2 6.60 6.08 0.68 o -2 5 1 -1 3.83 3.93 1.14 < -2 5 1 1 19.39 19.48 0.31 o -1 5 1 -2 10.09 9.82 0.37 o -1 5 1 0 151.88 149.47 1.53 o -1 5 1 2 7.55 8.10 0.32 o 0 5 1 -1 6.02 6.29 0.30 o 0 5 1 1 22.54 22.28 0.32 o 1 5 1 -2 12.69 12.79 0.23 o 1 5 1 0 152.31 149.51 1.54 o 1 5 1 2 5.27 6.24 0.87 o 2 5 1 -1 8.89 8.84 0.26 o 2 5 1 1 16.52 16.90 0.50 o 3 5 1 -2 9.86 9.68 0.29 o 3 5 1 0 107.68 105.84 1.16 o 3 5 1 2 4.21 5.47 1.45 < 4 5 1 -1 6.36 6.44 0.90 o 4 5 1 1 11.32 11.50 0.69 o 5 5 1 -2 7.04 6.70 0.72 o -3 6 1 1 27.96 26.63 0.93 o -2 6 1 0 58.15 57.89 0.62 o -2 6 1 2 22.81 22.96 0.38 o -1 6 1 -1 12.56 12.72 0.24 o -1 6 1 1 33.32 32.69 0.40 o 0 6 1 -2 1.79 1.19 0.75 < 0 6 1 0 73.43 72.13 0.77 o 0 6 1 2 22.91 22.93 0.34 o 1 6 1 -1 17.48 17.11 0.28 o 1 6 1 1 29.54 28.53 0.38 o 2 6 1 -2 0.55 1.26 3.29 < 2 6 1 0 59.21 57.56 0.65 o 2 6 1 2 19.28 19.17 0.81 o 3 6 1 -1 13.70 14.49 0.37 o 3 6 1 1 19.04 20.30 0.76 o 4 6 1 -2 0.00 2.62 13.78 < 4 6 1 0 40.78 40.62 0.76 o 4 6 1 2 14.96 15.25 0.83 o 5 6 1 -1 9.49 9.72 0.76 o -3 7 1 2 9.88 8.35 1.22 o -2 7 1 -1 32.04 30.63 0.51 o -2 7 1 1 26.75 26.02 0.39 o -1 7 1 -2 8.99 9.92 0.27 o -1 7 1 0 31.41 31.06 0.40 o -1 7 1 2 9.48 10.14 0.33 o 0 7 1 -1 36.06 34.69 0.42 o 0 7 1 1 27.69 26.66 0.38 o 1 7 1 -2 9.88 9.32 0.27 o 1 7 1 0 31.33 30.91 0.40 o 1 7 1 2 7.40 8.47 1.14 o 2 7 1 -1 26.39 25.36 0.35 o 2 7 1 1 19.93 20.12 0.78 o 3 7 1 -2 8.92 9.54 0.30 o 3 7 1 0 31.79 30.58 0.75 o 3 7 1 2 5.88 6.17 1.51 < 4 7 1 -1 16.04 16.40 0.73 o 4 7 1 1 12.42 13.41 0.86 o 5 7 1 -2 8.98 9.43 0.83 o 5 7 1 0 26.69 26.62 0.67 o -3 8 1 1 14.63 14.48 1.06 o -2 8 1 2 5.16 5.56 0.68 o -1 8 1 -1 16.28 16.40 0.29 o -1 8 1 1 14.63 14.64 0.30 o 0 8 1 -2 23.10 22.69 0.32 o 0 8 1 0 202.91 203.48 2.04 o 0 8 1 2 4.02 5.50 0.96 < 1 8 1 -1 24.66 23.85 0.35 o 1 8 1 1 8.80 9.55 0.49 o 2 8 1 -2 23.54 22.54 0.35 o 2 8 1 0 172.99 171.49 1.85 o 2 8 1 2 4.90 5.81 1.78 < 3 8 1 -1 23.22 22.60 0.53 o 3 8 1 1 5.49 7.00 1.43 < 4 8 1 -2 16.11 15.67 0.53 o 4 8 1 0 123.30 122.24 1.42 o 4 8 1 2 2.76 5.97 3.23 < 5 8 1 -1 15.94 16.56 0.79 o 5 8 1 1 4.73 6.43 1.86 < -2 9 1 1 29.24 28.35 0.45 o -1 9 1 -2 6.12 6.71 0.46 o -1 9 1 0 17.76 17.88 0.36 o -1 9 1 2 17.54 16.94 0.94 o 0 9 1 -1 8.23 8.27 0.32 o 0 9 1 1 32.22 30.44 0.49 o 1 9 1 -2 6.55 6.52 0.36 o 1 9 1 0 17.54 17.92 0.39 o 1 9 1 2 15.96 16.15 0.90 o 2 9 1 -1 15.99 14.93 0.45 o 2 9 1 1 27.46 26.41 0.82 o 3 9 1 -2 5.31 6.94 1.38 < 3 9 1 0 17.41 17.54 0.83 o 3 9 1 2 14.35 14.01 0.98 o 4 9 1 -1 13.30 14.03 0.88 o 4 9 1 1 20.18 20.11 0.88 o 5 9 1 -2 4.72 7.30 1.50 < 5 9 1 0 16.24 15.93 0.84 o -2 10 1 0 19.39 18.10 1.02 o -2 10 1 2 24.59 24.42 0.57 o -1 10 1 -1 33.76 32.83 0.46 o -1 10 1 1 36.26 34.94 0.58 o 0 10 1 -2 10.95 10.75 0.34 o 0 10 1 0 24.15 24.11 0.42 o 0 10 1 2 24.69 24.58 0.69 o 1 10 1 -1 31.06 29.84 0.42 o 1 10 1 1 34.92 33.43 0.83 o 2 10 1 -2 11.14 10.56 0.36 o 2 10 1 0 17.83 17.98 0.82 o 2 10 1 2 17.52 19.55 0.92 o 3 10 1 -1 22.28 21.81 0.79 o 3 10 1 1 26.37 26.06 0.88 o 4 10 1 -2 9.13 9.56 0.71 o 4 10 1 0 11.85 11.59 1.01 o 4 10 1 2 12.70 14.39 1.08 o 5 10 1 -1 14.15 15.62 0.87 o 5 10 1 1 17.64 18.87 0.95 o 6 10 1 -2 10.13 8.53 1.00 o -1 11 1 0 118.00 116.73 1.24 o 0 11 1 -1 29.40 28.11 0.46 o 0 11 1 1 13.75 13.87 1.04 o 1 11 1 -2 19.69 20.00 0.39 o 1 11 1 0 118.27 116.56 1.33 o 1 11 1 2 7.41 7.31 1.47 < 2 11 1 -1 30.35 27.46 1.01 o 2 11 1 1 12.51 12.12 1.05 o 3 11 1 -2 17.54 17.65 0.80 o 3 11 1 0 91.34 93.02 1.20 o 3 11 1 2 11.48 6.48 1.22 o 4 11 1 -1 21.82 22.10 0.84 o 4 11 1 1 9.66 10.04 1.27 o 5 11 1 -2 15.15 13.68 0.87 o 5 11 1 0 68.27 68.52 1.06 o 6 11 1 -1 15.52 16.22 0.92 o 0 12 1 -2 21.64 21.46 0.44 o 1 12 1 -1 5.87 5.04 2.16 < 1 12 1 1 26.96 25.82 0.89 o 2 12 1 -2 20.77 21.59 0.64 o 2 12 1 0 56.41 56.74 0.96 o 2 12 1 2 8.69 9.07 1.38 o 3 12 1 -1 2.10 2.88 3.79 < 3 12 1 1 21.74 21.93 0.95 o 4 12 1 -2 17.58 18.62 0.64 o 4 12 1 0 46.09 46.13 0.98 o 4 12 1 2 9.59 7.83 1.52 o 5 12 1 -1 2.65 1.99 3.48 < 5 12 1 1 15.75 16.95 1.09 o 6 12 1 -2 19.90 14.85 0.92 o 1 13 1 -2 11.53 13.03 1.28 o 1 13 1 2 26.07 26.92 0.98 o 2 13 1 -1 23.86 25.13 0.87 o 2 13 1 1 23.66 22.60 0.97 o 3 13 1 0 30.52 31.14 0.92 o 3 13 1 2 22.24 21.88 1.05 o 4 13 1 -1 19.34 19.91 0.99 o 4 13 1 1 17.30 17.70 1.07 o 5 13 1 -2 18.15 11.11 0.95 o 5 13 1 0 24.36 24.00 0.99 o 6 13 1 -1 15.39 15.02 1.08 o 2 14 1 -2 19.52 19.42 0.86 o 2 14 1 0 29.03 28.74 0.91 o 2 14 1 2 8.68 8.87 1.53 < 3 14 1 -1 28.60 29.90 0.92 o 3 14 1 1 9.97 10.32 1.43 o 4 14 1 -2 15.06 16.08 0.74 o 4 14 1 0 24.87 24.33 1.04 o 4 14 1 2 15.56 9.15 1.29 o 5 14 1 -1 23.61 23.50 0.99 o 5 14 1 1 11.14 7.88 1.47 o 6 14 1 -2 17.19 12.22 1.12 o 2 15 1 -1 8.35 8.49 1.30 o 2 15 1 1 22.12 19.93 1.03 o 3 15 1 -2 22.30 23.39 0.93 o 3 15 1 0 73.26 72.57 1.16 o 3 15 1 2 10.27 12.60 1.43 o 4 15 1 -1 6.02 6.58 1.81 < 4 15 1 1 16.34 16.13 1.29 o 5 15 1 -2 18.42 19.45 1.04 o 5 15 1 0 59.15 56.93 1.13 o 6 15 1 -1 9.40 5.02 1.58 < 2 16 1 0 33.88 33.78 1.00 o 2 16 1 2 18.76 18.50 1.17 o 3 16 1 -1 22.43 22.60 1.02 o 3 16 1 1 27.10 28.18 1.12 o 4 16 1 -2 11.33 9.12 0.92 o 4 16 1 0 25.12 26.45 1.11 o 5 16 1 -1 19.18 19.33 1.16 o 6 16 1 -2 7.42 9.04 1.84 < 2 17 1 1 14.91 14.78 1.24 o 3 17 1 0 26.09 26.79 1.01 o 3 17 1 2 19.74 18.67 1.27 o 4 17 1 -1 22.05 21.78 0.80 o 4 17 1 1 11.59 11.72 1.69 o 5 17 1 -2 16.20 16.96 1.15 o 2 18 1 2 23.52 9.59 1.28 o 3 18 1 -1 25.45 16.89 1.07 o 3 18 1 1 13.57 13.69 1.55 o 4 18 1 -2 16.98 17.86 0.84 o 4 18 1 0 28.96 27.19 1.16 o 5 18 1 -1 20.39 14.74 1.22 o 6 18 1 -2 17.16 14.52 1.27 o 3 19 1 0 27.82 20.33 1.15 o 3 19 1 2 17.21 17.74 1.32 o 4 19 1 -1 9.44 11.37 1.35 o 5 19 1 -2 16.27 17.59 1.25 o 3 20 1 1 19.84 18.97 1.38 o 4 20 1 -2 26.41 12.89 0.84 o 4 20 1 0 41.83 40.18 1.18 o 3 21 1 0 7.92 9.33 2.38 < 4 21 1 -1 19.13 17.46 0.93 o 5 21 1 -2 15.15 16.79 1.43 o 4 22 1 -2 17.38 17.85 0.92 o -1 -1 2 2 6.98 8.98 0.55 o 1 -1 2 2 5.51 6.82 0.66 o 3 -1 2 2 4.49 4.30 1.02 < -4 0 2 2 4.46 6.82 1.29 < -3 0 2 1 18.35 21.25 0.38 o -2 0 2 2 6.16 6.15 0.41 o -1 0 2 1 23.61 24.14 0.34 o 0 0 2 0 187.66 204.47 1.90 o 0 0 2 2 5.45 6.39 0.43 o 1 0 2 1 15.47 16.68 0.28 o 2 0 2 0 176.96 173.41 1.78 o 2 0 2 2 6.78 7.24 0.89 o 3 0 2 1 11.56 11.63 0.63 o -4 1 2 1 2.88 3.02 1.25 < -3 1 2 0 45.61 48.87 0.68 o -3 1 2 2 8.52 8.25 0.67 o -2 1 2 -1 14.21 13.94 0.26 o -2 1 2 1 5.81 5.89 0.37 o -1 1 2 0 72.12 70.77 0.75 o -1 1 2 2 8.44 8.09 0.35 o 0 1 2 -1 14.16 13.64 0.26 o 0 1 2 1 11.52 12.05 0.30 o 1 1 2 -2 2.49 2.96 0.70 < 1 1 2 0 72.70 70.98 0.76 o 1 1 2 2 6.80 8.10 0.50 o 2 1 2 -1 9.99 10.37 0.25 o 2 1 2 1 11.58 11.86 0.36 o 3 1 2 -2 2.35 2.79 0.51 < 3 1 2 0 49.26 49.30 0.65 o 3 1 2 2 7.99 8.01 0.90 o 4 1 2 -1 7.61 7.90 0.52 o -3 2 2 1 19.28 20.49 0.46 o -2 2 2 -2 5.43 6.00 1.22 < -2 2 2 0 12.68 12.64 0.30 o -2 2 2 2 11.96 12.51 0.30 o -1 2 2 -1 9.03 9.09 0.25 o -1 2 2 1 20.51 20.59 0.32 o 0 2 2 -2 7.13 6.25 0.28 o 0 2 2 0 18.60 17.20 0.29 o 0 2 2 2 12.16 12.53 0.30 o 1 2 2 -1 4.36 4.66 0.39 o 1 2 2 1 11.95 12.92 0.27 o 2 2 2 -2 5.50 6.10 0.27 o 2 2 2 0 12.68 12.38 0.26 o 3 2 2 -1 5.40 4.77 0.41 o 3 2 2 1 8.06 7.74 0.95 o 4 2 2 -2 5.57 5.65 0.82 o 4 2 2 0 15.52 15.17 0.58 o -3 3 2 0 135.95 133.80 1.61 o -3 3 2 2 7.05 6.48 0.79 o -2 3 2 -1 4.48 4.33 0.43 o -2 3 2 1 18.18 18.13 0.35 o -1 3 2 -2 3.83 4.24 0.33 o -1 3 2 0 191.93 190.40 1.93 o -1 3 2 2 7.50 7.27 0.34 o 0 3 2 -1 7.86 8.46 0.26 o 0 3 2 1 20.23 20.64 0.31 o 1 3 2 -2 5.86 6.16 0.25 o 1 3 2 0 191.28 190.16 1.92 o 1 3 2 2 6.32 6.60 0.68 o 2 3 2 -1 13.24 14.48 0.24 o 2 3 2 1 16.95 17.17 0.43 o 3 3 2 -2 3.38 4.11 0.46 o 3 3 2 0 138.09 133.34 1.43 o 3 3 2 2 4.27 6.44 1.79 <