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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_global _audit_creation_method 'Jana2006 Version : 17/11/2015' _journal_name_full 'American Mineralogist' _journal_year 2017 _journal_volume 102 _journal_page_first 21 _journal_page_last 32 _journal_paper_doi https://doi.org/10.2138/am-2017-5807 _publ_contact_author_name 'Xu, Huifang' _publ_contact_author_address ;NASA Astrobiology Institute Department of Geoscience University of Wisconsin-Madison Madison Wisconsin 53706 USA ; _publ_contact_author_email hfxu@geology.wisc.edu _publ_contact_author_phone '608-265-5887 (O)' _publ_requested_journal 'American Mineralogist' _publ_requested_category FA _publ_section_title ;Solved: The enigma of labradorite feldspar with incommensurately modulated structure ; loop_ _publ_author_name _publ_author_address 'Jin, Shiyun' ;NASA Astrobiology Institute Department of Geoscience University of Wisconsin-Madison Madison Wisconsin 53706 USA ; 'Xu, Huifang' ;NASA Astrobiology Institute Department of Geoscience University of Wisconsin-Madison Madison Wisconsin 53706 USA ; _publ_section_references ; Petricek, V., Dusek, M. & Palatinus L. (2014). Z. Kristallogr. 229(5), 345-352. Palatinus L. & Chapuis G. (2007). J. Appl. Cryst. 40, 786-790. ; data_I_Modulated_Structure _exptl_crystal_type_of_structure mod _chemical_name_common labradorite_An51 _chemical_formula_sum 'Ca0.518 Na0.482 Al1.518 Si2.482 O8' _chemical_compound_source 'Augusta, Maine' _chemical_formula_analytical An51 _chemical_formula_weight 270.5 _space_group_crystal_system triclinic _chemical_absolute_configuration ? _space_group_ssg_name X-1(\a\b\g)0 loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,-x2,-x3,-x4 3 x1,x2,x3+1/2,x4+1/2 4 -x1,-x2,-x3+1/2,-x4+1/2 5 x1+1/2,x2+1/2,x3,x4+1/2 6 -x1+1/2,-x2+1/2,-x3,-x4+1/2 7 x1+1/2,x2+1/2,x3+1/2,x4 8 -x1+1/2,-x2+1/2,-x3+1/2,-x4 _cell_length_a 8.1668(10) _cell_length_b 12.8509(10) _cell_length_c 14.2086(2) _cell_angle_alpha 93.5802(6) _cell_angle_beta 116.23(9) _cell_angle_gamma 89.8396(13) _cell_volume 1334.53(3) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.06707 0.05463 -0.23038 _cell_formula_units_Z 8 _cell_measurement_temperature 293 _exptl_crystal_density_diffrn 2.6927 _exptl_crystal_F_000 1073 _exptl_absorpt_coefficient_mu 1.26 _exptl_crystal_description 'irragular shaped' _exptl_crystal_colour colorless _diffrn_ambient_temperature 293 _exptl_crystal_size_max 0.153 _exptl_crystal_size_mid 0.059 _exptl_crystal_size_min 0.058 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details 'Gaussian integration method' _exptl_absorpt_correction_T_min 0.9252 _exptl_absorpt_correction_T_max 0.9582 _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'Bruker Microfocus' _diffrn_source_power 0.03 _diffrn_source_voltage 50 _diffrn_source_current 0.6 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker CCD' _diffrn_detector ApexII _diffrn_reflns_number 40659 _diffrn_reflns_theta_min 1.94 _diffrn_reflns_theta_max 30.54 _diffrn_reflns_theta_full 30.54 _diffrn_measured_fraction_theta_max 1 _diffrn_measured_fraction_theta_full 1 _diffrn_reflns_av_R_equivalents 0.0429 _diffrn_reflns_av_unetI/netI 0.0232 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_index_m_1_min -2 _diffrn_reflns_limit_index_m_1_max 2 _reflns_number_total 10168 _reflns_number_gt 5124 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0235 _refine_ls_wR_factor_gt 0.0696 _refine_ls_R_factor_all 0.0478 _refine_ls_wR_factor_ref 0.0718 _refine_ls_goodness_of_fit_ref 1.28 _refine_ls_goodness_of_fit_gt 1.8 _refine_ls_number_reflns 10168 _refine_ls_number_parameters 642 _refine_ls_number_constraints 250 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(I)+0.0004I^2^) _refine_ls_shift/su_max 0.0388 _refine_ls_shift/su_mean 0.0034 _refine_ls_extinction_method 'B-C type 2 (Becker & Coppens, 1974)' _refine_ls_extinction_coef -11300(255) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Al 0.0645 0.0514 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Ca 0.2262 0.3064 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Na 0.0362 0.0249 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.006 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Si 0.0817 0.0704 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group M2ca Ca 0.2705(2) 0.0274(2) 0.04913(16) Uani 0.0258(6) 8 0.361(10) d ? ? ? M1ca Ca 0.2684(2) -0.0116(4) 0.0794(4) Uani 0.0302(7) 8 0.158(10) d ? ? ? M1na Na 0.2684(2) -0.0116(4) 0.0794(4) Uani 0.0302(7) 8 0.482(14) d ? ? ? T1osi Si 0.49386(3) 0.335593(18) -0.107001(18) Uani 0.01011(8) 8 0.4069 d ? ? ? T1msi Si 0.50319(3) 0.317714(17) 0.116018(17) Uani 0.00995(8) 8 0.6967 d ? ? ? T2osi Si 0.68554(3) 0.109339(17) 0.158333(18) Uani 0.00992(8) 8 0.7158 d ? ? ? T2msi Si 0.18169(3) 0.37949(17) 0.178604(17) Uani 0.00979(8) 8 0.6626 d ? ? ? T1oal Al 0.49386(3) 0.335593(18) -0.107001(18) Uani 0.01011(8) 8 0.5931 d ? ? ? T1mal Al 0.50319(3) 0.317714(17) 0.116018(17) Uani 0.00995(8) 8 0.3033 d ? ? ? T2oal Al 0.68554(3) 0.109339(17) 0.158333(18) Uani 0.00992(8) 8 0.2842 d ? ? ? T2mal Al 0.18169(3) 0.37949(17) 0.178604(17) Uani 0.00979(8) 8 0.3374 d ? ? ? Odm O 0.68998(8) 0.36705(5) 0.21565(5) Uani 0.021(2) 8 1 d ? ? ? Oa2 O 0.58107(8) -0.00691(4) 0.13907(5) Uani 0.0135(2) 8 1 d ? ? ? Odo O 0.30165(8) 0.39258(5) 0.30849(5) Uani 0.0173(2) 8 1 d ? ? ? Oa1 O 0.49797(8) 0.37147(5) 0.01117(5) Uani 0.0183(2) 8 1 d ? ? ? Obm O 0.31664(8) 0.35355(5) 0.12255(6) Uani 0.0242(3) 8 1 d ? ? ? Obo O 0.81163(8) 0.10554(5) 0.09434(5) Uani 0.0181(2) 8 1 d ? ? ? Ocm O 0.51474(8) 0.18895(5) 0.1077(5) Uani 0.0179(2) 8 1 d ? ? ? Oco O 0.48585(8) 0.20771(5) -0.13984(5) Uani 0.0177(2) 8 1 d ? ? ? loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 M2ca Ca 0.0147(5) 0.0345(12) 0.0217(7) 0.0057(5) 0.0035(4) -0.0091(7) M1ca Ca 0.01(4) 0.0494(13) 0.0257(11) -0.004(5) 0.0061(4) -0.0221(9) M1na Na 0.01(4) 0.0494(13) 0.0257(11) -0.004(5) 0.0061(4) -0.0221(9) T1osi Si 0.0099(10) 0.01234(11) 0.00788(11) -0.00101(8) 0.00376(8) 0.00063(8) T1msi Si 0.01022(10) 0.01223(11) 0.00718(11) 0.00345(8) 0.00368(8) 0.00063(8) T2osi Si 0.00912(10) 0.00937(10) 0.01016(11) 0.00044(8) 0.00333(8) 0.00012(8) T2msi Si 0.00913(10) 0.01004(10) 0.00964(11) 0.00128(8) 0.00355(8) 0.00143(8) T1oal Al 0.0099(10) 0.01234(11) 0.00788(11) -0.00101(8) 0.00376(8) 0.00063(8) T1mal Al 0.01022(10) 0.01223(11) 0.00718(11) 0.00345(8) 0.00368(8) 0.00063(8) T2oal Al 0.00912(10) 0.00937(10) 0.01016(11) 0.00044(8) 0.00333(8) 0.00012(8) T2mal Al 0.00913(10) 0.01004(10) 0.00964(11) 0.00128(8) 0.00355(8) 0.00143(8) Odm O 0.0182(3) 0.0207(3) 0.0142(3) 0.0007(2) -0.0015(2) -0.0025(2) Oa2 O 0.0129(3) 0.012(3) 0.0139(3) 0.0007(2) 0.0043(2) 0.002(2) Odo O 0.0166(3) 0.0181(3) 0.0112(3) 0.0012(2) 0.0008(2) 0.001(2) Oa1 O 0.0259(3) 0.0215(3) 0.01(3) 0.0018(3) 0.0102(3) 0.0026(2) Obm O 0.0192(3) 0.0256(3) 0.0332(4) 0.0036(3) 0.017(3) -0.0012(3) Obo O 0.0175(3) 0.0167(3) 0.0235(3) -0.0029(2) 0.0125(3) -0.0011(2) Ocm O 0.0165(3) 0.0176(3) 0.0153(3) 0.005(2) 0.0035(2) -0.0009(2) Oco O 0.0169(3) 0.0173(3) 0.0186(3) -0.0022(2) 0.0077(3) -0.0001(2) loop_ _atom_site_Fourier_wave_vector_seq_id _jana_atom_site_Fourier_wave_vector_q1_coeff 1 1 2 2 loop_ _jana_atom_site_occ_Fourier_absolute_site_label _jana_atom_site_occ_Fourier_absolute M2ca 0.361(10) M1ca 0.158(10) M1na 0.482(14) T1osi 0.4069 T1msi 0.6967 T2osi 0.7158 T2msi 0.6626 T1oal 0.5931 T1mal 0.3033 T2oal 0.2842 T2mal 0.3374 loop_ _atom_site_occ_Fourier_id _atom_site_occ_Fourier_atom_site_label _atom_site_occ_Fourier_wave_vector_seq_id M2cao1 M2ca 1 M2cao2 M2ca 2 M1cao1 M1ca 1 M1cao2 M1ca 2 M1nao1 M1na 1 M1nao2 M1na 2 T1osio1 T1osi 1 T1osio2 T1osi 2 T1msio1 T1msi 1 T1msio2 T1msi 2 T2osio1 T2osi 1 T2osio2 T2osi 2 T2msio1 T2msi 1 T2msio2 T2msi 2 T1oalo1 T1oal 1 T1oalo2 T1oal 2 T1malo1 T1mal 1 T1malo2 T1mal 2 T2oalo1 T2oal 1 T2oalo2 T2oal 2 T2malo1 T2mal 1 T2malo2 T2mal 2 loop_ _atom_site_occ_Fourier_param_id _atom_site_occ_Fourier_param_cos _atom_site_occ_Fourier_param_sin M2cao1 0.129(10) -0.088(18) M2cao2 0.134(12) -0.023(9) M1cao1 -0.086(9) 0.044(19) M1cao2 -0.017(12) -0.024(10) M1nao1 -0.039(13) 0.05(3) M1nao2 -0.114(17) 0.062(14) T1osio1 0.4313 -0.0141 T1osio2 0.0736 -0.0318 T1msio1 -0.2986 0.2585 T1msio2 -0.0093 0.0982 T2osio1 0.3069 -0.0608 T2osio2 -0.0607 0.0232 T2msio1 0.3929 0.0862 T2msio2 -0.1019 -0.0441 T1oalo1 -0.4313 0.0141 T1oalo2 -0.0736 0.0318 T1malo1 0.2986 -0.2585 T1malo2 0.0093 -0.0982 T2oalo1 -0.3069 0.0608 T2oalo2 0.0607 -0.0232 T2malo1 -0.3929 -0.0862 T2malo2 0.1019 0.0441 loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id M2cax1 M2ca x 1 M2cay1 M2ca y 1 M2caz1 M2ca z 1 M2cax2 M2ca x 2 M2cay2 M2ca y 2 M2caz2 M2ca z 2 M1cax1 M1ca x 1 M1cay1 M1ca y 1 M1caz1 M1ca z 1 M1cax2 M1ca x 2 M1cay2 M1ca y 2 M1caz2 M1ca z 2 M1nax1 M1na x 1 M1nay1 M1na y 1 M1naz1 M1na z 1 M1nax2 M1na x 2 M1nay2 M1na y 2 M1naz2 M1na z 2 T1osix1 T1osi x 1 T1osiy1 T1osi y 1 T1osiz1 T1osi z 1 T1osix2 T1osi x 2 T1osiy2 T1osi y 2 T1osiz2 T1osi z 2 T1msix1 T1msi x 1 T1msiy1 T1msi y 1 T1msiz1 T1msi z 1 T1msix2 T1msi x 2 T1msiy2 T1msi y 2 T1msiz2 T1msi z 2 T2osix1 T2osi x 1 T2osiy1 T2osi y 1 T2osiz1 T2osi z 1 T2osix2 T2osi x 2 T2osiy2 T2osi y 2 T2osiz2 T2osi z 2 T2msix1 T2msi x 1 T2msiy1 T2msi y 1 T2msiz1 T2msi z 1 T2msix2 T2msi x 2 T2msiy2 T2msi y 2 T2msiz2 T2msi z 2 T1oalx1 T1oal x 1 T1oaly1 T1oal y 1 T1oalz1 T1oal z 1 T1oalx2 T1oal x 2 T1oaly2 T1oal y 2 T1oalz2 T1oal z 2 T1malx1 T1mal x 1 T1maly1 T1mal y 1 T1malz1 T1mal z 1 T1malx2 T1mal x 2 T1maly2 T1mal y 2 T1malz2 T1mal z 2 T2oalx1 T2oal x 1 T2oaly1 T2oal y 1 T2oalz1 T2oal z 1 T2oalx2 T2oal x 2 T2oaly2 T2oal y 2 T2oalz2 T2oal z 2 T2malx1 T2mal x 1 T2maly1 T2mal y 1 T2malz1 T2mal z 1 T2malx2 T2mal x 2 T2maly2 T2mal y 2 T2malz2 T2mal z 2 Odmx1 Odm x 1 Odmy1 Odm y 1 Odmz1 Odm z 1 Odmx2 Odm x 2 Odmy2 Odm y 2 Odmz2 Odm z 2 Oa2x1 Oa2 x 1 Oa2y1 Oa2 y 1 Oa2z1 Oa2 z 1 Oa2x2 Oa2 x 2 Oa2y2 Oa2 y 2 Oa2z2 Oa2 z 2 Odox1 Odo x 1 Odoy1 Odo y 1 Odoz1 Odo z 1 Odox2 Odo x 2 Odoy2 Odo y 2 Odoz2 Odo z 2 Oa1x1 Oa1 x 1 Oa1y1 Oa1 y 1 Oa1z1 Oa1 z 1 Oa1x2 Oa1 x 2 Oa1y2 Oa1 y 2 Oa1z2 Oa1 z 2 Obmx1 Obm x 1 Obmy1 Obm y 1 Obmz1 Obm z 1 Obmx2 Obm x 2 Obmy2 Obm y 2 Obmz2 Obm z 2 Obox1 Obo x 1 Oboy1 Obo y 1 Oboz1 Obo z 1 Obox2 Obo x 2 Oboy2 Obo y 2 Oboz2 Obo z 2 Ocmx1 Ocm x 1 Ocmy1 Ocm y 1 Ocmz1 Ocm z 1 Ocmx2 Ocm x 2 Ocmy2 Ocm y 2 Ocmz2 Ocm z 2 Ocox1 Oco x 1 Ocoy1 Oco y 1 Ocoz1 Oco z 1 Ocox2 Oco x 2 Ocoy2 Oco y 2 Ocoz2 Oco z 2 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin M2cax1 -0.00426(19) 0.0015(4) M2cay1 -0.00174(15) -0.007(3) M2caz1 0.00082(17) 0.001(3) M2cax2 0.0018(4) -0.0002(3) M2cay2 0.004(3) -0.0001(2) M2caz2 -0.0015(3) -0.0007(19) M1cax1 -0.0024(3) 0.0008(4) M1cay1 0.0047(8) -0.0284(7) M1caz1 -0.0049(5) 0.0116(8) M1cax2 -0.0018(3) -0.0029(3) M1cay2 -0.0056(6) 0.0004(7) M1caz2 0.0029(5) -0.0007(5) M1nax1 -0.0024(3) 0.0008(4) M1nay1 0.0047(8) -0.0284(7) M1naz1 -0.0049(5) 0.0116(8) M1nax2 -0.0018(3) -0.0029(3) M1nay2 -0.0056(6) 0.0004(7) M1naz2 0.0029(5) -0.0007(5) T1osix1 -0.00224(4) -0.00602(4) T1osiy1 0.00169(3) 0.00959(2) T1osiz1 0.00311(3) 0.00134(3) T1osix2 0.00025(7) -0.0023(7) T1osiy2 0.00118(4) 0.00021(4) T1osiz2 -0.00053(5) -0.00094(4) T1msix1 -0.0023(4) 0.00689(4) T1msiy1 -0.00078(2) 0.00912(2) T1msiz1 0.00286(2) -0.00099(2) T1msix2 -0.00003(7) -0.00159(7) T1msiy2 0.00009(4) -0.00046(4) T1msiz2 -0.00046(4) -0.00042(4) T2osix1 -0.00445(4) 0.00216(4) T2osiy1 -0.00256(2) 0.00586(2) T2osiz1 0.0008(2) -0.00184(2) T2osix2 -0.00079(7) -0.00181(7) T2osiy2 -0.00006(4) -0.00004(4) T2osiz2 0.0006(4) -0.0011(4) T2msix1 -0.00224(4) 0.00479(4) T2msiy1 0.00238(2) -0.00701(2) T2msiz1 0.00233(2) -0.00006(2) T2msix2 -0.00131(7) -0.0019(7) T2msiy2 -0.00065(4) 0.00007(4) T2msiz2 0.00003(4) -0.00038(4) T1oalx1 -0.00224(4) -0.00602(4) T1oaly1 0.00169(3) 0.00959(2) T1oalz1 0.00311(3) 0.00134(3) T1oalx2 0.00025(7) -0.0023(7) T1oaly2 0.00118(4) 0.00021(4) T1oalz2 -0.00053(5) -0.00094(4) T1malx1 -0.0023(4) 0.00689(4) T1maly1 -0.00078(2) 0.00912(2) T1malz1 0.00286(2) -0.00099(2) T1malx2 -0.00003(7) -0.00159(7) T1maly2 0.00009(4) -0.00046(4) T1malz2 -0.00046(4) -0.00042(4) T2oalx1 -0.00445(4) 0.00216(4) T2oaly1 -0.00256(2) 0.00586(2) T2oalz1 0.0008(2) -0.00184(2) T2oalx2 -0.00079(7) -0.00181(7) T2oaly2 -0.00006(4) -0.00004(4) T2oalz2 0.0006(4) -0.0011(4) T2malx1 -0.00224(4) 0.00479(4) T2maly1 0.00238(2) -0.00701(2) T2malz1 0.00233(2) -0.00006(2) T2malx2 -0.00131(7) -0.0019(7) T2maly2 -0.00065(4) 0.00007(4) T2malz2 0.00003(4) -0.00038(4) Odmx1 0.00732(10) 0.002(10) Odmy1 0.00165(6) 0.00922(6) Odmz1 0.00233(6) -0.00143(6) Odmx2 0.00015(17) -0.00158(17) Odmy2 -0.00054(9) -0.00095(9) Odmz2 -0.00044(10) -0.0018(10) Oa2x1 -0.00294(9) -0.00455(9) Oa2y1 0.00085(5) 0.00819(5) Oa2z1 0.00005(6) -0.00008(6) Oa2x2 -0.0032(16) -0.00174(15) Oa2y2 -0.00027(9) 0.00022(9) Oa2z2 -0.00005(10) -0.00172(10) Odox1 -0.008(10) 0.00494(10) Odoy1 0.0017(6) -0.00998(6) Odoz1 -0.00168(6) -0.00012(6) Odox2 -0.00062(16) -0.00403(17) Odoy2 0.00008(9) 0.00081(9) Odoz2 0.00127(10) -0.00008(10) Oa1x1 -0.0085(11) -0.00234(11) Oa1y1 -0.00106(6) 0.01413(6) Oa1z1 -0.00132(6) 0.00181(6) Oa1x2 0.00181(17) -0.00331(17) Oa1y2 0.00155(9) -0.00105(9) Oa1z2 -0.00065(10) -0.0005(10) Obmx1 -0.00214(11) 0.01079(11) Obmy1 -0.00124(6) -0.00081(6) Obmz1 0.00876(7) 0.00407(7) Obmx2 -0.00118(17) 0.00197(17) Obmy2 0.00136(9) -0.00134(10) Obmz2 -0.0017(11) 0.00182(11) Obox1 -0.00766(10) 0.00419(10) Oboy1 -0.00106(6) -0.00617(6) Oboz1 0.00317(6) -0.00038(6) Obox2 0.00117(17) -0.00331(16) Oboy2 -0.00191(9) 0.00122(9) Oboz2 0.00042(10) -0.00196(10) Ocmx1 0.00059(11) 0.01302(10) Ocmy1 -0.00422(6) 0.01234(6) Ocmz1 0.00282(6) -0.00538(6) Ocmx2 -0.00297(17) -0.0026(16) Ocmy2 -0.00055(9) 0.00032(9) Ocmz2 -0.0013(10) -0.00025(10) Ocox1 0.00181(10) -0.01117(10) Ocoy1 0.00612(6) 0.00975(6) Ocoz1 0.00449(6) 0.00201(6) Ocox2 0.00145(16) -0.0021(17) Ocoy2 0.00249(9) -0.00009(9) Ocoz2 0(10) -0.00148(10) loop_ _atom_site_U_Fourier_id _atom_site_U_Fourier_atom_site_label _atom_site_U_Fourier_tens_elem _atom_site_U_Fourier_wave_vector_seq_id M2caU111 M2ca U11 1 M2caU221 M2ca U22 1 M2caU331 M2ca U33 1 M2caU121 M2ca U12 1 M2caU131 M2ca U13 1 M2caU231 M2ca U23 1 M2caU112 M2ca U11 2 M2caU222 M2ca U22 2 M2caU332 M2ca U33 2 M2caU122 M2ca U12 2 M2caU132 M2ca U13 2 M2caU232 M2ca U23 2 M1caU111 M1ca U11 1 M1caU221 M1ca U22 1 M1caU331 M1ca U33 1 M1caU121 M1ca U12 1 M1caU131 M1ca U13 1 M1caU231 M1ca U23 1 M1caU112 M1ca U11 2 M1caU222 M1ca U22 2 M1caU332 M1ca U33 2 M1caU122 M1ca U12 2 M1caU132 M1ca U13 2 M1caU232 M1ca U23 2 M1naU111 M1na U11 1 M1naU221 M1na U22 1 M1naU331 M1na U33 1 M1naU121 M1na U12 1 M1naU131 M1na U13 1 M1naU231 M1na U23 1 M1naU112 M1na U11 2 M1naU222 M1na U22 2 M1naU332 M1na U33 2 M1naU122 M1na U12 2 M1naU132 M1na U13 2 M1naU232 M1na U23 2 T1osiU111 T1osi U11 1 T1osiU221 T1osi U22 1 T1osiU331 T1osi U33 1 T1osiU121 T1osi U12 1 T1osiU131 T1osi U13 1 T1osiU231 T1osi U23 1 T1osiU112 T1osi U11 2 T1osiU222 T1osi U22 2 T1osiU332 T1osi U33 2 T1osiU122 T1osi U12 2 T1osiU132 T1osi U13 2 T1osiU232 T1osi U23 2 T1msiU111 T1msi U11 1 T1msiU221 T1msi U22 1 T1msiU331 T1msi U33 1 T1msiU121 T1msi U12 1 T1msiU131 T1msi U13 1 T1msiU231 T1msi U23 1 T1msiU112 T1msi U11 2 T1msiU222 T1msi U22 2 T1msiU332 T1msi U33 2 T1msiU122 T1msi U12 2 T1msiU132 T1msi U13 2 T1msiU232 T1msi U23 2 T2osiU111 T2osi U11 1 T2osiU221 T2osi U22 1 T2osiU331 T2osi U33 1 T2osiU121 T2osi U12 1 T2osiU131 T2osi U13 1 T2osiU231 T2osi U23 1 T2osiU112 T2osi U11 2 T2osiU222 T2osi U22 2 T2osiU332 T2osi U33 2 T2osiU122 T2osi U12 2 T2osiU132 T2osi U13 2 T2osiU232 T2osi U23 2 T2msiU111 T2msi U11 1 T2msiU221 T2msi U22 1 T2msiU331 T2msi U33 1 T2msiU121 T2msi U12 1 T2msiU131 T2msi U13 1 T2msiU231 T2msi U23 1 T2msiU112 T2msi U11 2 T2msiU222 T2msi U22 2 T2msiU332 T2msi U33 2 T2msiU122 T2msi U12 2 T2msiU132 T2msi U13 2 T2msiU232 T2msi U23 2 T1oalU111 T1oal U11 1 T1oalU221 T1oal U22 1 T1oalU331 T1oal U33 1 T1oalU121 T1oal U12 1 T1oalU131 T1oal U13 1 T1oalU231 T1oal U23 1 T1oalU112 T1oal U11 2 T1oalU222 T1oal U22 2 T1oalU332 T1oal U33 2 T1oalU122 T1oal U12 2 T1oalU132 T1oal U13 2 T1oalU232 T1oal U23 2 T1malU111 T1mal U11 1 T1malU221 T1mal U22 1 T1malU331 T1mal U33 1 T1malU121 T1mal U12 1 T1malU131 T1mal U13 1 T1malU231 T1mal U23 1 T1malU112 T1mal U11 2 T1malU222 T1mal U22 2 T1malU332 T1mal U33 2 T1malU122 T1mal U12 2 T1malU132 T1mal U13 2 T1malU232 T1mal U23 2 T2oalU111 T2oal U11 1 T2oalU221 T2oal U22 1 T2oalU331 T2oal U33 1 T2oalU121 T2oal U12 1 T2oalU131 T2oal U13 1 T2oalU231 T2oal U23 1 T2oalU112 T2oal U11 2 T2oalU222 T2oal U22 2 T2oalU332 T2oal U33 2 T2oalU122 T2oal U12 2 T2oalU132 T2oal U13 2 T2oalU232 T2oal U23 2 T2malU111 T2mal U11 1 T2malU221 T2mal U22 1 T2malU331 T2mal U33 1 T2malU121 T2mal U12 1 T2malU131 T2mal U13 1 T2malU231 T2mal U23 1 T2malU112 T2mal U11 2 T2malU222 T2mal U22 2 T2malU332 T2mal U33 2 T2malU122 T2mal U12 2 T2malU132 T2mal U13 2 T2malU232 T2mal U23 2 OdmU111 Odm U11 1 OdmU221 Odm U22 1 OdmU331 Odm U33 1 OdmU121 Odm U12 1 OdmU131 Odm U13 1 OdmU231 Odm U23 1 OdmU112 Odm U11 2 OdmU222 Odm U22 2 OdmU332 Odm U33 2 OdmU122 Odm U12 2 OdmU132 Odm U13 2 OdmU232 Odm U23 2 Oa2U111 Oa2 U11 1 Oa2U221 Oa2 U22 1 Oa2U331 Oa2 U33 1 Oa2U121 Oa2 U12 1 Oa2U131 Oa2 U13 1 Oa2U231 Oa2 U23 1 Oa2U112 Oa2 U11 2 Oa2U222 Oa2 U22 2 Oa2U332 Oa2 U33 2 Oa2U122 Oa2 U12 2 Oa2U132 Oa2 U13 2 Oa2U232 Oa2 U23 2 OdoU111 Odo U11 1 OdoU221 Odo U22 1 OdoU331 Odo U33 1 OdoU121 Odo U12 1 OdoU131 Odo U13 1 OdoU231 Odo U23 1 OdoU112 Odo U11 2 OdoU222 Odo U22 2 OdoU332 Odo U33 2 OdoU122 Odo U12 2 OdoU132 Odo U13 2 OdoU232 Odo U23 2 Oa1U111 Oa1 U11 1 Oa1U221 Oa1 U22 1 Oa1U331 Oa1 U33 1 Oa1U121 Oa1 U12 1 Oa1U131 Oa1 U13 1 Oa1U231 Oa1 U23 1 Oa1U112 Oa1 U11 2 Oa1U222 Oa1 U22 2 Oa1U332 Oa1 U33 2 Oa1U122 Oa1 U12 2 Oa1U132 Oa1 U13 2 Oa1U232 Oa1 U23 2 ObmU111 Obm U11 1 ObmU221 Obm U22 1 ObmU331 Obm U33 1 ObmU121 Obm U12 1 ObmU131 Obm U13 1 ObmU231 Obm U23 1 ObmU112 Obm U11 2 ObmU222 Obm U22 2 ObmU332 Obm U33 2 ObmU122 Obm U12 2 ObmU132 Obm U13 2 ObmU232 Obm U23 2 OboU111 Obo U11 1 OboU221 Obo U22 1 OboU331 Obo U33 1 OboU121 Obo U12 1 OboU131 Obo U13 1 OboU231 Obo U23 1 OboU112 Obo U11 2 OboU222 Obo U22 2 OboU332 Obo U33 2 OboU122 Obo U12 2 OboU132 Obo U13 2 OboU232 Obo U23 2 OcmU111 Ocm U11 1 OcmU221 Ocm U22 1 OcmU331 Ocm U33 1 OcmU121 Ocm U12 1 OcmU131 Ocm U13 1 OcmU231 Ocm U23 1 OcmU112 Ocm U11 2 OcmU222 Ocm U22 2 OcmU332 Ocm U33 2 OcmU122 Ocm U12 2 OcmU132 Ocm U13 2 OcmU232 Ocm U23 2 OcoU111 Oco U11 1 OcoU221 Oco U22 1 OcoU331 Oco U33 1 OcoU121 Oco U12 1 OcoU131 Oco U13 1 OcoU231 Oco U23 1 OcoU112 Oco U11 2 OcoU222 Oco U22 2 OcoU332 Oco U33 2 OcoU122 Oco U12 2 OcoU132 Oco U13 2 OcoU232 Oco U23 2 loop_ _atom_site_U_Fourier_param_id _atom_site_U_Fourier_param_cos _atom_site_U_Fourier_param_sin M2caU111 -0.0009(4) 0.0063(8) M2caU221 -0.0048(8) 0.03(2) M2caU331 -0.0045(7) 0.0151(13) M2caU121 -0.0007(4) 0.0043(8) M2caU131 0.0007(4) 0.0021(7) M2caU231 0.0043(5) -0.0131(13) M2caU112 -0.008(9) -0.0009(8) M2caU222 -0.0164(16) -0.0048(13) M2caU332 -0.0099(12) -0.0047(11) M2caU122 0.0003(8) 0.0006(7) M2caU132 -0.0028(8) 0.0001(7) M2caU232 0.005(11) 0.0048(9) M1caU111 -0.001(5) -0.0013(6) M1caU221 0(3) -0.0154(15) M1caU331 -0.001(18) -0.0088(19) M1caU121 0.0022(8) -0.0066(8) M1caU131 -0.0013(6) 0.0032(7) M1caU231 0.002(2) 0.0092(12) M1caU112 0.0001(7) 0.0002(7) M1caU222 0.015(2) 0.012(3) M1caU332 -0.0016(17) 0.0036(18) M1caU122 -0.0068(9) -0.0033(9) M1caU132 0.0031(8) 0.001(8) M1caU232 -0.001(14) -0.0062(19) M1naU111 -0.001(5) -0.0013(6) M1naU221 0(3) -0.0154(15) M1naU331 -0.001(18) -0.0088(19) M1naU121 0.0022(8) -0.0066(8) M1naU131 -0.0013(6) 0.0032(7) M1naU231 0.002(2) 0.0092(12) M1naU112 0.0001(7) 0.0002(7) M1naU222 0.015(2) 0.012(3) M1naU332 -0.0016(17) 0.0036(18) M1naU122 -0.0068(9) -0.0033(9) M1naU132 0.0031(8) 0.001(8) M1naU232 -0.001(14) -0.0062(19) T1osiU111 0.00026(15) 0.00041(15) T1osiU221 0.00065(16) -0.00101(15) T1osiU331 -0.00138(16) 0.00022(16) T1osiU121 -0.00111(12) 0.00002(12) T1osiU131 0(14) 0.00008(13) T1osiU231 -0.00072(13) -0.00026(12) T1osiU112 0.0002(3) 0.0002(3) T1osiU222 0.0028(3) -0.0008(3) T1osiU332 0.0008(3) 0.0001(3) T1osiU122 -0.0009(2) 0.0004(2) T1osiU132 0.0001(2) 0.0004(2) T1osiU232 0.0001(2) 0.0002(2) T1msiU111 0.00001(15) 0.00054(15) T1msiU221 -0.0003(15) 0.00158(14) T1msiU331 0.00037(16) 0.00058(16) T1msiU121 -0.0008(12) 0.0001(12) T1msiU131 0.00034(13) 0.00048(13) T1msiU231 -0.00045(12) 0.00006(12) T1msiU112 0.0006(3) 0.0003(3) T1msiU222 0.0029(3) 0(3) T1msiU332 0(3) -0.0006(3) T1msiU122 0.0012(2) -0.0001(2) T1msiU132 -0.0001(2) 0(2) T1msiU232 -0.0006(2) -0.0002(2) T2osiU111 -0.0003(15) -0.00046(15) T2osiU221 -0.00007(14) 0.00043(13) T2osiU331 0.00142(16) -0.00039(16) T2osiU121 -0.00022(11) -0.0002(11) T2osiU131 0.00023(13) 0.00015(13) T2osiU231 -0.00116(12) -0.00032(12) T2osiU112 -0.0001(3) 0.0003(3) T2osiU222 0.001(3) 0.0005(3) T2osiU332 0.001(3) 0.0004(3) T2osiU122 -0.0001(2) 0.0003(2) T2osiU132 0.0002(2) 0.0004(2) T2osiU232 -0.0009(2) 0.0002(2) T2msiU111 0.00012(15) 0.0004(14) T2msiU221 -0.00116(15) -0.00035(14) T2msiU331 -0.00002(16) 0.00044(16) T2msiU121 0.00082(12) 0.00027(11) T2msiU131 -0.00022(13) 0.00039(13) T2msiU231 -0.00004(12) 0.00033(12) T2msiU112 0.0002(3) 0.0001(3) T2msiU222 0.0016(3) 0.0001(3) T2msiU332 -0.0003(3) -0.0001(3) T2msiU122 -0.0001(2) -0.0001(2) T2msiU132 -0.0002(2) 0(2) T2msiU232 0(2) -0.0002(2) T1oalU111 0.00026(15) 0.00041(15) T1oalU221 0.00065(16) -0.00101(15) T1oalU331 -0.00138(16) 0.00022(16) T1oalU121 -0.00111(12) 0.00002(12) T1oalU131 0(14) 0.00008(13) T1oalU231 -0.00072(13) -0.00026(12) T1oalU112 0.0002(3) 0.0002(3) T1oalU222 0.0028(3) -0.0008(3) T1oalU332 0.0008(3) 0.0001(3) T1oalU122 -0.0009(2) 0.0004(2) T1oalU132 0.0001(2) 0.0004(2) T1oalU232 0.0001(2) 0.0002(2) T1malU111 0.00001(15) 0.00054(15) T1malU221 -0.0003(15) 0.00158(14) T1malU331 0.00037(16) 0.00058(16) T1malU121 -0.0008(12) 0.0001(12) T1malU131 0.00034(13) 0.00048(13) T1malU231 -0.00045(12) 0.00006(12) T1malU112 0.0006(3) 0.0003(3) T1malU222 0.0029(3) 0(3) T1malU332 0(3) -0.0006(3) T1malU122 0.0012(2) -0.0001(2) T1malU132 -0.0001(2) 0(2) T1malU232 -0.0006(2) -0.0002(2) T2oalU111 -0.0003(15) -0.00046(15) T2oalU221 -0.00007(14) 0.00043(13) T2oalU331 0.00142(16) -0.00039(16) T2oalU121 -0.00022(11) -0.0002(11) T2oalU131 0.00023(13) 0.00015(13) T2oalU231 -0.00116(12) -0.00032(12) T2oalU112 -0.0001(3) 0.0003(3) T2oalU222 0.001(3) 0.0005(3) T2oalU332 0.001(3) 0.0004(3) T2oalU122 -0.0001(2) 0.0003(2) T2oalU132 0.0002(2) 0.0004(2) T2oalU232 -0.0009(2) 0.0002(2) T2malU111 0.00012(15) 0.0004(14) T2malU221 -0.00116(15) -0.00035(14) T2malU331 -0.00002(16) 0.00044(16) T2malU121 0.00082(12) 0.00027(11) T2malU131 -0.00022(13) 0.00039(13) T2malU231 -0.00004(12) 0.00033(12) T2malU112 0.0002(3) 0.0001(3) T2malU222 0.0016(3) 0.0001(3) T2malU332 -0.0003(3) -0.0001(3) T2malU122 -0.0001(2) -0.0001(2) T2malU132 -0.0002(2) 0(2) T2malU232 0(2) -0.0002(2) OdmU111 -0.0008(4) 0.0027(4) OdmU221 -0.0018(4) -0.0002(4) OdmU331 0.0004(4) 0.0007(4) OdmU121 -0.0008(3) 0.0004(3) OdmU131 -0.0003(4) -0.0015(4) OdmU231 -0.0022(4) -0.0008(3) OdmU112 -0.0007(8) 0(8) OdmU222 0.0035(7) -0.0001(7) OdmU332 0.0006(8) -0.0013(8) OdmU122 0.0006(6) -0.0001(6) OdmU132 -0.0006(6) 0.0005(6) OdmU232 -0.0008(6) -0.0001(6) Oa2U111 -0.0005(4) -0.0018(4) Oa2U221 0.0002(4) 0.0008(4) Oa2U331 0(4) 0.0003(4) Oa2U121 -0.0024(3) 0.0003(3) Oa2U131 -0.0001(3) -0.0003(3) Oa2U231 -0.0023(3) 0.0003(3) Oa2U112 -0.0003(7) -0.0004(7) Oa2U222 0.001(6) 0.0009(6) Oa2U332 0.0005(8) -0.0013(8) Oa2U122 0.0004(5) 0.0007(5) Oa2U132 0.0005(6) -0.0012(6) Oa2U232 0.0001(6) 0.0003(6) OdoU111 -0.0006(4) -0.0005(4) OdoU221 -0.0021(4) 0.0009(4) OdoU331 -0.0004(4) -0.0003(4) OdoU121 0.0014(3) -0.0012(3) OdoU131 -0.0009(4) 0(4) OdoU231 -0.0003(3) 0.0011(3) OdoU112 -0.0002(7) -0.0019(7) OdoU222 0.0026(7) -0.0016(7) OdoU332 0(8) 0.0008(8) OdoU122 -0.0005(6) 0.0007(5) OdoU132 -0.0003(6) 0.0015(6) OdoU232 -0.0005(6) -0.0003(6) Oa1U111 -0.0025(5) 0.007(5) Oa1U221 -0.0025(5) 0.001(4) Oa1U331 -0.0004(4) 0.0013(4) Oa1U121 -0.0038(4) 0.0005(3) Oa1U131 -0.0007(4) 0.0023(4) Oa1U231 -0.0019(4) 0.0007(3) Oa1U112 0.0001(8) -0.0004(8) Oa1U222 0.0051(7) -0.0006(7) Oa1U332 -0.0014(8) -0.0002(8) Oa1U122 0.001(6) 0.0005(6) Oa1U132 -0.001(6) 0.0001(7) Oa1U232 0.0011(6) -0.0006(6) ObmU111 0.0024(4) 0.0028(5) ObmU221 -0.0017(4) 0.0038(4) ObmU331 0.0021(6) 0.0088(6) ObmU121 -0.0007(3) 0.0013(4) ObmU131 0.0028(4) 0.0065(4) ObmU231 0.0002(4) 0.0014(4) ObmU112 0.0002(8) -0.0003(7) ObmU222 -0.0026(8) -0.0024(8) ObmU332 0.0015(9) -0.0036(9) ObmU122 0.0002(6) 0.0008(6) ObmU132 0.0005(7) -0.001(7) ObmU232 -0.001(7) 0.0032(7) OboU111 -0.0005(4) 0.0004(4) OboU221 -0.0012(4) -0.0003(4) OboU331 0.0025(5) 0.0003(5) OboU121 0.0023(3) -0.0002(3) OboU131 0.001(4) 0.0007(4) OboU231 0.001(3) -0.0001(3) OboU112 -0.0014(7) 0.0006(7) OboU222 0.001(7) 0.0004(7) OboU332 0.0007(9) 0.0024(8) OboU122 -0.0017(6) -0.0003(6) OboU132 -0.0001(7) 0.0019(7) OboU232 -0.0016(6) -0.0006(6) OcmU111 -0.0038(4) 0.0019(4) OcmU221 0.0024(4) 0.0018(4) OcmU331 0.0002(5) 0.0001(4) OcmU121 0.0003(4) 0.0017(3) OcmU131 -0.0001(4) -0.0005(4) OcmU231 0.0005(4) 0(3) OcmU112 0.0017(7) 0.0008(7) OcmU222 0.0028(7) 0.0015(7) OcmU332 -0.0004(8) -0.0011(8) OcmU122 0.0026(5) 0.0019(5) OcmU132 -0.0012(6) 0.0003(6) OcmU232 -0.001(6) 0.0019(6) OcoU111 0.0021(4) 0.0018(4) OcoU221 0.0026(4) -0.0022(4) OcoU331 0.0006(5) 0.0003(5) OcoU121 0.0002(3) 0.0009(3) OcoU131 0.0019(4) -0.0006(4) OcoU231 -0.0002(3) -0.0004(4) OcoU112 0.0007(7) 0.0015(7) OcoU222 0.0001(7) 0.0003(7) OcoU332 -0.0007(8) 0.0003(8) OcoU122 -0.0025(5) 0.0014(5) OcoU132 -0.0007(7) 0.0006(6) OcoU232 -0.0019(6) 0.0012(6) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 2 0 0 -2 3.23 4.05 2.20 < 2 0 0 0 212.52 250.32 4.53 o 2 0 0 2 0.42 0.41 2.08 < 4 0 0 -2 13.77 8.61 4.30 < 4 0 0 0 68743.00 68112.40 167.81 o 4 0 0 2 105.04 100.54 5.33 o 6 0 0 -2 52.34 57.42 9.18 o 6 0 0 0 42497.10 41392.70 115.14 o 6 0 0 2 77.99 80.32 12.82 o 8 0 0 -2 6.91 -0.55 12.36 < 8 0 0 0 39.50 46.82 13.97 o 8 0 0 2 8.70 15.89 13.23 < 10 0 0 -2 56.22 73.73 23.42 o 10 0 0 0 9476.35 9554.99 105.52 o 10 0 0 2 14.14 32.88 22.92 < -9 1 0 -2 3.28 1.58 15.14 < -9 1 0 0 732.46 690.55 30.30 o -9 1 0 2 5.84 0.44 14.15 < -7 1 0 -2 17.41 19.83 9.11 < -7 1 0 0 7053.47 6915.36 52.42 o -7 1 0 2 6.34 4.74 9.04 < -5 1 0 -2 5.33 4.37 4.30 < -5 1 0 0 889.48 882.18 13.71 o -5 1 0 2 2.98 4.60 4.53 < -3 1 0 -2 0.02 0.89 2.45 < -3 1 0 0 10137.00 9115.45 27.95 o -3 1 0 2 12.09 8.15 2.72 < -1 1 0 -2 6.47 5.59 1.99 < -1 1 0 0 1975.47 2128.87 11.32 o -1 1 0 2 9.09 3.87 1.26 o 1 1 0 -2 18.85 14.38 1.85 o 1 1 0 0 233.06 251.26 3.98 o 1 1 0 2 0.23 0.64 1.63 < 3 1 0 -2 1.06 3.48 3.14 < 3 1 0 0 8526.60 7457.71 30.25 o 3 1 0 2 7.50 6.21 3.09 < 5 1 0 -2 12.45 10.40 5.47 < 5 1 0 0 587.37 574.42 12.38 o 5 1 0 2 0.14 0.07 5.08 < 7 1 0 -2 3.75 12.07 9.59 < 7 1 0 0 5211.26 5241.32 46.55 o 7 1 0 2 17.63 21.96 11.20 < 9 1 0 -2 0.98 -0.05 14.33 < 9 1 0 0 197.15 198.95 25.39 o 9 1 0 2 0.25 -0.96 17.31 < -10 2 0 -2 17.30 15.62 19.10 < -10 2 0 0 579.32 572.72 33.28 o -10 2 0 2 12.53 12.85 19.49 < -8 2 0 -2 6.06 11.47 12.00 < -8 2 0 0 2166.13 2106.25 38.23 o -8 2 0 2 4.68 2.38 11.98 < -6 2 0 -2 52.90 62.51 7.49 o -6 2 0 0 12653.20 12866.40 64.03 o -6 2 0 2 0.22 3.66 7.51 < -4 2 0 -2 4.95 8.70 3.53 < -4 2 0 0 3436.89 3603.32 21.20 o -4 2 0 2 7.91 7.83 3.48 < -2 2 0 -2 71.41 61.54 5.68 o -2 2 0 0 66137.10 69193.20 206.08 o -2 2 0 2 0.04 1.51 2.95 < 0 2 0 -2 28.54 21.11 1.79 o 0 2 0 0 123.71 126.36 3.27 o 0 2 0 2 17.77 10.92 1.83 o 2 2 0 -2 2.55 -0.23 2.56 < 2 2 0 0 59091.50 58779.00 168.27 o 2 2 0 2 5.39 3.34 2.86 < 4 2 0 -2 27.68 29.29 4.79 o 4 2 0 0 6049.15 6453.84 33.25 o 4 2 0 2 0.07 0.60 4.08 < 6 2 0 -2 9.31 14.68 7.92 < 6 2 0 0 17225.90 17210.70 76.35 o 6 2 0 2 31.78 28.23 8.08 o 8 2 0 -2 0.75 7.40 15.18 < 8 2 0 0 2298.88 2341.63 48.68 o 8 2 0 2 5.21 3.05 14.49 < 10 2 0 -2 4.57 3.02 22.14 < 10 2 0 0 1784.06 1805.54 54.87 o 10 2 0 2 24.35 28.99 24.09 < -9 3 0 -2 26.25 28.53 16.12 < -9 3 0 0 5200.19 4991.22 61.04 o -9 3 0 2 2.46 12.64 15.52 < -7 3 0 -2 0.68 -5.15 8.75 < -7 3 0 0 1215.08 1186.01 23.43 o -7 3 0 2 11.10 11.13 9.32 < -5 3 0 -2 2.95 1.85 4.42 < -5 3 0 0 6857.45 7041.85 32.15 o -5 3 0 2 3.88 4.95 5.11 < -3 3 0 -2 48.47 46.62 3.66 o -3 3 0 0 3691.45 2871.65 16.62 o -3 3 0 2 30.33 30.09 3.16 o -1 3 0 -2 7.71 8.27 2.11 o -1 3 0 0 38329.60 40788.30 113.42 o -1 3 0 2 32.28 30.18 3.02 o 1 3 0 -2 12.88 10.42 2.72 o 1 3 0 0 31821.50 32309.10 108.97 o 1 3 0 2 43.78 40.32 3.48 o 3 3 0 -2 37.68 34.32 4.42 o 3 3 0 0 4809.20 3839.53 23.39 o 3 3 0 2 0.09 -0.64 3.66 < 5 3 0 -2 4.60 6.00 5.45 < 5 3 0 0 10761.80 11062.70 53.57 o 5 3 0 2 38.95 40.64 7.17 o 7 3 0 -2 55.23 52.14 11.95 o 7 3 0 0 81.98 101.38 16.78 o 7 3 0 2 7.68 0.66 12.46 < 9 3 0 -2 3.34 16.33 19.03 < 9 3 0 0 7855.14 8065.20 93.29 o 9 3 0 2 33.88 38.21 20.97 < -10 4 0 -2 43.48 52.46 20.84 < -10 4 0 0 4885.68 4697.98 65.29 o -10 4 0 2 3.25 10.62 20.01 < -8 4 0 -2 28.04 29.45 12.85 < -8 4 0 0 6531.40 6320.17 61.98 o -8 4 0 2 1.64 8.06 10.88 < -6 4 0 -2 152.12 166.79 16.26 o -6 4 0 0 36496.10 36483.80 75.78 o -6 4 0 2 0.05 7.97 6.25 < -4 4 0 -2 16.71 19.65 3.96 o -4 4 0 0 626.68 640.29 9.29 o -4 4 0 2 76.59 83.00 5.04 o -2 4 0 -2 5.75 9.02 2.56 o -2 4 0 0 6894.26 7885.85 27.08 o -2 4 0 2 27.85 31.51 3.23 o 0 4 0 -2 13.33 11.20 2.72 o 0 4 0 0 83146.60 82528.20 197.66 o 0 4 0 2 0.23 2.43 2.70 < 2 4 0 -2 6.55 6.02 3.37 < 2 4 0 0 10529.90 11993.90 39.38 o 2 4 0 2 4.54 2.13 3.34 < 4 4 0 -2 10.32 7.56 4.81 < 4 4 0 0 8.22 14.93 5.17 < 4 4 0 2 2.33 1.35 4.58 < 6 4 0 -2 70.87 69.47 11.20 o 6 4 0 0 34495.70 33940.00 122.17 o 6 4 0 2 63.09 60.95 10.56 o 8 4 0 -2 43.56 56.39 17.75 o 8 4 0 0 6462.18 6591.42 79.65 o 8 4 0 2 0.81 5.06 15.55 < 10 4 0 -2 54.67 67.09 26.51 < 10 4 0 0 3094.24 3161.05 69.44 o 10 4 0 2 5.53 3.32 24.48 < -9 5 0 -2 8.93 10.19 16.14 < -9 5 0 0 224.96 247.76 22.62 o -9 5 0 2 0.00 -4.58 14.40 < -7 5 0 -2 0.34 -0.27 8.29 < -7 5 0 0 1103.55 1057.31 23.00 o -7 5 0 2 8.01 4.76 9.36 < -5 5 0 -2 5.45 6.73 4.51 < -5 5 0 0 5367.61 5688.57 28.67 o -5 5 0 2 4.95 7.44 4.56 < -3 5 0 -2 11.03 11.95 3.46 o -3 5 0 0 291.30 245.91 6.14 o -3 5 0 2 53.97 55.09 4.10 o -1 5 0 -2 2.77 1.95 2.56 < -1 5 0 0 2098.91 3613.30 17.65 o -1 5 0 2 14.02 14.01 2.79 o 1 5 0 -2 27.01 28.35 3.87 o 1 5 0 0 735.10 1538.44 14.23 o 1 5 0 2 93.58 96.76 5.50 o 3 5 0 -2 8.58 8.59 4.49 < 3 5 0 0 249.73 200.68 8.29 o 3 5 0 2 1.84 4.83 4.51 < 5 5 0 -2 87.15 86.98 9.09 o 5 5 0 0 815.82 977.26 19.11 o 5 5 0 2 74.39 72.12 8.79 o 7 5 0 -2 6.99 9.20 13.74 < 7 5 0 0 5568.16 5618.80 69.09 o 7 5 0 2 19.96 23.01 14.84 < 9 5 0 -2 16.30 19.16 20.61 < 9 5 0 0 500.06 455.67 34.11 o 9 5 0 2 7.24 16.65 21.07 < -8 6 0 -2 50.30 64.02 14.65 o -8 6 0 0 10129.10 10041.80 68.97 o -8 6 0 2 4.56 16.92 12.00 < -6 6 0 -2 32.68 32.51 6.07 o -6 6 0 0 392.81 569.40 12.32 o -6 6 0 2 58.65 51.38 6.66 o -4 6 0 -2 46.34 44.44 4.81 o -4 6 0 0 12038.30 12291.30 40.23 o -4 6 0 2 30.15 34.80 4.67 o -2 6 0 -2 1.21 2.95 3.30 < -2 6 0 0 26164.90 27150.50 64.92 o -2 6 0 2 57.07 54.61 4.65 o 0 6 0 -2 0.05 2.24 3.16 < 0 6 0 0 26804.90 28124.20 79.84 o 0 6 0 2 6.59 4.67 3.53 < 2 6 0 -2 5.23 7.24 4.12 < 2 6 0 0 24530.80 24425.10 64.44 o 2 6 0 2 6.10 4.42 4.44 < 4 6 0 -2 8.84 9.50 5.88 < 4 6 0 0 20141.70 19268.00 72.20 o 4 6 0 2 7.14 4.30 5.98 < 6 6 0 -2 0.43 -0.60 9.91 < 6 6 0 0 1186.11 1324.27 28.37 o 6 6 0 2 26.62 31.46 10.56 < 8 6 0 -2 47.09 60.10 19.07 o 8 6 0 0 5931.27 5946.45 79.07 o 8 6 0 2 1.72 10.51 17.68 < -9 7 0 -2 26.84 30.77 16.17 < -9 7 0 0 4.63 -3.02 16.30 < -9 7 0 2 15.21 10.62 18.78 < -7 7 0 -2 27.85 35.33 9.87 o -7 7 0 0 2031.87 2183.56 29.27 o -7 7 0 2 10.47 11.63 10.26 < -5 7 0 -2 19.77 14.33 5.24 < -5 7 0 0 2861.63 2851.64 21.87 o -5 7 0 2 78.62 82.91 6.55 o -3 7 0 -2 40.19 41.24 4.90 o -3 7 0 0 2431.79 2426.06 19.09 o -3 7 0 2 22.35 22.23 4.40 o -1 7 0 -2 10.57 9.46 3.62 < -1 7 0 0 11707.80 12775.20 39.22 o -1 7 0 2 90.43 88.97 5.40 o 1 7 0 -2 5.88 7.95 4.35 < 1 7 0 0 411.74 528.21 10.83 o 1 7 0 2 10.87 7.81 4.37 < 3 7 0 -2 16.76 14.56 5.68 < 3 7 0 0 6804.10 6711.27 38.53 o 3 7 0 2 114.33 119.84 8.36 o 5 7 0 -2 6.11 7.69 8.08 < 5 7 0 0 2835.02 2678.35 31.70 o 5 7 0 2 1.38 3.50 7.99 < 7 7 0 -2 0.31 2.89 15.20 < 7 7 0 0 1564.01 1655.95 42.50 o 7 7 0 2 46.48 62.60 17.75 o 9 7 0 -2 0.02 -6.53 22.19 < 9 7 0 0 837.41 900.15 44.14 o 9 7 0 2 14.20 21.04 22.99 < -8 8 0 -2 2.09 11.95 13.10 < -8 8 0 0 7567.11 7395.10 67.01 o -8 8 0 2 84.23 85.29 16.69 o -6 8 0 -2 0.17 -1.31 8.20 < -6 8 0 0 311.80 317.93 11.31 o -6 8 0 2 20.48 15.91 6.57 < -4 8 0 -2 30.68 32.58 5.38 o -4 8 0 0 3161.90 3034.42 22.07 o -4 8 0 2 17.25 12.85 5.13 < -2 8 0 -2 4.39 6.62 4.42 < -2 8 0 0 41239.20 41277.90 99.68 o -2 8 0 2 1.70 7.40 4.56 < 0 8 0 -2 36.75 28.44 4.99 o 0 8 0 0 12250.90 13034.30 49.23 o 0 8 0 2 16.04 12.87 4.99 < 2 8 0 -2 15.92 20.61 5.93 o 2 8 0 0 29654.70 29680.90 79.40 o 2 8 0 2 0.15 0.98 5.43 < 4 8 0 -2 1.77 2.98 7.19 < 4 8 0 0 8363.56 7978.39 51.09 o 4 8 0 2 18.65 12.73 7.88 < 6 8 0 -2 0.14 1.26 11.61 < 6 8 0 0 35.99 37.87 12.82 < 6 8 0 2 11.77 14.29 14.63 < 8 8 0 -2 12.99 40.89 21.25 < 8 8 0 0 14499.10 15341.40 128.32 o 8 8 0 2 65.62 75.76 23.10 o -9 9 0 -2 1.14 -9.16 26.88 < -9 9 0 0 9.00 28.07 29.58 < -9 9 0 2 3.83 1.28 28.64 < -7 9 0 -2 0.11 1.03 13.40 < -7 9 0 0 152.48 167.64 26.51 o -7 9 0 2 28.31 29.61 14.36 < -5 9 0 -2 2.91 9.04 5.88 < -5 9 0 0 7089.05 7266.69 38.41 o -5 9 0 2 11.66 11.81 7.30 < -3 9 0 -2 30.31 28.64 5.61 o -3 9 0 0 353.93 531.37 11.49 o -3 9 0 2 45.12 48.13 6.27 o -1 9 0 -2 5.18 10.12 5.34 < -1 9 0 0 5145.50 5239.95 33.40 o -1 9 0 2 43.77 42.40 6.37 o 1 9 0 -2 21.70 20.03 6.55 o 1 9 0 0 29117.90 28789.40 86.23 o 1 9 0 2 125.33 125.24 9.16 o 3 9 0 -2 1.81 -2.01 6.96 < 3 9 0 0 162.57 254.32 12.94 o 3 9 0 2 10.86 8.33 7.33 < 5 9 0 -2 2.99 7.24 9.91 < 5 9 0 0 6627.53 6888.41 57.94 o 5 9 0 2 62.32 68.48 12.30 o 7 9 0 -2 3.69 -3.16 20.88 < 7 9 0 0 2747.26 2795.23 67.96 o 7 9 0 2 10.13 17.36 22.19 < 9 9 0 -2 0.01 -12.48 28.58 < -8 10 0 -2 19.99 37.12 18.55 < -8 10 0 0 722.44 699.57 32.82 o -8 10 0 2 44.94 38.05 18.84 < -6 10 0 -2 4.11 0.00 9.39 < -6 10 0 0 98.95 102.07 11.84 o -6 10 0 2 27.57 25.35 10.44 < -4 10 0 -2 16.28 14.75 7.44 < -4 10 0 0 500.57 497.79 15.24 o -4 10 0 2 12.35 11.13 8.56 < -2 10 0 -2 18.39 22.16 6.23 o -2 10 0 0 1979.77 2140.30 27.46 o -2 10 0 2 0.01 4.42 6.89 < 0 10 0 -2 0.03 1.51 5.86 < 0 10 0 0 8528.83 8040.78 47.08 o 0 10 0 2 2.89 2.61 5.86 < 2 10 0 -2 5.54 8.72 7.30 < 2 10 0 0 340.75 287.76 13.23 o 2 10 0 2 1.47 2.98 7.12 < 4 10 0 -2 0.00 -1.67 9.20 < 4 10 0 0 356.99 357.53 17.60 o 4 10 0 2 7.21 3.00 9.55 < 6 10 0 -2 0.16 -2.15 15.00 < 6 10 0 0 1787.47 1698.93 51.26 o 6 10 0 2 3.01 -0.87 18.36 < 8 10 0 -2 2.54 13.05 27.16 < 8 10 0 0 960.63 1032.73 54.46 o 8 10 0 2 1.31 -2.08 26.90 < -7 11 0 -2 0.27 -0.48 18.18 < -7 11 0 0 18.72 12.48 18.98 < -7 11 0 2 2.23 8.86 19.00 < -5 11 0 -2 6.93 7.74 9.11 < -5 11 0 0 3021.45 2942.77 36.20 o -5 11 0 2 10.14 7.08 10.19 < -3 11 0 -2 15.52 15.41 7.83 < -3 11 0 0 1141.16 1128.29 22.93 o -3 11 0 2 23.26 19.85 8.72 < -1 11 0 -2 0.03 0.64 7.26 < -1 11 0 0 397.76 381.48 15.41 o -1 11 0 2 53.14 67.34 9.39 o 1 11 0 -2 0.10 0.32 7.24 < 1 11 0 0 638.39 627.72 19.52 o 1 11 0 2 43.98 39.95 9.80 o 3 11 0 -2 7.01 7.60 8.86 < 3 11 0 0 651.80 663.97 19.27 o 3 11 0 2 23.71 19.67 9.04 < 5 11 0 -2 0.89 -3.43 11.77 < 5 11 0 0 1021.94 1025.75 27.89 o 5 11 0 2 1.02 1.17 11.95 < 7 11 0 -2 0.84 -9.57 22.85 < 7 11 0 0 1336.16 1370.31 54.73 o 7 11 0 2 22.38 4.95 24.98 < -8 12 0 -2 9.55 2.15 29.29 < -8 12 0 0 2257.46 2080.87 70.64 o -8 12 0 2 0.26 2.91 20.79 < -6 12 0 -2 0.01 -0.02 12.27 < -6 12 0 0 50.70 52.52 13.76 o -6 12 0 2 42.56 34.87 13.39 < -4 12 0 -2 6.22 7.58 9.80 < -4 12 0 0 17.02 39.02 10.74 o -4 12 0 2 8.69 9.69 9.78 < -2 12 0 -2 34.25 44.26 9.89 o -2 12 0 0 8518.27 8731.30 58.87 o -2 12 0 2 17.56 13.76 8.59 < 0 12 0 -2 0.05 3.21 9.09 < 0 12 0 0 1897.08 2136.44 33.73 o 0 12 0 2 0.06 1.79 9.20 < 2 12 0 -2 1.87 2.45 10.17 < 2 12 0 0 7519.79 7686.26 63.49 o 2 12 0 2 0.12 6.55 10.69 < 4 12 0 -2 2.39 6.41 11.68 < 4 12 0 0 876.94 873.35 26.27 o 4 12 0 2 9.41 5.66 13.92 < 6 12 0 -2 0.03 -4.58 21.25 < 6 12 0 0 392.30 394.63 35.51 o 6 12 0 2 1.00 -1.51 22.23 < -7 13 0 -2 0.84 14.91 27.36 < -7 13 0 0 1544.31 1410.01 60.21 o -7 13 0 2 0.56 -1.90 19.00 < -5 13 0 -2 14.74 19.83 13.94 < -5 13 0 0 5625.06 5730.05 61.10 o -5 13 0 2 37.90 45.86 14.88 o -3 13 0 -2 11.44 13.30 12.14 < -3 13 0 0 2722.95 2737.61 42.52 o -3 13 0 2 29.23 30.48 12.41 < -1 13 0 -2 37.58 33.75 13.44 < -1 13 0 0 24.09 26.40 13.92 < -1 13 0 2 32.68 29.51 11.81 < 1 13 0 -2 24.79 32.95 14.26 < 1 13 0 0 1706.05 1753.41 40.28 o 1 13 0 2 2.23 5.47 10.99 < 3 13 0 -2 1.40 0.92 14.75 < 3 13 0 0 2838.77 2988.79 53.16 o 3 13 0 2 0.54 -1.56 12.55 < 5 13 0 -2 4.33 14.49 21.52 < 5 13 0 0 1414.89 1407.66 50.44 o 5 13 0 2 1.92 -2.43 28.97 < -6 14 0 -2 0.07 -8.20 16.26 < -6 14 0 0 1534.09 1497.26 38.34 o -6 14 0 2 0.08 1.67 16.07 < -4 14 0 -2 3.81 9.85 13.37 < -4 14 0 0 5430.10 5268.86 60.92 o -4 14 0 2 0.02 1.01 13.97 < -2 14 0 -2 22.38 36.82 13.28 < -2 14 0 0 1499.76 1519.12 35.12 o -2 14 0 2 13.23 13.12 12.18 < 0 14 0 -2 0.33 4.99 14.47 < 0 14 0 0 7912.83 8009.47 83.42 o 0 14 0 2 0.17 5.70 14.29 < 2 14 0 -2 1.95 -1.21 14.59 < 2 14 0 0 94.58 99.39 19.62 o 2 14 0 2 5.40 -5.75 15.16 < 4 14 0 -2 9.32 7.79 21.02 < 4 14 0 0 145.45 150.47 27.70 o 4 14 0 2 10.40 12.14 22.23 < -5 15 0 -2 0.49 -1.85 16.60 < -5 15 0 0 126.75 189.05 22.53 o -5 15 0 2 0.85 0.78 16.55 < -3 15 0 -2 24.34 19.26 15.11 < -3 15 0 0 1140.34 1157.74 34.74 o -3 15 0 2 16.02 22.58 14.84 < -1 15 0 -2 29.57 24.25 16.33 < -1 15 0 0 306.84 334.63 27.38 o -1 15 0 2 9.82 4.01 15.71 < 1 15 0 -2 15.66 25.83 16.39 < 1 15 0 0 1849.48 1796.39 45.88 o 1 15 0 2 20.40 18.39 17.08 < 3 15 0 -2 8.01 5.61 22.49 < 3 15 0 0 1681.22 1684.30 57.66 o 3 15 0 2 13.09 -0.85 23.06 < 5 15 0 -2 11.67 24.39 37.69 < 5 15 0 0 339.71 351.50 54.41 o 5 15 0 2 52.70 44.42 39.29 < -4 16 0 -2 12.15 5.43 17.40 < -4 16 0 0 54.92 67.75 20.31 o -4 16 0 2 3.66 -6.30 16.72 < -2 16 0 -2 2.28 -2.72 18.09 < -2 16 0 0 22.03 21.07 18.16 < -2 16 0 2 12.31 7.19 18.00 < 0 16 0 -2 5.19 -3.59 17.38 < 0 16 0 0 462.20 548.24 32.21 o 0 16 0 2 16.17 17.77 18.64 < 2 16 0 -2 3.75 -4.67 19.30 < 2 16 0 0 700.25 637.80 36.78 o 2 16 0 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50.58 8.24 o 2 -10 2 -2 0.67 -0.11 7.24 < 2 -10 2 0 1680.92 1609.90 25.04 o 2 -10 2 2 3.32 5.15 7.37 < 4 -10 2 -2 33.30 42.34 11.06 o 4 -10 2 0 424.16 448.45 18.63 o 4 -10 2 2 25.65 36.13 10.44 o 6 -10 2 -2 42.73 50.65 15.98 o 6 -10 2 0 2278.05 2347.57 44.12 o 6 -10 2 2 11.30 8.77 13.88 < 8 -10 2 -2 43.90 33.43 18.39 < 8 -10 2 0 992.65 985.95 34.39 o 8 -10 2 2 2.13 9.43 17.79 < -9 -9 2 -2 1.86 -17.22 28.67 < -9 -9 2 0 147.17 156.19 33.31 o -9 -9 2 2 0.07 -10.05 27.91 < -7 -9 2 -2 23.43 38.70 19.33 < -7 -9 2 0 1904.83 2143.02 48.17 o -7 -9 2 2 61.31 81.51 19.23 o -5 -9 2 -2 0.25 -1.69 8.66 < -5 -9 2 0 1474.24 1483.33 25.92 o -5 -9 2 2 15.53 18.94 9.14 < -3 -9 2 -2 149.01 148.52 10.72 o -3 -9 2 0 156.11 213.66 12.07 o -3 -9 2 2 16.56 15.07 6.87 < -1 -9 2 -2 0.93 -0.53 5.29 < -1 -9 2 0 1427.93 1467.74 18.60 o -1 -9 2 2 56.44 51.43 6.32 o 1 -9 2 -2 38.00 38.19 7.53 o 1 -9 2 0 29586.00 29389.60 92.22 o 1 -9 2 2 62.68 65.03 7.74 o 3 -9 2 -2 18.19 17.93 8.40 < 3 -9 2 0 15.84 14.22 8.17 < 3 -9 2 2 22.20 23.49 8.11 < 5 -9 2 -2 7.69 10.17 9.75 < 5 -9 2 0 2505.45 2552.50 35.29 o 5 -9 2 2 31.45 31.39 10.30 o 7 -9 2 -2 2.29 3.82 14.40 < 7 -9 2 0 5117.60 5038.36 64.06 o 7 -9 2 2 45.73 60.42 16.55 o -8 -8 2 -2 23.17 37.48 19.39 < -8 -8 2 0 6559.27 6705.51 83.88 o -8 -8 2 2 0.10 12.00 17.42 < -6 -8 2 -2 11.74 9.32 10.62 < -6 -8 2 0 431.78 376.52 19.71 o -6 -8 2 2 0.45 -2.20 10.40 < -4 -8 2 -2 18.58 13.12 7.01 < -4 -8 2 0 626.24 517.62 14.35 o -4 -8 2 2 35.72 38.05 7.49 o -2 -8 2 -2 5.25 6.59 5.20 < -2 -8 2 0 38582.10 38012.00 92.56 o -2 -8 2 2 11.58 17.68 5.47 o 0 -8 2 -2 28.34 21.20 6.11 o 0 -8 2 0 11196.70 11951.20 47.57 o 0 -8 2 2 4.68 7.40 4.58 < 2 -8 2 -2 51.56 51.68 6.04 o 2 -8 2 0 9868.20 10450.20 38.97 o 2 -8 2 2 51.95 48.45 5.27 o 4 -8 2 -2 30.17 36.20 9.30 o 4 -8 2 0 8065.64 8343.49 44.31 o 4 -8 2 2 47.34 38.81 6.27 o 6 -8 2 -2 22.74 25.03 12.25 < 6 -8 2 0 2008.92 2047.02 39.30 o 6 -8 2 2 1.90 0.78 11.70 < 8 -8 2 -2 1.85 18.07 15.62 < 8 -8 2 0 9710.83 9834.28 83.23 o 8 -8 2 2 103.26 89.06 16.92 o -9 -7 2 -2 11.76 10.24 21.16 < -9 -7 2 0 1557.75 1635.41 50.23 o -9 -7 2 2 82.47 88.84 22.87 o -7 -7 2 -2 0.06 6.80 14.88 < -7 -7 2 0 46.12 48.36 15.78 o -7 -7 2 2 0.44 -3.82 13.49 < -5 -7 2 -2 38.32 43.98 8.68 o -5 -7 2 0 233.12 238.49 12.91 o -5 -7 2 2 43.50 39.34 8.54 o -3 -7 2 -2 1.41 0.46 5.15 < -3 -7 2 0 1880.11 1998.87 22.92 o -3 -7 2 2 31.78 30.54 5.82 o -1 -7 2 -2 45.37 39.11 4.76 o -1 -7 2 0 6049.28 6343.62 29.99 o -1 -7 2 2 6.84 7.53 3.89 < 1 -7 2 -2 8.88 8.72 4.85 < 1 -7 2 0 5919.86 6126.63 27.21 o 1 -7 2 2 4.56 6.41 3.87 < 3 -7 2 -2 7.52 3.39 4.97 < 3 -7 2 0 8.19 30.89 4.99 o 3 -7 2 2 5.17 6.69 4.21 < 5 -7 2 -2 3.11 -0.05 7.51 < 5 -7 2 0 2597.83 2489.29 28.82 o 5 -7 2 2 8.50 6.23 5.91 < 7 -7 2 -2 8.61 8.49 14.24 < 7 -7 2 0 56.14 50.26 13.69 o 7 -7 2 2 9.22 5.06 10.67 < 9 -7 2 -2 1.35 10.51 21.25 < 9 -7 2 0 2666.46 2580.61 57.06 o 9 -7 2 2 27.85 19.03 20.31 < -10 -6 2 -2 2.70 2.95 23.63 < -10 -6 2 0 18.46 16.46 24.48 < -10 -6 2 2 0.23 0.09 23.40 < 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41.58 7.72 o -5 -5 2 0 7850.89 7724.93 46.09 o -5 -5 2 2 2.31 2.20 6.23 < -3 -5 2 -2 21.80 18.16 4.49 o -3 -5 2 0 4785.94 5371.31 29.81 o -3 -5 2 2 41.93 42.27 5.01 o -1 -5 2 -2 17.16 19.05 3.48 o -1 -5 2 0 10080.90 10837.30 33.86 o -1 -5 2 2 2.42 1.14 2.68 < 1 -5 2 -2 10.60 8.70 3.34 < 1 -5 2 0 11050.20 10739.80 33.84 o 1 -5 2 2 11.78 10.01 2.79 o 3 -5 2 -2 40.73 41.08 5.22 o 3 -5 2 0 9359.77 9943.91 35.94 o 3 -5 2 2 11.07 11.52 3.59 o 5 -5 2 -2 8.93 9.89 7.74 < 5 -5 2 0 49.83 40.39 7.17 o 5 -5 2 2 8.16 12.48 5.31 < 7 -5 2 -2 3.53 6.73 10.12 < 7 -5 2 0 2064.56 2017.20 32.47 o 7 -5 2 2 7.31 7.08 10.65 < 9 -5 2 -2 18.20 7.44 17.24 < 9 -5 2 0 693.74 640.95 32.70 o 9 -5 2 2 9.43 6.62 18.07 < -10 -4 2 -2 0.05 -3.11 21.82 < -10 -4 2 0 702.50 700.92 40.60 o -10 -4 2 2 4.13 1.83 21.68 < -8 -4 2 -2 7.30 12.00 14.40 < -8 -4 2 0 5014.23 5042.67 67.48 o -8 -4 2 2 16.50 12.11 15.11 < -6 -4 2 -2 0.27 0.32 8.49 < -6 -4 2 0 70.70 44.60 8.33 o -6 -4 2 2 4.86 6.89 7.05 < -4 -4 2 -2 1.80 -0.64 4.37 < -4 -4 2 0 10074.50 10148.80 42.13 o -4 -4 2 2 2.45 2.72 4.26 < -2 -4 2 -2 114.11 110.38 4.99 o -2 -4 2 0 58681.50 57376.00 178.85 o -2 -4 2 2 19.60 22.48 3.50 o 0 -4 2 -2 45.61 46.87 5.01 o 0 -4 2 0 38679.50 40803.80 163.55 o 0 -4 2 2 16.58 14.79 3.87 o 2 -4 2 -2 48.83 51.43 4.40 o 2 -4 2 0 38352.80 44727.40 130.94 o 2 -4 2 2 102.48 110.17 5.13 o 4 -4 2 -2 124.52 124.05 7.44 o 4 -4 2 0 6066.78 6299.97 30.04 o 4 -4 2 2 7.99 5.77 4.08 < 6 -4 2 -2 115.19 119.08 12.91 o 6 -4 2 0 5754.91 5725.45 51.10 o 6 -4 2 2 3.07 11.24 8.59 < 8 -4 2 -2 71.05 60.95 13.69 o 8 -4 2 0 1904.15 1785.93 34.35 o 8 -4 2 2 3.41 7.97 12.62 < -9 -3 2 -2 10.81 24.96 18.23 < -9 -3 2 0 1416.46 1377.21 42.64 o -9 -3 2 2 5.96 15.84 16.85 < -7 -3 2 -2 1.19 -3.76 9.09 < -7 -3 2 0 1465.67 1494.03 34.84 o -7 -3 2 2 11.75 8.47 10.67 < -5 -3 2 -2 33.66 37.67 5.95 o -5 -3 2 0 7683.02 7518.11 42.18 o -5 -3 2 2 7.98 8.06 5.43 < -3 -3 2 -2 22.51 21.13 3.62 o -3 -3 2 0 20982.30 23841.50 55.43 o -3 -3 2 2 92.89 88.01 4.85 o -1 -3 2 -2 21.53 18.43 2.68 o -1 -3 2 0 12737.80 13816.80 36.34 o -1 -3 2 2 10.28 8.43 2.31 o 1 -3 2 -2 23.01 18.89 3.07 o 1 -3 2 0 35039.70 37841.60 120.32 o 1 -3 2 2 4.12 3.07 2.08 < 3 -3 2 -2 0.60 1.14 3.46 < 3 -3 2 0 6437.18 6216.59 26.13 o 3 -3 2 2 2.19 1.60 3.14 < 5 -3 2 -2 0.14 -1.60 6.94 < 5 -3 2 0 200.29 272.92 13.85 o 5 -3 2 2 4.96 3.78 7.24 < 7 -3 2 -2 21.37 22.23 10.90 < 7 -3 2 0 1272.36 1208.10 26.56 o 7 -3 2 2 2.68 8.98 10.24 < 9 -3 2 -2 19.58 23.77 16.83 < 9 -3 2 0 68.89 58.66 18.52 o 9 -3 2 2 3.07 2.70 17.49 < -10 -2 2 -2 4.15 -0.73 19.87 < -10 -2 2 0 1542.83 1552.14 48.91 o -10 -2 2 2 1.34 -1.92 20.91 < -8 -2 2 -2 0.01 0.82 12.59 < -8 -2 2 0 218.49 267.31 22.30 o -8 -2 2 2 37.12 29.83 14.63 < -6 -2 2 -2 0.40 -0.02 6.11 < -6 -2 2 0 4469.63 4753.99 33.95 o -6 -2 2 2 5.46 2.61 5.98 < -4 -2 2 -2 48.53 41.31 4.83 o -4 -2 2 0 3717.68 3576.20 23.46 o -4 -2 2 2 56.64 54.79 4.99 o -2 -2 2 -2 23.45 20.91 2.79 o -2 -2 2 0 5617.91 5821.86 21.06 o -2 -2 2 2 3.46 4.79 2.31 < 0 -2 2 -2 20.58 18.87 2.86 o 0 -2 2 0 2915.59 3253.11 16.31 o 0 -2 2 2 144.74 116.17 6.64 o 2 -2 2 -2 1.13 2.50 2.98 < 2 -2 2 0 7362.66 8223.16 29.17 o 2 -2 2 2 41.38 40.98 3.11 o 4 -2 2 -2 0.53 -1.33 4.17 < 4 -2 2 0 1315.19 1458.47 14.34 o 4 -2 2 2 11.25 11.13 3.82 < 6 -2 2 -2 76.60 73.13 10.07 o 6 -2 2 0 26.04 24.13 8.91 < 6 -2 2 2 0.01 -1.67 7.62 < 8 -2 2 -2 9.48 5.54 12.59 < 8 -2 2 0 706.03 683.76 25.01 o 8 -2 2 2 6.78 8.06 13.01 < -9 -1 2 -2 2.49 -0.16 15.43 < -9 -1 2 0 1091.65 1070.74 36.89 o -9 -1 2 2 34.84 27.73 17.04 < -7 -1 2 -2 1.72 -0.30 8.08 < -7 -1 2 0 1239.14 1156.30 30.32 o -7 -1 2 2 7.33 4.37 9.48 < -5 -1 2 -2 3.26 4.42 4.28 < -5 -1 2 0 5408.22 5525.21 27.97 o -5 -1 2 2 38.82 41.67 4.74 o -3 -1 2 -2 0.34 1.05 2.82 < -3 -1 2 0 863.81 855.60 10.14 o -3 -1 2 2 9.26 7.46 2.70 < -1 -1 2 -2 3.58 3.14 2.04 < -1 -1 2 0 728.92 655.40 6.04 o -1 -1 2 2 0.00 -0.27 1.35 < 1 -1 2 -2 3.32 3.64 2.72 < 1 -1 2 0 13992.10 14599.90 50.10 o 1 -1 2 2 6.96 3.07 2.20 < 3 -1 2 -2 0.81 1.31 3.41 < 3 -1 2 0 7088.53 8737.89 30.62 o 3 -1 2 2 6.71 10.05 3.66 < 5 -1 2 -2 15.75 14.77 7.01 < 5 -1 2 0 3297.00 3288.55 32.66 o 5 -1 2 2 4.57 2.52 6.91 < 7 -1 2 -2 5.71 8.40 10.17 < 7 -1 2 0 7059.22 7163.68 57.42 o 7 -1 2 2 50.18 47.90 11.40 o 9 -1 2 -2 1.52 6.89 18.07 < 9 -1 2 0 5622.97 5509.97 69.52 o 9 -1 2 2 48.99 63.79 18.73 o -10 0 2 -2 4.12 10.19 19.65 < -10 0 2 0 2311.01 2347.29 54.32 o -10 0 2 2 2.47 3.27 18.04 < -8 0 2 -2 104.29 109.69 16.49 o -8 0 2 0 19218.40 18947.60 103.62 o -8 0 2 2 14.87 27.57 12.30 < -6 0 2 -2 0.27 -0.11 5.29 < -6 0 2 0 202.46 228.33 9.64 o -6 0 2 2 50.81 52.85 6.73 o -4 0 2 -2 23.85 26.24 3.78 o -4 0 2 0 14223.50 16672.70 42.25 o -4 0 2 2 3.19 6.73 3.16 < -2 0 2 -2 1.94 3.14 2.68 < -2 0 2 0 64967.40 65498.50 190.37 o -2 0 2 2 109.73 104.04 3.73 o 0 0 2 -2 34.24 27.52 2.43 o 0 0 2 0 334.16 315.98 4.69 o 0 0 2 2 37.10 31.23 1.92 o 2 0 2 -2 0.14 1.10 3.94 < 2 0 2 0 78.80 41.21 5.01 o 2 0 2 2 14.10 16.81 3.43 o 4 0 2 -2 1.21 1.05 4.92 < 4 0 2 0 7631.90 7630.82 34.35 o 4 0 2 2 48.40 52.57 5.27 o 6 0 2 -2 23.34 22.58 9.02 < 6 0 2 0 8396.30 8201.58 55.87 o 6 0 2 2 23.38 21.18 8.79 < 8 0 2 -2 9.41 2.68 13.37 < 8 0 2 0 1116.35 1101.98 33.06 o 8 0 2 2 0.18 1.81 13.44 < -9 1 2 -2 1.61 -0.78 14.27 < -9 1 2 0 1897.84 1854.68 39.06 o -9 1 2 2 53.80 54.65 15.84 o -7 1 2 -2 3.73 5.98 7.72 < -7 1 2 0 1966.63 1850.64 23.10 o -7 1 2 2 0.01 1.40 7.44 < -5 1 2 -2 6.96 8.43 4.17 < -5 1 2 0 11247.50 11279.90 38.59 o -5 1 2 2 1.19 1.03 3.73 < -3 1 2 -2 1.73 4.24 2.59 < -3 1 2 0 1268.44 1341.93 10.68 o -3 1 2 2 26.02 23.29 2.89 o -1 1 2 -2 25.87 27.38 2.59 o -1 1 2 0 318.21 314.05 5.15 o -1 1 2 2 9.54 10.14 1.40 o 1 1 2 -2 31.31 26.97 3.32 o 1 1 2 0 26238.20 27142.10 84.61 o 1 1 2 2 10.82 9.96 2.47 o 3 1 2 -2 0.02 0.44 4.40 < 3 1 2 0 7916.10 8826.45 36.62 o 3 1 2 2 41.66 46.00 4.88 o 5 1 2 -2 0.07 -0.34 6.94 < 5 1 2 0 2180.76 2286.69 28.10 o 5 1 2 2 27.08 29.56 7.78 o 7 1 2 -2 0.10 10.58 10.62 < 7 1 2 0 11255.90 11161.50 71.84 o 7 1 2 2 60.90 56.55 11.93 o 9 1 2 -2 5.10 8.40 18.29 < 9 1 2 0 5572.97 5772.05 72.06 o 9 1 2 2 31.78 41.24 21.59 < -10 2 2 -2 66.13 61.93 21.09 < -10 2 2 0 5998.90 5995.06 79.41 o -10 2 2 2 0.46 7.26 16.92 < -8 2 2 -2 7.82 4.08 9.59 < -8 2 2 0 678.40 666.70 21.95 o -8 2 2 2 0.05 4.79 11.54 < -6 2 2 -2 67.58 68.48 6.48 o -6 2 2 0 5555.25 5795.37 30.96 o -6 2 2 2 11.81 11.88 4.92 < -4 2 2 -2 16.24 15.50 3.55 o -4 2 2 0 379.34 354.18 6.98 o -4 2 2 2 4.80 7.12 3.11 < -2 2 2 -2 41.54 42.86 2.68 o -2 2 2 0 409.07 442.19 5.22 o -2 2 2 2 11.48 13.39 2.93 o 0 2 2 -2 1.33 -0.02 2.27 < 0 2 2 0 0.31 11.20 2.13 o 0 2 2 2 11.01 10.37 2.13 o 2 2 2 -2 1.69 0.80 2.89 < 2 2 2 0 7918.44 8334.98 29.43 o 2 2 2 2 2.79 2.79 2.98 < 4 2 2 -2 2.55 0.09 4.69 < 4 2 2 0 2.11 6.34 4.85 < 4 2 2 2 4.38 3.21 4.85 < 6 2 2 -2 0.82 -0.39 8.45 < 6 2 2 0 30.11 30.86 9.34 o 6 2 2 2 2.41 0.16 8.43 < 8 2 2 -2 25.96 27.45 15.48 < 8 2 2 0 34.45 34.83 16.21 < 8 2 2 2 0.02 -0.87 13.60 < -9 3 2 -2 0.36 0.16 14.01 < -9 3 2 0 1128.51 1074.00 30.39 o -9 3 2 2 3.43 8.95 13.58 < -7 3 2 -2 33.55 37.67 7.30 o -7 3 2 0 119.74 115.12 8.93 o -7 3 2 2 3.69 5.36 6.41 < -5 3 2 -2 11.96 10.12 4.21 < -5 3 2 0 6955.42 6963.18 30.36 o -5 3 2 2 11.91 13.92 4.10 o -3 3 2 -2 4.34 6.80 2.52 < -3 3 2 0 15686.20 16695.90 56.94 o -3 3 2 2 27.57 30.29 4.81 o -1 3 2 -2 2.67 5.06 2.43 < -1 3 2 0 1579.41 1699.88 11.43 o -1 3 2 2 24.64 28.21 3.00 o 1 3 2 -2 8.11 12.02 2.68 o 1 3 2 0 39118.60 39324.50 120.60 o 1 3 2 2 12.05 10.51 3.16 o 3 3 2 -2 16.39 18.20 4.40 o 3 3 2 0 6423.92 6155.51 29.77 o 3 3 2 2 30.98 25.16 4.42 o 5 3 2 -2 6.49 6.34 7.56 < 5 3 2 0 4342.81 4421.45 39.40 o 5 3 2 2 2.55 2.98 7.58 < 7 3 2 -2 2.32 3.69 10.07 < 7 3 2 0 780.01 735.12 23.07 o 7 3 2 2 5.20 10.97 12.18 < 9 3 2 -2 0.22 5.63 21.84 < 9 3 2 0 424.22 358.97 31.47 o 9 3 2 2 3.14 1.44 21.84 < -10 4 2 -2 5.83 5.31 17.38 < -10 4 2 0 175.44 185.77 22.02 o -10 4 2 2 27.75 11.20 17.31 < -8 4 2 -2 2.74 4.19 10.49 < -8 4 2 0 1097.16 1042.55 24.87 o -8 4 2 2 20.51 17.84 10.99 < -6 4 2 -2 20.88 26.03 5.66 o -6 4 2 0 12937.50 13229.60 46.71 o -6 4 2 2 13.06 15.43 5.36 < -4 4 2 -2 69.54 68.48 6.39 o -4 4 2 0 17189.60 18090.90 68.38 o -4 4 2 2 12.55 11.91 5.24 < -2 4 2 -2 13.71 13.37 2.86 o -2 4 2 0 43017.00 43446.20 120.99 o -2 4 2 2 0.24 -0.39 2.45 < 0 4 2 -2 3.37 0.98 2.75 < 0 4 2 0 887.83 827.83 9.88 o 0 4 2 2 10.51 9.16 3.11 < 2 4 2 -2 30.10 27.11 4.37 o 2 4 2 0 3139.29 3786.61 24.15 o 2 4 2 2 3.58 1.79 3.87 < 4 4 2 -2 4.80 5.86 5.66 < 4 4 2 0 20063.20 19059.50 69.00 o 4 4 2 2 68.15 67.91 7.72 o 6 4 2 -2 10.42 11.36 9.34 < 6 4 2 0 3344.58 3261.52 42.29 o 6 4 2 2 3.48 1.35 9.89 < 8 4 2 -2 0.26 0.53 17.65 < 8 4 2 0 774.44 729.99 35.04 o 8 4 2 2 1.55 -4.79 17.61 < -9 5 2 -2 2.65 0.96 12.75 < -9 5 2 0 182.84 172.88 19.35 o -9 5 2 2 50.72 53.67 15.66 o -7 5 2 -2 0.05 4.08 6.41 < -7 5 2 0 4040.01 4060.19 29.10 o -7 5 2 2 27.33 28.74 7.42 o -5 5 2 -2 0.12 4.46 5.61 < -5 5 2 0 7920.80 7980.32 42.52 o -5 5 2 2 9.35 13.60 6.21 < -3 5 2 -2 47.73 54.45 4.37 o -3 5 2 0 4152.73 4910.16 23.49 o -3 5 2 2 0.23 1.08 3.11 < -1 5 2 -2 23.09 24.73 3.34 o -1 5 2 0 7064.76 6317.48 25.43 o -1 5 2 2 1.19 2.68 2.66 < 1 5 2 -2 47.85 51.77 4.60 o 1 5 2 0 27274.30 27186.20 67.18 o 1 5 2 2 92.88 127.51 7.90 o 3 5 2 -2 3.96 1.19 5.11 < 3 5 2 0 23829.20 24452.00 75.57 o 3 5 2 2 2.63 6.43 5.13 < 5 5 2 -2 5.95 0.64 8.88 < 5 5 2 0 7.18 5.61 9.11 < 5 5 2 2 5.79 6.07 9.32 < 7 5 2 -2 3.74 0.64 12.82 < 7 5 2 0 342.19 379.69 25.32 o 7 5 2 2 0.76 2.13 15.55 < 9 5 2 -2 5.10 -2.47 23.22 < 9 5 2 0 878.97 888.83 45.10 o 9 5 2 2 1.03 -1.99 23.17 < -10 6 2 -2 1.90 1.08 18.23 < -10 6 2 0 2239.49 2152.91 45.04 o -10 6 2 2 33.75 27.91 18.52 < -8 6 2 -2 34.41 43.39 11.75 o -8 6 2 0 1926.79 1807.83 30.53 o -8 6 2 2 15.95 15.91 9.80 < -6 6 2 -2 8.25 5.08 6.46 < -6 6 2 0 222.61 206.53 11.70 o -6 6 2 2 22.63 17.26 6.75 < -4 6 2 -2 14.22 24.87 5.24 o -4 6 2 0 40371.50 41043.20 101.66 o -4 6 2 2 4.17 10.56 4.10 < -2 6 2 -2 19.46 14.52 3.55 o -2 6 2 0 8.75 20.26 3.50 o -2 6 2 2 21.62 14.45 3.62 o 0 6 2 -2 0.26 1.05 3.64 < 0 6 2 0 15708.80 16540.40 53.99 o 0 6 2 2 20.14 19.46 4.14 o 2 6 2 -2 22.03 23.49 5.15 o 2 6 2 0 2478.08 2432.32 22.10 o 2 6 2 2 29.73 32.42 5.59 o 4 6 2 -2 0.31 3.53 6.91 < 4 6 2 0 512.87 492.75 15.22 o 4 6 2 2 1.74 4.95 7.01 < 6 6 2 -2 5.11 2.79 11.49 < 6 6 2 0 2689.25 2678.29 41.42 o 6 6 2 2 0.76 1.88 11.31 < 8 6 2 -2 4.74 0.82 19.07 < 8 6 2 0 75.05 91.52 22.80 o 8 6 2 2 2.07 -6.78 19.33 < -9 7 2 -2 8.20 4.14 17.17 < -9 7 2 0 2512.12 2505.24 48.01 o -9 7 2 2 19.28 16.35 14.93 < -7 7 2 -2 1.02 -1.24 7.37 < -7 7 2 0 457.71 445.87 14.31 o -7 7 2 2 76.90 74.16 9.62 o -5 7 2 -2 45.83 46.69 7.53 o -5 7 2 0 8222.06 8076.93 45.81 o -5 7 2 2 21.95 26.40 6.41 o -3 7 2 -2 26.15 27.96 4.58 o -3 7 2 0 89.92 87.03 5.54 o -3 7 2 2 34.86 34.55 4.69 o -1 7 2 -2 126.46 134.83 6.57 o -1 7 2 0 4892.53 5334.47 27.51 o -1 7 2 2 49.71 53.35 4.88 o 1 7 2 -2 0.83 2.06 4.69 < 1 7 2 0 2161.23 2247.28 20.92 o 1 7 2 2 14.11 14.06 4.88 < 3 7 2 -2 29.28 32.03 6.85 o 3 7 2 0 2766.24 2783.44 26.83 o 3 7 2 2 72.11 77.60 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18.84 7.21 < -2 10 2 -2 0.33 3.39 6.04 < -2 10 2 0 9660.64 9520.90 48.23 o -2 10 2 2 7.21 8.63 5.91 < 0 10 2 -2 24.71 22.23 7.10 o 0 10 2 0 93.21 116.36 9.71 o 0 10 2 2 0.64 -1.74 6.57 < 2 10 2 -2 9.32 6.30 7.67 < 2 10 2 0 1832.03 1861.18 26.80 o 2 10 2 2 4.89 6.07 7.60 < 4 10 2 -2 0.34 4.53 10.62 < 4 10 2 0 1251.02 1251.72 28.16 o 4 10 2 2 23.18 13.12 10.78 < 6 10 2 -2 15.27 9.09 17.40 < 6 10 2 0 741.11 724.29 32.77 o 6 10 2 2 13.83 15.59 22.10 < 8 10 2 -2 10.02 -4.14 33.06 < -7 11 2 -2 0.02 -3.30 14.63 < -7 11 2 0 36.67 26.95 15.78 < -7 11 2 2 22.32 10.94 14.86 < -5 11 2 -2 2.86 8.40 9.80 < -5 11 2 0 599.17 593.24 20.01 o -5 11 2 2 35.17 30.34 9.62 o -3 11 2 -2 1.56 5.50 8.33 < -3 11 2 0 305.73 280.00 15.86 o -3 11 2 2 73.43 72.56 9.69 o -1 11 2 -2 1.18 -0.80 7.56 < -1 11 2 0 0.29 6.18 8.43 < -1 11 2 2 48.78 45.63 10.37 o 1 11 2 -2 0.31 -2.72 9.04 < 1 11 2 0 1063.15 1026.70 24.41 o 1 11 2 2 19.34 15.82 8.13 < 3 11 2 -2 4.74 6.18 10.76 < 3 11 2 0 1618.15 1565.39 30.38 o 3 11 2 2 13.96 11.91 9.82 < 5 11 2 -2 0.88 5.91 19.81 < 5 11 2 0 352.93 381.41 31.00 o 5 11 2 2 1.60 1.10 15.30 < 7 11 2 -2 0.15 -9.11 37.21 < 7 11 2 0 301.46 295.73 55.79 o 7 11 2 2 5.33 9.62 40.92 < -8 12 2 -2 0.28 -4.69 27.84 < -8 12 2 0 472.03 422.37 42.26 o -8 12 2 2 1.26 0.05 27.36 < -6 12 2 -2 7.13 5.04 11.70 < -6 12 2 0 65.80 72.49 13.97 o -6 12 2 2 4.29 7.10 11.75 < -4 12 2 -2 53.29 71.16 12.23 o -4 12 2 0 7730.89 7618.84 58.96 o -4 12 2 2 2.49 7.62 9.34 < -2 12 2 -2 5.98 1.37 9.41 < -2 12 2 0 477.14 539.74 24.68 o -2 12 2 2 8.68 11.65 11.84 < 0 12 2 -2 2.42 -2.75 10.37 < 0 12 2 0 0.27 16.19 11.93 < 0 12 2 2 3.19 -2.45 11.59 < 2 12 2 -2 0.80 9.23 11.31 < 2 12 2 0 8784.94 8928.01 69.88 o 2 12 2 2 65.25 75.40 13.53 o 4 12 2 -2 0.16 -1.47 14.97 < 4 12 2 0 3052.37 3004.76 51.67 o 4 12 2 2 46.59 42.31 16.69 < 6 12 2 -2 14.64 8.61 37.41 < 6 12 2 0 1987.77 2066.50 94.16 o 6 12 2 2 37.17 55.32 40.00 < -7 13 2 -2 7.50 14.61 18.62 < -7 13 2 0 2601.27 2548.98 50.09 o -7 13 2 2 33.56 36.15 22.83 < -5 13 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0 1238.88 1139.88 67.56 o 4 16 2 2 1.41 -4.33 29.13 < -3 17 2 -2 77.67 90.62 24.48 o -3 17 2 0 1069.96 980.33 42.36 o -3 17 2 2 1.90 -0.07 20.42 < -1 17 2 -2 4.13 6.48 20.56 < -1 17 2 0 12.38 3.02 20.15 < -1 17 2 2 34.81 29.83 22.21 < 1 17 2 -2 53.54 65.99 24.55 < 1 17 2 0 4360.44 4419.94 76.51 o 1 17 2 2 14.25 18.09 23.26 < -2 18 2 -2 3.42 7.42 21.89 < -2 18 2 0 3474.56 3503.59 92.96 o 0 18 2 -2 34.57 51.56 25.14 < 0 18 2 0 288.99 360.64 35.48 o 0 18 2 2 9.40 12.20 24.11 < -1 -18 3 -1 883.53 834.15 44.72 o -1 -18 3 1 1260.10 1301.63 50.31 o 1 -18 3 -1 6.42 -1.26 22.39 < 1 -18 3 1 3.82 11.61 22.69 < -4 -17 3 -1 789.20 786.27 75.91 o -4 -17 3 1 1091.54 1134.66 84.08 o -2 -17 3 -1 927.66 999.24 43.96 o -2 -17 3 1 706.25 747.71 40.74 o 0 -17 3 -1 43.25 33.20 22.12 < 0 -17 3 1 106.97 76.79 22.62 o 2 -17 3 -1 1563.20 1594.63 43.74 o 2 -17 3 1 1252.79 1343.26 41.51 o -5 -16 3 -1 146.46 183.30 50.90 o -5 -16 3 1 0.04 -6.39 35.88 < -3 -16 3 -1 273.91 314.42 36.97 o -3 -16 3 1 73.05 65.83 22.94 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12142.00 11908.60 45.29 o 3 3 4 2 82.97 81.51 6.59 o 5 3 4 -2 0.25 -2.34 8.36 < 5 3 4 0 658.43 634.32 19.13 o 5 3 4 2 12.91 9.43 8.72 < 7 3 4 -2 4.61 13.37 12.94 < 7 3 4 0 3197.44 3227.88 44.37 o 7 3 4 2 11.67 17.93 12.52 < 9 3 4 -2 14.93 9.94 28.58 < 9 3 4 0 658.57 656.48 40.94 o 9 3 4 2 1.89 10.21 24.59 < -10 4 4 -2 19.23 11.47 16.35 < -10 4 4 0 1434.86 1394.65 36.86 o -10 4 4 2 0.23 2.18 14.52 < -8 4 4 -2 23.11 19.14 9.00 < -8 4 4 0 52.71 43.94 9.94 o -8 4 4 2 7.10 6.89 8.38 < -6 4 4 -2 12.48 16.85 5.04 o -6 4 4 0 24103.50 23024.50 58.80 o -6 4 4 2 33.57 31.41 4.97 o -4 4 4 -2 44.65 41.40 4.08 o -4 4 4 0 18154.90 19101.80 46.71 o -4 4 4 2 0.01 0.14 3.02 < -2 4 4 -2 4.02 4.79 3.11 < -2 4 4 0 6723.11 6663.31 28.13 o -2 4 4 2 0.55 -0.87 2.54 < 0 4 4 -2 6.00 6.30 3.53 < 0 4 4 0 5760.84 5561.85 25.30 o 0 4 4 2 3.17 5.20 3.14 < 2 4 4 -2 15.40 19.37 4.67 o 2 4 4 0 20410.80 21603.20 57.79 o 2 4 4 2 6.99 1.60 4.10 < 4 4 4 -2 92.65 90.05 10.01 o 4 4 4 0 17470.40 16478.60 74.35 o 4 4 4 2 13.63 12.14 7.76 < 6 4 4 -2 16.90 19.03 11.33 < 6 4 4 0 1495.08 1410.71 29.19 o 6 4 4 2 26.32 20.08 11.01 < 8 4 4 -2 3.82 -8.27 21.13 < 8 4 4 0 1771.46 1679.89 51.16 o 8 4 4 2 8.72 10.37 21.64 < -9 5 4 -2 18.79 12.87 12.73 < -9 5 4 0 584.41 561.29 22.16 o -9 5 4 2 4.90 7.65 11.79 < -7 5 4 -2 12.39 13.17 6.87 < -7 5 4 0 9330.45 9475.41 40.03 o -7 5 4 2 11.22 11.20 5.61 < -5 5 4 -2 40.42 50.65 5.17 o -5 5 4 0 465.61 525.88 9.66 o -5 5 4 2 77.29 77.94 5.33 o -3 5 4 -2 5.19 8.40 3.39 < -3 5 4 0 4017.08 4347.88 22.07 o -3 5 4 2 44.86 46.14 4.30 o -1 5 4 -2 43.73 44.95 6.20 o -1 5 4 0 4585.07 5898.76 44.36 o -1 5 4 2 14.32 19.51 4.65 o 1 5 4 -2 5.60 7.28 4.12 < 1 5 4 0 8563.00 8641.11 35.42 o 1 5 4 2 29.44 31.41 4.67 o 3 5 4 -2 7.33 7.21 5.40 < 3 5 4 0 3250.92 3033.22 29.33 o 3 5 4 2 7.78 7.17 5.82 < 5 5 4 -2 37.67 30.04 10.14 < 5 5 4 0 13561.20 13380.80 84.10 o 5 5 4 2 21.28 22.90 11.06 < 7 5 4 -2 3.51 2.40 14.95 < 7 5 4 0 49.94 65.10 17.22 o 7 5 4 2 1.50 -1.21 15.20 < -10 6 4 -2 14.99 15.18 17.61 < -10 6 4 0 4473.78 4286.71 52.04 o -10 6 4 2 1.17 -3.85 15.25 < -8 6 4 -2 1.56 0.48 9.39 < -8 6 4 0 2724.07 2644.47 31.66 o -8 6 4 2 3.61 4.99 7.62 < -6 6 4 -2 0.18 0.94 5.06 < -6 6 4 0 43.51 73.57 6.43 o -6 6 4 2 15.18 15.30 6.80 < -4 6 4 -2 13.42 21.16 4.28 o -4 6 4 0 33487.10 32810.00 71.86 o -4 6 4 2 33.75 43.60 4.72 o -2 6 4 -2 16.25 20.31 3.71 o -2 6 4 0 10930.40 11287.60 45.79 o -2 6 4 2 14.07 18.04 4.05 o 0 6 4 -2 7.40 8.22 4.14 < 0 6 4 0 15745.20 16176.30 48.98 o 0 6 4 2 51.36 47.40 4.99 o 2 6 4 -2 98.17 99.18 8.08 o 2 6 4 0 37822.70 36390.10 89.06 o 2 6 4 2 20.59 17.17 5.84 < 4 6 4 -2 12.10 10.17 10.05 < 4 6 4 0 3019.72 2846.63 43.52 o 4 6 4 2 88.90 82.31 11.84 o 6 6 4 -2 30.53 26.79 14.22 < 6 6 4 0 1470.90 1364.38 34.45 o 6 6 4 2 1.55 3.80 12.98 < 8 6 4 -2 4.63 5.52 22.83 < 8 6 4 0 7670.37 8093.52 101.09 o 8 6 4 2 70.63 84.62 25.87 o -9 7 4 -2 1.46 4.33 16.19 < -9 7 4 0 755.32 723.36 30.51 o -9 7 4 2 6.27 -3.14 15.09 < -7 7 4 -2 65.64 63.72 9.34 o -7 7 4 0 3389.75 3331.68 31.67 o -7 7 4 2 21.98 25.07 8.33 o -5 7 4 -2 0.36 0.71 4.67 < -5 7 4 0 206.78 234.37 8.43 o -5 7 4 2 5.28 5.01 5.29 < -3 7 4 -2 72.21 86.73 5.88 o -3 7 4 0 2461.64 2545.23 20.41 o -3 7 4 2 21.75 22.14 4.56 o -1 7 4 -2 12.73 17.97 5.79 o -1 7 4 0 91.47 88.84 6.57 o -1 7 4 2 21.83 21.48 5.17 o 1 7 4 -2 34.21 32.42 5.95 o 1 7 4 0 496.59 517.20 11.63 o 1 7 4 2 0.88 2.34 5.13 < 3 7 4 -2 1.36 3.62 8.49 < 3 7 4 0 260.85 240.43 13.21 o 3 7 4 2 6.88 4.44 7.24 < 5 7 4 -2 2.79 4.01 11.91 < 5 7 4 0 2100.47 2083.00 37.66 o 5 7 4 2 0.36 0.32 12.00 < 7 7 4 -2 9.34 1.79 17.47 < 7 7 4 0 170.62 163.20 25.71 o 7 7 4 2 12.05 15.14 20.77 < -10 8 4 -2 0.05 0.57 21.45 < -10 8 4 0 917.74 837.92 37.21 o -10 8 4 2 3.29 0.46 20.20 < -8 8 4 -2 2.28 14.45 11.27 < -8 8 4 0 6759.29 6855.72 53.67 o -8 8 4 2 6.91 5.93 10.78 < -6 8 4 -2 21.78 21.20 7.17 < -6 8 4 0 538.34 504.20 11.54 o -6 8 4 2 60.98 64.34 8.52 o -4 8 4 -2 0.02 11.17 4.99 < -4 8 4 0 39659.70 39090.90 83.26 o -4 8 4 2 9.73 20.56 5.36 o -2 8 4 -2 0.57 5.01 6.00 < -2 8 4 0 2550.37 2518.44 23.47 o -2 8 4 2 72.92 76.15 6.89 o 0 8 4 -2 69.51 76.50 8.47 o 0 8 4 0 1.01 28.19 6.00 o 0 8 4 2 16.36 12.96 5.47 < 2 8 4 -2 0.03 10.42 7.79 < 2 8 4 0 49796.90 48229.20 121.10 o 2 8 4 2 161.52 167.09 11.54 o 4 8 4 -2 16.13 11.81 12.66 < 4 8 4 0 582.37 561.91 24.51 o 4 8 4 2 11.83 7.28 12.20 < 6 8 4 -2 4.81 20.01 17.93 < 6 8 4 0 9415.22 9244.25 92.77 o 6 8 4 2 62.01 63.47 18.68 o -9 9 4 -2 12.29 14.97 26.40 < -9 9 4 0 9.61 1.69 25.26 < -9 9 4 2 70.93 58.52 27.50 < -7 9 4 -2 11.95 9.85 10.03 < -7 9 4 0 128.62 128.35 12.20 o -7 9 4 2 5.19 1.63 8.20 < -5 9 4 -2 81.96 76.40 8.95 o -5 9 4 0 6321.96 6359.06 38.38 o -5 9 4 2 16.18 20.77 6.25 o -3 9 4 -2 1.03 2.04 6.78 < -3 9 4 0 283.93 290.19 13.32 o -3 9 4 2 0.59 1.95 6.82 < -1 9 4 -2 16.86 17.22 7.40 < -1 9 4 0 15428.90 16013.40 70.99 o -1 9 4 2 29.00 32.61 7.37 o 1 9 4 -2 5.35 10.49 8.88 < 1 9 4 0 7277.96 7058.93 55.22 o 1 9 4 2 15.37 19.39 7.37 < 3 9 4 -2 0.50 3.55 11.29 < 3 9 4 0 294.83 329.00 17.06 o 3 9 4 2 6.33 9.41 9.50 < 5 9 4 -2 0.29 5.52 18.84 < 5 9 4 0 5957.81 6003.61 72.05 o 5 9 4 2 33.39 37.96 16.14 < 7 9 4 -2 0.01 -10.74 40.18 < 7 9 4 0 114.69 105.30 48.29 < 7 9 4 2 4.75 15.14 28.19 < -8 10 4 -2 28.81 36.09 17.54 < -8 10 4 0 859.00 797.31 42.45 o -8 10 4 2 25.70 21.55 15.89 < -6 10 4 -2 8.82 9.16 9.04 < -6 10 4 0 3582.38 3469.74 35.07 o -6 10 4 2 8.67 13.88 9.07 < -4 10 4 -2 19.62 26.45 9.07 < -4 10 4 0 4011.93 4033.82 38.75 o -4 10 4 2 16.45 18.82 7.95 < -2 10 4 -2 17.48 26.61 7.99 o -2 10 4 0 422.99 384.15 15.22 o -2 10 4 2 15.99 16.81 7.79 < 0 10 4 -2 0.15 9.73 7.74 < 0 10 4 0 9735.35 9606.95 58.80 o 0 10 4 2 62.78 54.10 9.85 o 2 10 4 -2 8.54 13.69 10.33 < 2 10 4 0 5709.14 5836.51 54.99 o 2 10 4 2 56.94 60.54 12.23 o 4 10 4 -2 1.91 5.01 18.23 < 4 10 4 0 3520.53 3475.03 69.11 o 4 10 4 2 34.73 31.03 19.81 < 6 10 4 -2 1.89 -7.26 24.91 < 6 10 4 0 160.78 147.05 31.25 o 6 10 4 2 10.91 8.77 24.87 < -7 11 4 -2 20.90 19.83 15.11 < -7 11 4 0 255.76 226.81 20.90 o -7 11 4 2 55.44 55.23 15.80 o -5 11 4 -2 24.06 20.88 10.14 < -5 11 4 0 1037.99 972.33 21.92 o -5 11 4 2 18.28 12.59 9.82 < -3 11 4 -2 0.02 0.57 8.24 < -3 11 4 0 2362.62 2410.48 32.33 o -3 11 4 2 34.55 35.56 9.16 o -1 11 4 -2 0.03 -1.40 7.88 < -1 11 4 0 282.93 303.03 15.52 o -1 11 4 2 2.18 -2.40 7.76 < 1 11 4 -2 1.42 -1.53 9.80 < 1 11 4 0 1071.44 1060.64 26.61 o 1 11 4 2 0.37 -1.53 10.01 < 3 11 4 -2 0.61 -7.30 13.37 < 3 11 4 0 358.52 350.75 24.95 o 3 11 4 2 0.05 4.17 13.69 < 5 11 4 -2 0.37 11.17 23.72 < 5 11 4 0 252.27 261.38 33.47 o 5 11 4 2 0.00 -3.78 22.94 < -8 12 4 -2 3.07 -3.32 25.51 < -8 12 4 0 1471.54 1498.68 52.78 o -8 12 4 2 0.16 1.42 18.59 < -6 12 4 -2 14.84 11.13 13.10 < -6 12 4 0 1649.17 1544.44 30.84 o -6 12 4 2 12.67 11.75 11.20 < -4 12 4 -2 19.04 19.78 11.86 < -4 12 4 0 7318.16 7320.78 65.06 o -4 12 4 2 54.88 56.58 12.68 o -2 12 4 -2 2.29 -3.27 9.09 < -2 12 4 0 49.14 76.34 11.72 o -2 12 4 2 22.08 12.94 10.49 < 0 12 4 -2 0.25 -3.92 10.44 < 0 12 4 0 550.86 547.69 21.90 o 0 12 4 2 68.31 56.42 11.97 o 2 12 4 -2 1.74 4.35 11.86 < 2 12 4 0 8775.42 8937.34 73.48 o 2 12 4 2 1.31 5.22 11.84 < 4 12 4 -2 7.94 4.81 21.91 < 4 12 4 0 229.32 271.91 32.81 o 4 12 4 2 24.98 33.64 23.84 < 6 12 4 -2 16.60 9.14 29.47 < 6 12 4 0 583.59 588.38 69.10 o 6 12 4 2 1.59 10.42 39.75 < -7 13 4 -2 19.01 15.48 20.74 < -7 13 4 0 72.65 66.49 15.84 o -7 13 4 2 96.75 113.45 17.61 o -5 13 4 -2 27.99 22.14 13.10 < -5 13 4 0 1630.16 1608.64 35.13 o -5 13 4 2 6.59 7.03 12.73 < -3 13 4 -2 3.19 5.17 11.86 < -3 13 4 0 1605.34 1643.16 34.63 o -3 13 4 2 46.51 42.38 13.07 o -1 13 4 -2 1.29 3.94 13.85 < -1 13 4 0 1692.56 1758.27 41.08 o -1 13 4 2 3.51 10.19 13.42 < 1 13 4 -2 32.63 29.22 13.19 < 1 13 4 0 192.91 166.90 17.79 o 1 13 4 2 6.19 7.85 14.38 < 3 13 4 -2 6.10 5.13 17.06 < 3 13 4 0 255.51 272.02 25.94 o 3 13 4 2 2.62 7.03 17.06 < 5 13 4 -2 0.37 -4.35 27.23 < 5 13 4 0 2579.43 2612.86 74.18 o 5 13 4 2 5.83 6.00 27.25 < -6 14 4 -2 0.10 18.13 16.74 < -6 14 4 0 8901.19 8937.43 80.22 o -6 14 4 2 28.32 46.44 16.99 < -4 14 4 -2 33.73 22.05 15.11 < -4 14 4 0 829.87 875.37 30.80 o -4 14 4 2 27.54 19.92 14.91 < -2 14 4 -2 19.65 24.64 15.80 < -2 14 4 0 735.31 693.86 30.55 o -2 14 4 2 67.89 68.51 17.47 o 0 14 4 -2 8.87 13.44 15.66 < 0 14 4 0 3258.83 3150.12 56.78 o 0 14 4 2 6.99 9.69 15.52 < 2 14 4 -2 6.01 9.55 18.36 < 2 14 4 0 2090.23 2190.95 53.44 o 2 14 4 2 14.16 10.58 19.07 < 4 14 4 -2 10.63 -5.50 38.86 < 4 14 4 0 2805.58 2735.32 106.33 o 4 14 4 2 0.10 19.12 38.65 < -5 15 4 -2 10.20 10.33 16.74 < -5 15 4 0 33.83 45.75 17.36 < -5 15 4 2 22.86 18.59 19.07 < -3 15 4 -2 0.03 -3.46 16.42 < -3 15 4 0 1537.00 1492.79 43.28 o -3 15 4 2 12.71 20.97 18.27 < -1 15 4 -2 11.52 2.04 16.39 < -1 15 4 0 91.75 116.93 21.25 o -1 15 4 2 14.69 11.61 17.15 < 1 15 4 -2 5.00 20.93 19.33 < 1 15 4 0 3306.98 3312.87 62.88 o 1 15 4 2 12.60 16.97 19.30 < 3 15 4 -2 2.03 2.36 28.87 < 3 15 4 0 438.11 469.67 42.55 o 3 15 4 2 12.14 8.20 26.54 < -4 16 4 -2 57.07 48.61 20.95 < -4 16 4 0 0.96 15.91 20.36 < -4 16 4 2 0.64 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4.44 o 1 4 5 1 381.42 393.01 8.26 o 3 4 5 -1 1.93 2.38 7.01 < 3 4 5 1 383.56 372.83 13.92 o 5 4 5 -1 50.39 53.14 11.31 o 5 4 5 1 59.37 55.50 11.40 o 7 4 5 -1 10.82 -0.46 14.22 < 7 4 5 1 21.41 22.32 16.33 < -10 5 5 -1 10.54 7.97 15.66 < -10 5 5 1 0.64 -0.57 15.80 < -8 5 5 -1 53.55 45.98 9.78 o -8 5 5 1 212.27 227.46 13.83 o -6 5 5 -1 131.35 134.21 7.30 o -6 5 5 1 443.99 422.95 10.07 o -4 5 5 -1 320.45 323.60 8.20 o -4 5 5 1 193.51 188.30 6.94 o -2 5 5 -1 4.82 10.10 4.69 < -2 5 5 1 199.14 178.02 8.15 o 0 5 5 -1 100.12 93.87 6.02 o 0 5 5 1 503.03 498.99 9.75 o 2 5 5 -1 222.00 225.91 9.41 o 2 5 5 1 133.24 127.60 7.92 o 4 5 5 -1 345.05 335.96 15.82 o 4 5 5 1 344.21 353.04 15.98 o 6 5 5 -1 28.54 17.26 14.40 < 6 5 5 1 28.95 24.73 14.20 < 8 5 5 -1 0.49 -7.28 24.20 < 8 5 5 1 204.44 211.02 30.40 o -9 6 5 -1 50.03 44.95 12.94 o -9 6 5 1 5.99 7.69 11.77 < -7 6 5 -1 564.81 552.76 12.68 o -7 6 5 1 183.02 190.23 9.50 o -5 6 5 -1 5.71 10.97 4.60 < -5 6 5 1 366.90 367.73 8.93 o -3 6 5 -1 3641.11 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9.02 7.85 < 0 4 10 -2 2.10 3.00 8.75 < 0 4 10 0 11863.40 11420.70 71.47 o 0 4 10 2 43.31 44.30 10.37 o 2 4 10 -2 2.39 1.56 15.62 < 2 4 10 0 7223.13 7371.01 93.44 o 2 4 10 2 0.13 3.80 9.50 < 4 4 10 -2 1.22 -13.07 21.39 < 4 4 10 0 57.57 70.34 21.11 o 4 4 10 2 23.84 27.48 13.51 < 6 4 10 -2 0.28 3.27 46.76 < 6 4 10 0 1317.55 1307.06 64.54 o 6 4 10 2 0.09 13.30 28.51 < -11 5 10 -2 6.07 -0.14 20.38 < -11 5 10 0 1443.00 1356.69 40.49 o -11 5 10 2 17.66 27.89 18.25 < -9 5 10 -2 0.41 3.23 14.40 < -9 5 10 0 5406.24 5484.60 69.93 o -9 5 10 2 0.27 8.36 15.14 < -7 5 10 -2 28.09 22.87 12.82 < -7 5 10 0 288.61 292.73 19.76 o -7 5 10 2 1.74 0.16 11.27 < -5 5 10 -2 1.81 -0.39 8.75 < -5 5 10 0 9201.39 8771.05 62.42 o -5 5 10 2 66.04 70.11 10.23 o -3 5 10 -2 12.67 16.49 8.77 < -3 5 10 0 24680.30 23786.10 101.00 o -3 5 10 2 0.08 4.53 7.99 < -1 5 10 -2 0.02 -0.44 8.75 < -1 5 10 0 19867.10 19350.80 105.90 o -1 5 10 2 0.04 1.88 8.72 < 1 5 10 -2 15.32 11.70 16.17 < 1 5 10 0 7790.38 7420.44 94.13 o 1 5 10 2 24.51 20.61 16.26 < 3 5 10 -2 29.53 13.28 20.42 < 3 5 10 0 2221.41 2122.58 60.52 o 3 5 10 2 1.66 -6.69 18.32 < 5 5 10 -2 23.05 11.04 28.55 < 5 5 10 0 1327.25 1259.70 59.37 o 5 5 10 2 0.04 -8.40 27.13 < -10 6 10 -2 32.33 28.55 18.29 < -10 6 10 0 1544.81 1496.14 39.35 o -10 6 10 2 1.93 3.98 16.58 < -8 6 10 -2 10.88 9.87 14.54 < -8 6 10 0 1512.12 1501.00 37.97 o -8 6 10 2 0.04 3.23 12.96 < -6 6 10 -2 24.55 35.33 12.68 < -6 6 10 0 30576.20 30337.00 120.77 o -6 6 10 2 15.43 21.78 9.98 < -4 6 10 -2 12.79 21.07 9.91 < -4 6 10 0 19.36 17.86 9.36 < -4 6 10 2 41.29 36.38 9.89 o -2 6 10 -2 1.20 6.34 9.11 < -2 6 10 0 32350.10 32136.10 121.81 o -2 6 10 2 77.42 68.94 10.69 o 0 6 10 -2 0.55 -3.00 8.75 < 0 6 10 0 3169.73 3346.86 37.21 o 0 6 10 2 4.80 2.54 8.15 < 2 6 10 -2 17.95 19.62 18.66 < 2 6 10 0 322.20 320.70 31.25 o 2 6 10 2 9.02 13.12 17.17 < 4 6 10 -2 6.30 19.44 25.39 < 4 6 10 0 6875.69 7141.23 111.85 o 4 6 10 2 9.55 24.48 24.02 < -9 7 10 -2 4.28 7.37 16.44 < -9 7 10 0 2534.52 2567.54 51.27 o -9 7 10 2 4.61 8.66 15.23 < -7 7 10 -2 27.92 31.00 14.40 < -7 7 10 0 1223.10 1187.58 34.07 o -7 7 10 2 14.30 16.76 11.86 < -5 7 10 -2 0.87 3.18 9.37 < -5 7 10 0 0.05 2.31 9.53 < -5 7 10 2 18.97 20.54 9.78 < -3 7 10 -2 39.89 44.24 10.49 o -3 7 10 0 8778.69 8765.84 66.34 o -3 7 10 2 10.63 9.91 9.41 < -1 7 10 -2 0.51 3.87 11.63 < -1 7 10 0 280.49 299.55 16.07 o -1 7 10 2 11.69 14.81 8.68 < 1 7 10 -2 3.69 4.46 17.15 < 1 7 10 0 8312.00 8143.05 103.46 o 1 7 10 2 2.61 5.77 16.39 < 3 7 10 -2 0.54 3.76 21.29 < 3 7 10 0 257.07 234.50 32.14 o 3 7 10 2 8.66 3.85 22.32 < 5 7 10 -2 9.07 8.33 31.69 < 5 7 10 0 1031.55 1128.27 61.05 o 5 7 10 2 22.42 23.13 29.15 < -10 8 10 -2 4.19 10.88 19.07 < -10 8 10 0 4.90 11.01 17.33 < -10 8 10 2 4.31 1.99 16.99 < -8 8 10 -2 7.06 9.18 15.75 < -8 8 10 0 4513.74 4464.81 62.71 o -8 8 10 2 20.14 25.28 15.20 < -6 8 10 -2 4.30 0.21 11.40 < -6 8 10 0 189.06 216.42 16.74 o -6 8 10 2 12.52 6.23 10.01 < -4 8 10 -2 0.88 1.88 9.73 < -4 8 10 0 1585.34 1549.23 31.06 o -4 8 10 2 7.87 6.07 9.62 < -2 8 10 -2 2.98 1.99 11.86 < -2 8 10 0 1358.80 1356.37 26.79 o -2 8 10 2 2.64 1.95 8.70 < 0 8 10 -2 2.15 -0.87 10.24 < 0 8 10 0 2781.61 2907.56 37.73 o 0 8 10 2 16.04 19.55 10.42 < 2 8 10 -2 0.57 -3.62 19.60 < 2 8 10 0 888.82 857.72 44.62 o 2 8 10 2 4.95 7.58 19.90 < 4 8 10 -2 0.86 0.32 26.42 < 4 8 10 0 1253.37 1296.82 58.09 o 4 8 10 2 8.54 11.06 27.06 < -9 9 10 -2 31.99 45.84 19.99 < -9 9 10 0 6602.80 6782.36 81.16 o -9 9 10 2 2.76 17.24 18.50 < -7 9 10 -2 6.64 5.56 14.93 < -7 9 10 0 28.20 36.18 15.07 < -7 9 10 2 25.81 27.20 14.91 < -5 9 10 -2 31.25 33.89 12.30 < -5 9 10 0 1192.57 1233.84 29.74 o -5 9 10 2 26.03 25.12 11.43 < -3 9 10 -2 19.37 29.95 14.36 < -3 9 10 0 15633.30 15550.70 84.62 o -3 9 10 2 24.06 30.98 10.26 o -1 9 10 -2 20.96 21.73 11.04 < -1 9 10 0 5.19 20.22 10.72 < -1 9 10 2 3.55 3.18 9.82 < 1 9 10 -2 19.02 9.53 20.72 < 1 9 10 0 438.08 440.34 35.92 o 1 9 10 2 9.09 3.30 18.36 < 3 9 10 -2 0.58 10.46 25.16 < 3 9 10 0 9976.36 9963.78 132.42 o 3 9 10 2 33.19 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821.85 26.29 o -1 11 10 2 1.46 2.22 11.24 < 1 11 10 -2 3.17 -6.34 22.35 < 1 11 10 0 1619.59 1582.14 57.35 o 1 11 10 2 33.92 41.17 24.41 < 3 11 10 -2 31.51 39.98 30.84 < 3 11 10 0 15.93 16.74 30.13 < 3 11 10 2 0.01 1.37 27.23 < -8 12 10 -2 20.06 25.83 18.78 < -8 12 10 0 612.90 569.59 31.36 o -8 12 10 2 0.50 2.68 18.04 < -6 12 10 -2 70.04 52.68 15.11 o -6 12 10 0 2229.03 2147.52 39.78 o -6 12 10 2 1.87 -0.50 13.88 < -4 12 10 -2 13.28 23.47 13.72 < -4 12 10 0 2901.61 2848.16 43.53 o -4 12 10 2 20.06 30.87 13.69 < -2 12 10 -2 0.20 0.69 13.37 < -2 12 10 0 2697.09 2714.01 42.51 o -2 12 10 2 4.47 1.88 12.52 < 0 12 10 -2 17.55 15.87 14.86 < 0 12 10 0 1580.32 1617.99 40.67 o 0 12 10 2 33.31 35.01 17.08 < 2 12 10 -2 28.32 25.28 27.55 < 2 12 10 0 626.74 612.50 48.82 o 2 12 10 2 0.10 -1.49 27.66 < -7 13 10 -2 35.32 25.26 19.05 < -7 13 10 0 212.32 221.20 28.62 o -7 13 10 2 1.38 -3.21 20.29 < -5 13 10 -2 1.32 -2.63 15.11 < -5 13 10 0 466.91 457.01 25.66 o -5 13 10 2 56.03 45.31 15.75 < -3 13 10 -2 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21.05 16.81 29.22 < -8 3 17 -1 45.49 42.84 22.14 < -8 3 17 1 3.17 10.72 19.49 < -6 3 17 -1 844.24 813.27 37.83 o -6 3 17 1 0.49 7.12 16.53 < -4 3 17 -1 72.03 52.73 23.06 < -4 3 17 1 134.90 137.88 21.02 o -2 3 17 -1 94.68 85.95 27.70 o -2 3 17 1 26.50 29.38 23.13 < 0 3 17 -1 0.05 4.30 27.55 < 0 3 17 1 15.80 18.82 27.98 < -9 4 17 -1 54.32 53.28 24.48 < -9 4 17 1 8.02 3.69 22.05 < -7 4 17 -1 14.55 18.11 20.93 < -7 4 17 1 190.90 161.11 25.41 o -5 4 17 -1 470.26 469.57 33.19 o -5 4 17 1 44.60 46.02 20.13 < -3 4 17 -1 28.85 32.10 24.89 < -3 4 17 1 199.64 193.04 30.88 o -1 4 17 -1 157.13 141.35 33.34 o -1 4 17 1 346.00 305.18 37.04 o -8 5 17 -1 1175.43 1276.10 46.69 o -8 5 17 1 165.44 159.94 25.78 o -6 5 17 -1 152.13 148.24 24.63 o -6 5 17 1 0.19 -3.57 18.73 < -4 5 17 -1 564.60 525.76 30.30 o -4 5 17 1 4.63 2.68 16.28 < -2 5 17 -1 145.11 148.25 32.05 o -2 5 17 1 16.50 15.68 24.27 < 0 5 17 1 275.30 260.57 40.89 o -7 6 17 -1 18.52 22.99 21.41 < -7 6 17 1 25.45 25.48 21.20 < -5 6 17 -1 7.04 4.74 20.31 < -5 6 17 1 68.91 49.36 21.52 < -3 6 17 -1 1.62 -2.50 25.83 < -3 6 17 1 127.92 137.60 31.73 o -1 6 17 -1 0.60 -4.40 27.89 < -1 6 17 1 26.10 29.65 28.42 < -8 7 17 1 19.83 27.80 23.63 < -6 7 17 -1 34.06 28.69 22.21 < -6 7 17 1 14.91 16.23 20.47 < -4 7 17 -1 127.31 118.67 22.05 o -4 7 17 1 56.82 75.03 20.33 o -2 7 17 -1 92.63 81.60 32.88 < -2 7 17 1 174.57 180.82 35.56 o -7 8 17 1 307.73 321.04 33.17 o -5 8 17 -1 453.88 454.32 36.53 o -5 8 17 1 4.02 1.47 21.59 < -3 8 17 -1 9.72 -3.23 29.42 < -3 8 17 1 0.80 -3.94 27.71 < -4 9 17 1 8.66 19.14 18.29 < -4 -10 18 2 2.99 3.09 28.76 < -7 -9 18 2 0.02 4.92 28.26 < -5 -9 18 0 1869.30 1675.55 66.39 o -5 -9 18 2 11.02 12.36 26.42 < -3 -9 18 0 155.62 189.04 51.97 o -3 -9 18 2 9.50 10.56 37.05 < -8 -8 18 2 8.49 34.41 40.55 < -6 -8 18 -2 0.66 17.08 28.05 < -6 -8 18 0 122.79 99.00 31.32 o -6 -8 18 2 53.27 26.42 26.15 < -4 -8 18 -2 0.03 42.54 29.10 < -4 -8 18 0 3931.44 3809.53 88.33 o -4 -8 18 2 69.51 59.05 27.36 < -2 -8 18 0 2104.48 2147.09 104.22 o -2 -8 18 2 14.71 5.24 27.64 < -7 -7 18 -2 17.93 27.18 29.45 < -7 -7 18 0 1077.06 938.08 54.16 o -7 -7 18 2 5.91 1.37 26.22 < -5 -7 18 -2 64.64 72.01 28.67 < -5 -7 18 0 1564.13 1535.62 60.04 o -5 -7 18 2 4.08 13.76 24.43 < -3 -7 18 -2 26.94 34.48 39.52 < -3 -7 18 0 2502.88 2305.77 101.54 o -3 -7 18 2 5.31 -6.41 34.14 < -1 -7 18 2 3.99 3.30 27.11 < -8 -6 18 0 32.00 18.98 28.78 < -8 -6 18 2 0.02 3.27 24.96 < -6 -6 18 0 6991.74 6643.45 111.29 o -6 -6 18 2 11.81 40.85 23.90 < -4 -6 18 -2 0.12 14.70 56.74 < -4 -6 18 0 1419.15 1305.72 66.70 o -4 -6 18 2 49.56 30.15 56.33 < -2 -6 18 -2 28.80 20.47 40.12 < -2 -6 18 0 180.12 258.39 36.75 o -2 -6 18 2 52.49 54.61 26.95 < -9 -5 18 2 1.77 19.39 27.89 < -7 -5 18 -2 0.00 22.35 25.83 < -7 -5 18 0 1935.91 1917.07 65.91 o -7 -5 18 2 22.35 23.33 24.96 < -5 -5 18 -2 18.29 22.07 35.26 < -5 -5 18 0 2352.29 2391.55 94.73 o -5 -5 18 2 14.35 18.96 31.78 < -3 -5 18 -2 3.77 55.39 37.53 < -3 -5 18 0 5623.82 6061.98 144.99 o -3 -5 18 2 3.60 19.51 32.81 < -1 -5 18 -2 19.52 11.70 28.90 < -1 -5 18 0 1521.85 1481.02 60.34 o -1 -5 18 2 19.35 3.98 25.23 < -8 -4 18 -2 15.25 15.11 114.46 < -8 -4 18 0 601.27 604.83 65.71 o -8 -4 18 2 13.66 12.25 41.72 < -6 -4 18 -2 8.31 29.42 37.35 < -6 -4 18 0 5.14 17.13 23.47 < -6 -4 18 2 1.69 1.42 21.68 < -4 -4 18 -2 7.43 34.25 56.05 < -4 -4 18 0 392.62 434.03 51.50 o -4 -4 18 2 12.86 18.96 29.90 < -2 -4 18 -2 15.24 16.55 37.85 < -2 -4 18 0 189.18 217.93 33.13 o -2 -4 18 2 0.74 11.17 23.56 < 0 -4 18 0 760.31 772.54 63.99 o 0 -4 18 2 44.00 37.87 28.58 < -9 -3 18 0 6957.87 7096.98 99.57 o -9 -3 18 2 0.33 15.36 23.13 < -7 -3 18 -2 5.69 24.23 63.38 < -7 -3 18 0 1700.91 1783.39 74.70 o -7 -3 18 2 8.04 11.95 62.83 < -5 -3 18 0 1992.10 2036.27 117.36 o -5 -3 18 2 3.90 6.98 28.78 < -3 -3 18 2 12.39 25.55 32.45 < -1 -3 18 -2 8.05 26.01 39.43 < -1 -3 18 0 174.14 214.25 48.31 o -1 -3 18 2 8.73 29.95 36.61 < -8 -2 18 -2 9.35 10.53 34.05 < -8 -2 18 0 253.20 297.43 38.12 o -8 -2 18 2 43.14 28.23 21.02 < -6 -2 18 -2 0.61 59.51 36.41 < -6 -2 18 0 6721.03 6913.49 147.30 o -6 -2 18 2 39.57 40.39 32.31 < -4 -2 18 -2 3.11 59.05 24.66 < -4 -2 18 0 3795.44 3839.63 78.35 o -4 -2 18 2 0.12 13.81 20.95 < -2 -2 18 -2 7.14 1.12 35.44 < -2 -2 18 0 987.09 971.91 69.45 o -2 -2 18 2 1.43 2.38 22.78 < 0 -2 18 0 9741.24 10258.10 199.47 o 0 -2 18 2 3.06 23.90 40.09 < -9 -1 18 0 591.11 606.15 41.24 o -9 -1 18 2 3.44 3.41 21.73 < -7 -1 18 -2 30.76 23.42 40.64 < -7 -1 18 0 7.81 14.84 28.76 < -7 -1 18 2 22.50 3.37 18.57 < -5 -1 18 -2 13.83 14.52 22.87 < -5 -1 18 0 173.01 181.85 29.53 o -5 -1 18 2 4.73 4.17 20.22 < -3 -1 18 -2 34.89 24.16 34.85 < -3 -1 18 0 104.94 111.09 27.18 o -3 -1 18 2 9.71 1.31 20.56 < -1 -1 18 -2 0.13 -0.66 29.03 < -1 -1 18 0 53.30 73.77 28.78 < -1 -1 18 2 0.14 5.13 24.00 < -8 0 18 -2 7.23 3.96 22.16 < -8 0 18 0 519.62 529.72 35.89 o -8 0 18 2 6.96 0.23 20.10 < -6 0 18 -2 0.51 30.80 24.59 < -6 0 18 0 5752.48 5859.15 101.39 o -6 0 18 2 27.99 43.73 18.89 < -4 0 18 -2 0.06 13.90 23.40 < -4 0 18 0 1684.08 1598.96 55.43 o -4 0 18 2 3.60 1.83 20.47 < -2 0 18 -2 0.41 8.47 25.39 < -2 0 18 0 1407.52 1567.87 57.83 o -2 0 18 2 0.35 2.98 22.71 < 0 0 18 0 3060.89 3052.13 82.37 o 0 0 18 2 9.98 6.53 27.64 < -9 1 18 0 3200.07 3150.18 72.39 o -9 1 18 2 10.18 7.81 49.23 < -7 1 18 -2 2.60 11.15 21.00 < -7 1 18 0 2049.26 2014.00 54.32 o -7 1 18 2 0.04 0.11 18.04 < -5 1 18 -2 32.06 24.27 25.09 < -5 1 18 0 0.29 9.00 22.83 < -5 1 18 2 12.22 13.07 21.89 < -3 1 18 -2 0.20 27.96 24.52 < -3 1 18 0 11940.20 12178.10 136.50 o -3 1 18 2 24.45 16.85 21.94 < -1 1 18 -2 34.40 38.51 29.17 < -1 1 18 0 336.15 294.99 38.23 o -1 1 18 2 5.43 0.69 24.80 < -8 2 18 -2 14.52 13.69 23.24 < -8 2 18 0 735.43 775.71 40.00 o -8 2 18 2 3.43 -4.83 19.71 < -6 2 18 -2 7.94 24.27 21.45 < -6 2 18 0 4185.50 4329.27 73.14 o -6 2 18 2 0.00 10.49 18.75 < -4 2 18 -2 0.78 4.72 24.57 < -4 2 18 0 94.35 59.80 25.39 < -4 2 18 2 10.70 19.71 22.12 < -2 2 18 -2 0.27 8.43 26.10 < -2 2 18 0 679.13 625.98 46.14 o -2 2 18 2 0.09 11.54 22.19 < 0 2 18 2 0.58 9.62 29.26 < -9 3 18 2 7.02 -1.56 21.98 < -7 3 18 -2 24.33 21.75 21.73 < -7 3 18 0 1414.91 1365.57 48.20 o -7 3 18 2 0.80 10.46 19.35 < -5 3 18 -2 0.05 13.74 25.62 < -5 3 18 0 5016.73 5299.98 97.84 o -5 3 18 2 26.57 27.98 19.28 < -3 3 18 -2 15.14 23.54 26.17 < -3 3 18 0 87.95 81.67 26.95 o -3 3 18 2 12.80 14.81 24.23 < -1 3 18 -2 0.47 10.51 30.43 < -1 3 18 0 2434.88 2556.86 76.81 o -1 3 18 2 25.62 33.41 28.09 < -8 4 18 0 914.18 958.28 45.38 o -8 4 18 2 3.44 6.73 21.07 < -6 4 18 -2 14.22 25.23 21.98 < -6 4 18 0 2536.96 2362.26 57.91 o -6 4 18 2 1.23 5.52 18.30 < -4 4 18 -2 9.30 -2.11 25.37 < -4 4 18 0 1447.63 1430.75 56.20 o -4 4 18 2 7.11 6.43 18.34 < -2 4 18 -2 20.65 9.39 26.63 < -2 4 18 0 2800.98 2748.18 77.77 o -2 4 18 2 6.38 5.95 24.91 < -7 5 18 -2 0.16 0.80 22.26 < -7 5 18 0 364.69 380.43 34.75 o -7 5 18 2 49.46 34.44 22.37 < -5 5 18 -2 7.45 9.02 22.74 < -5 5 18 0 1460.31 1464.48 48.90 o -5 5 18 2 3.37 4.76 19.42 < -3 5 18 -2 0.21 4.67 28.42 < -3 5 18 0 1873.21 1818.64 66.62 o -3 5 18 2 10.52 9.23 24.73 < -1 5 18 2 5.60 -5.22 29.72 < -8 6 18 2 4.30 16.21 22.00 < -6 6 18 -2 0.01 2.93 23.70 < -6 6 18 0 3.83 21.02 23.03 < -6 6 18 2 13.64 13.46 21.98 < -4 6 18 -2 0.99 10.19 42.36 < -4 6 18 0 4074.49 4371.29 100.22 o -4 6 18 2 40.77 39.68 22.58 < -2 6 18 0 2992.84 3118.34 84.10 o -2 6 18 2 30.18 25.76 29.67 < -7 7 18 2 11.90 7.12 23.47 < -5 7 18 0 3020.34 3123.18 68.92 o -5 7 18 2 17.54 21.32 22.60 < -3 7 18 2 9.37 6.30 26.84 < -4 8 18 2 26.72 15.75 28.42 < -5 -8 19 1 213.65 226.93 37.94 o -6 -7 19 1 123.27 144.97 33.22 o -4 -7 19 1 0.36 -8.79 33.75 < -7 -6 19 1 9.13 7.17 27.91 < -5 -6 19 -1 23.19 25.32 43.89 < -5 -6 19 1 5.28 14.04 43.12 < -3 -6 19 -1 11.44 10.30 41.38 < -3 -6 19 1 0.50 1.44 38.06 < -8 -5 19 1 7.63 5.04 27.02 < -6 -5 19 -1 6.80 19.65 38.90 < -6 -5 19 1 156.77 158.16 31.34 o -4 -5 19 -1 16.95 18.36 43.92 < -4 -5 19 1 7.18 -0.44 34.90 < -2 -5 19 1 6.83 23.79 28.76 < -7 -4 19 -1 177.36 181.74 90.75 < -7 -4 19 1 20.46 36.68 90.76 < -5 -4 19 -1 82.69 78.40 82.63 < -5 -4 19 1 304.81 304.45 82.60 o -8 -3 19 1 24.82 32.95 29.38 < -6 -3 19 -1 8.48 9.34 84.40 < -6 -3 19 1 277.50 250.29 84.36 < -2 -3 19 -1 76.68 83.07 45.47 < -2 -3 19 1 54.39 60.54 42.36 < -7 -2 19 -1 171.33 175.56 51.08 o -7 -2 19 1 310.79 323.81 52.65 o -5 -2 19 -1 3.94 14.72 25.78 < -5 -2 19 1 36.23 34.46 24.66 < -1 -2 19 1 10.82 13.78 41.60 < -8 -1 19 -1 63.13 40.09 37.78 < -8 -1 19 1 45.12 51.52 34.00 < -6 -1 19 -1 26.37 48.88 43.89 < -6 -1 19 1 320.05 354.19 48.10 o -4 -1 19 -1 9.95 11.70 77.39 < -4 -1 19 1 162.95 103.55 77.38 < -2 -1 19 -1 7.01 12.39 39.98 < -2 -1 19 1 6.94 6.98 26.68 < -7 0 19 -1 75.59 59.55 28.85 < -7 0 19 1 28.36 32.90 22.39 < -5 0 19 -1 540.58 513.91 43.19 o -5 0 19 1 10.38 7.12 24.50 < -3 0 19 -1 11.81 8.52 36.20 < -3 0 19 1 182.96 199.11 33.70 o -1 0 19 1 64.45 59.97 30.57 < -8 1 19 -1 4.00 -4.40 39.64 < -8 1 19 1 35.64 33.77 24.22 < -6 1 19 -1 70.01 60.70 43.14 < -6 1 19 1 2.14 -3.05 41.72 < -4 1 19 -1 54.18 70.61 42.56 < -4 1 19 1 16.84 10.81 35.90 < -2 1 19 -1 117.91 95.79 31.71 o -2 1 19 1 159.14 176.79 34.37 o -7 2 19 -1 152.77 153.65 28.87 o -7 2 19 1 0.28 3.71 21.11 < -5 2 19 -1 106.08 113.56 30.25 o -5 2 19 1 204.39 206.16 33.79 o -3 2 19 -1 169.46 174.96 40.18 o -3 2 19 1 19.21 6.96 26.56 < -8 3 19 1 13.14 19.44 23.74 < -6 3 19 -1 40.12 56.23 30.73 < -6 3 19 1 857.86 855.20 41.51 o -4 3 19 -1 171.62 185.93 51.35 o -4 3 19 1 0.81 19.26 37.51 < -2 3 19 1 198.89 213.01 37.36 o -7 4 19 1 150.93 135.63 28.44 o -5 4 19 -1 29.17 34.02 28.71 < -5 4 19 1 15.98 7.76 26.06 < -3 4 19 1 2.93 0.16 27.34 < -6 5 19 1 1.04 -0.39 23.42 < -4 5 19 1 291.54 310.22 56.02 o -5 -5 20 2 54.84 39.70 40.73 < -6 -4 20 2 0.05 14.27 38.72 < -7 -3 20 2 28.95 48.20 41.90 < -5 -3 20 0 3745.66 3796.15 136.81 o -5 -3 20 2 3.25 15.25 137.25 < -6 -2 20 0 356.24 308.29 91.93 o -6 -2 20 2 41.71 62.28 50.65 < -7 -1 20 2 4.79 -5.84 27.52 < -5 -1 20 0 2857.37 2736.27 82.55 o -5 -1 20 2 13.27 10.35 66.01 < -3 -1 20 2 36.01 43.64 38.15 < -6 0 20 0 88.88 99.37 45.36 < -6 0 20 2 0.05 0.18 43.69 < -4 0 20 0 17.11 16.69 83.89 < -4 0 20 2 1.10 9.02 83.90 < -7 1 20 2 19.71 16.05 27.32 < -5 1 20 0 5080.54 4893.54 141.91 o -5 1 20 2 11.41 33.32 40.83 < -3 1 20 2 1.75 -3.18 39.29 < -6 2 20 2 56.63 39.54 27.54 < -4 2 20 2 1.64 9.30 39.77 < -5 3 20 2 0.39 -1.37 28.07 < data_II_Average_Structure _exptl_crystal_type_of_structure cryst _chemical_name_common labradorite_An51 _chemical_formula_analytical An51 _chemical_formula_sum 'Ca0.522 Na0.478 Al1.522 Si2.478 O8' _chemical_formula_weight 270.567 _chemical_compound_source 'Augusta, Maine' _space_group_crystal_system triclinic _space_group_name_H-M_alt C-1 _space_group_name_Hall -C loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z 3 x+1/2,y+1/2,z 4 -x+1/2,-y+1/2,-z _cell_length_a 8.1668(10) _cell_length_b 12.8509(10) _cell_length_c 7.1043(10) _cell_angle_alpha 93.5802(6) _cell_angle_beta 116.23(9) _cell_angle_gamma 89.8396(13) _cell_volume 667.263(14) _cell_formula_units_Z 4 _cell_measurement_temperature 293 _exptl_crystal_density_diffrn 2.685 _exptl_crystal_F_000 537 _exptl_absorpt_coefficient_mu 1.248 _exptl_crystal_description 'irragular shaped' _exptl_crystal_size_max 0.153 _exptl_crystal_size_mid 0.059 _exptl_crystal_size_min 0.058 _exptl_crystal_colour colorless _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details 'Gaussian integration method' _exptl_absorpt_correction_T_min 0.9252 _exptl_absorpt_correction_T_max 0.9582 _diffrn_ambient_temperature 293 _diffrn_source 'Bruker I|\`IS Microfocus' _diffrn_source_power 0.03 _diffrn_source_voltage 50 _diffrn_source_current 0.6 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker CCD' _diffrn_detector ApexII _diffrn_reflns_number 8136 _diffrn_reflns_theta_min 3.17 _diffrn_reflns_theta_max 30.53 _diffrn_reflns_theta_full 30.53 _diffrn_measured_fraction_theta_max 1 _diffrn_measured_fraction_theta_full 1 _diffrn_reflns_av_R_equivalents 0.0389 _diffrn_reflns_av_unetI/netI 0.01 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 9 _diffrn_radiation_probe x-ray _reflns_number_total 2033 _reflns_number_gt 1842 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0244 _refine_ls_wR_factor_gt 0.08 _refine_ls_R_factor_all 0.0267 _refine_ls_wR_factor_ref 0.0803 _refine_ls_goodness_of_fit_ref 2.64 _refine_ls_goodness_of_fit_gt 2.77 _refine_ls_number_reflns 2033 _refine_ls_number_parameters 131 _refine_ls_number_constraints 59 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(I)+0.0004I^2^) _refine_ls_shift/su_max 0.0476 _refine_ls_shift/su_mean 0.0032 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef -2300(255) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Al 0.0645 0.0514 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Ca 0.2262 0.3064 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Na 0.0362 0.0249 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.006 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Si 0.0817 0.0704 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group M2ca Ca 0.2697(12) 0.02878(11) 0.1021(2) Uani 0.0206(4) 4 0.328(7) d ? ? ? M2na Na 0.2697(12) 0.02878(11) 0.1021(2) Uani 0.0206(4) 4 0.199(10) d ? ? ? M1ca Ca 0.269(17) -0.0257(2) 0.1719(3) Uani 0.0339(9) 4 0.19(3) d ? ? ? M1na Na 0.269(17) -0.0257(2) 0.1719(3) Uani 0.0339(9) 4 0.28(3) d ? ? ? T1osi Si 0.49387(6) 0.33567(4) -0.21377(8) Uani 0.01438(17) 4 0.4016 d ? ? ? T1msi Si 0.50323(6) 0.3177(4) 0.23193(7) Uani 0.01398(17) 4 0.697 d ? ? ? T2osi Si 0.68547(6) 0.10928(4) 0.31662(7) Uani 0.01212(16) 4 0.7224 d ? ? ? T2msi Si 0.18165(6) 0.37952(4) 0.35731(7) Uani 0.01229(17) 4 0.657 d ? ? ? T1oal Al 0.49387(6) 0.33567(4) -0.21377(8) Uani 0.01438(17) 4 0.5984 d ? ? ? T1mal Al 0.50323(6) 0.3177(4) 0.23193(7) Uani 0.01398(17) 4 0.303 d ? ? ? T2oal Al 0.68547(6) 0.10928(4) 0.31662(7) Uani 0.01212(16) 4 0.2776 d ? ? ? T2mal Al 0.18165(6) 0.37952(4) 0.35731(7) Uani 0.01229(17) 4 0.343 d ? ? ? Oa1 O 0.49785(18) 0.37113(11) 0.0221(2) Uani 0.0255(5) 4 1 d ? ? ? Oa2 O 0.58094(16) -0.00688(9) 0.278(19) Uani 0.0162(4) 4 1 d ? ? ? Obo O 0.81143(17) 0.10559(11) 0.1886(2) Uani 0.0214(5) 4 1 d ? ? ? Obm O 0.31632(19) 0.35352(12) 0.2447(2) Uani 0.0289(5) 4 1 d ? ? ? Oco O 0.48582(18) 0.2078(11) -0.2798(2) Uani 0.0244(6) 4 1 d ? ? ? Ocm O 0.51425(17) 0.1887(10) 0.2155(2) Uani 0.0285(5) 4 1 d ? ? ? Odo O 0.30138(18) 0.39282(12) 0.6171(2) Uani 0.0215(5) 4 1 d ? ? ? Odm O 0.68996(18) 0.36705(12) 0.4314(2) Uani 0.0247(5) 4 1 d ? ? ? loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 M2ca Ca 0.0105(4) 0.0245(7) 0.02(6) 0.0047(4) 0.0017(3) -0.0071(5) M2na Na 0.0105(4) 0.0245(7) 0.02(6) 0.0047(4) 0.0017(3) -0.0071(5) M1ca Ca 0.0131(9) 0.0604(18) 0.0264(11) -0.0095(6) 0.01(6) -0.0211(10) M1na Na 0.0131(9) 0.0604(18) 0.0264(11) -0.0095(6) 0.01(6) -0.0211(10) T1osi Si 0.0115(2) 0.0213(3) 0.009(2) -0.00424(18) 0.00314(18) 0.0021(19) T1msi Si 0.012(2) 0.0201(2) 0.0082(2) 0.00676(18) 0.00312(18) -0.00028(18) T2osi Si 0.0103(2) 0.0133(2) 0.0109(2) 0.00165(16) 0.00317(17) -0.00095(17) T2msi Si 0.0103(2) 0.0152(2) 0.0103(2) -0.00062(17) 0.00336(17) 0.00194(17) T1oal Al 0.0115(2) 0.0213(3) 0.009(2) -0.00424(18) 0.00314(18) 0.0021(19) T1mal Al 0.012(2) 0.0201(2) 0.0082(2) 0.00676(18) 0.00312(18) -0.00028(18) T2oal Al 0.0103(2) 0.0133(2) 0.0109(2) 0.00165(16) 0.00317(17) -0.00095(17) T2mal Al 0.0103(2) 0.0152(2) 0.0103(2) -0.00062(17) 0.00336(17) 0.00194(17) Oa1 O 0.0281(6) 0.0406(7) 0.0105(7) 0.0008(5) 0.0105(5) 0.0052(5) Oa2 O 0.0144(5) 0.0179(6) 0.0144(6) -0.0012(5) 0.0046(5) 0.002(5) Obo O 0.0203(6) 0.0204(7) 0.025(6) -0.0039(5) 0.0117(5) -0.0014(5) Obm O 0.0228(7) 0.0267(8) 0.0414(6) 0.003(6) 0.0187(6) -0.003(6) Oco O 0.0208(7) 0.0297(7) 0.0209(9) -0.0073(6) 0.0072(7) 0.0035(6) Ocm O 0.0221(6) 0.0338(6) 0.0184(7) 0.0136(5) -0.0001(6) -0.0074(5) Odo O 0.0196(7) 0.0268(8) 0.0119(7) -0.0019(6) 0.0014(6) 0.0008(6) Odm O 0.0201(6) 0.0287(7) 0.0151(7) 0.0022(5) -0.0006(6) -0.0034(6) data_section_1_I-1_t0.00 _exptl_crystal_type_of_structure cryst _pd_phase_name 'Ca0.615 Na0.385 Si2.535 Al1.465 O8' _cell_length_a 8.1668(1) _cell_length_b 12.8509(15) _cell_length_c 14.2086(19) _cell_angle_alpha 93.5804(14) _cell_angle_beta 116.23(17) _cell_angle_gamma 89.8396(13) _space_group_name_H-M_alt 'I -1' _space_group_IT_number 2 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 'x, y, z' 2 '-x, -y, -z' 3 'x+1/2, y+1/2, z+1/2' 4 '-x+1/2, -y+1/2, -z+1/2' loop_ _atom_type_symbol Ca Na Si Al O loop_ _atom_site_label _atom_site_occupancy _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_type_symbol Mo2ca 0.616 0.268106 0.029236 0.548461 Uiso 0.009955 Ca Mz2ca 0.3564 0.275245 0.034407 0.046444 Uiso 0.011366 Ca Mo1ca 0.0555 0.264197 0.987656 0.577273 Uiso 0.033043 Ca Mz1ca 0.1996 0.267317 0.987777 0.082631 Uiso 0.039651 Ca Mo1na 0.3285 0.264197 0.987656 0.577273 Uiso 0.033043 Na Mz1na 0.444 0.267317 0.987777 0.082631 Uiso 0.039651 Na T1oosi 0.9063 0.491264 0.339029 0.39554 Uiso 0.011142 Si T1ozsi 0.0451 0.996473 0.83419 0.389077 Uiso 0.011549 Si T1omsi 0.4618 0.501454 0.318277 0.618127 Uiso 0.011207 Si T1mzsi 0.9944 0.00767 0.82083 0.612779 Uiso 0.011391 Si T2oosi 0.9637 0.681095 0.105021 0.660827 Uiso 0.010764 Si T2ozsi 0.4311 0.686943 0.109343 0.15794 Uiso 0.010334 Si T2mosi 0.9543 0.678766 0.879256 0.180636 Uiso 0.010037 Si T2mzsi 0.3102 0.686335 0.873911 0.676769 Uiso 0.010435 Si T1ooal 0.0937 0.491264 0.339029 0.39554 Uiso 0.011142 Al T1ozal 0.9549 0.996473 0.83419 0.389077 Uiso 0.011549 Al T1moal 0.5382 0.501454 0.318277 0.618127 Uiso 0.011207 Al T1mzal 0.0056 0.00767 0.82083 0.612779 Uiso 0.011391 Al T2ooal 0.0363 0.681095 0.105021 0.660827 Uiso 0.010764 Al T2ozal 0.5689 0.686943 0.109343 0.15794 Uiso 0.010334 Al T2moal 0.0457 0.678766 0.879256 0.180636 Uiso 0.010037 Al T2mzal 0.6898 0.686335 0.873911 0.676769 Uiso 0.010435 Al Odmo 1 0.196314 0.871436 0.215464 Uiso 0.021623 O Odmz 1 0.18445 0.868035 0.713597 Uiso 0.023702 O Oa2o 1 0.57461 0.994019 0.638929 Uiso 0.01367 O Oa2z 1 0.581797 0.989457 0.137917 Uiso 0.013839 O Odoo 1 0.792682 0.893027 0.307997 Uiso 0.016965 O Odoz 1 0.814435 0.88509 0.810449 Uiso 0.019712 O Oa1o 1 0.488633 0.375541 0.509668 Uiso 0.018464 O Oa1z 1 0.00851 0.875057 0.512017 Uiso 0.021648 O Obmo 1 0.314479 0.353393 0.630201 Uiso 0.024089 O Obmz 1 0.819826 0.856369 0.612971 Uiso 0.026091 O Oboo 1 0.805607 0.103381 0.598619 Uiso 0.01797 O Oboz 1 0.321846 0.603558 0.592095 Uiso 0.017965 O Ocmo 1 0.513435 0.18586 0.6085 Uiso 0.019398 O Ocmz 1 0.016157 0.695521 0.602604 Uiso 0.020583 O Ocoo 1 0.488225 0.216836 0.364591 Uiso 0.019438 O Ocoz 1 0.986153 0.703108 0.35521 Uiso 0.016844 O loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Mo2ca 0.00607 0.01445 0.00766 0.00556 0.00164 -0.00004 Mz2ca 0.00666 0.01295 0.01012 0.00547 0.00009 -0.00166 Mo1ca 0.00921 0.06427 0.02312 -0.00861 0.00786 -0.02108 Mz1ca 0.01154 0.07309 0.02992 -0.01167 0.00949 -0.031 Mo1na 0.00921 0.06427 0.02312 -0.00861 0.00786 -0.02108 Mz1na 0.01154 0.07309 0.02992 -0.01167 0.00949 -0.031 T1oosi 0.01038 0.01562 0.00728 -0.00299 0.00386 -0.00002 T1ozsi 0.00981 0.01439 0.00999 -0.00072 0.00388 0.00147 T1omsi 0.01091 0.01493 0.00746 0.00378 0.00394 -0.00039 T1mzsi 0.01071 0.01549 0.00724 0.00534 0.00335 0.00067 T2oosi 0.00877 0.00968 0.01218 -0 0.00344 -0.00172 T2ozsi 0.00975 0.01033 0.00994 0.00089 0.00346 0.00079 T2mosi 0.00952 0.01023 0.00945 0.00201 0.00329 0.0014 T2mzsi 0.00925 0.0119 0.00977 0.00062 0.00373 0.00176 T1ooal 0.01038 0.01562 0.00728 -0.00299 0.00386 -0.00002 T1ozal 0.00981 0.01439 0.00999 -0.00072 0.00388 0.00147 T1moal 0.01091 0.01493 0.00746 0.00378 0.00394 -0.00039 T1mzal 0.01071 0.01549 0.00724 0.00534 0.00335 0.00067 T2ooal 0.00877 0.00968 0.01218 -0 0.00344 -0.00172 T2ozal 0.00975 0.01033 0.00994 0.00089 0.00346 0.00079 T2moal 0.00952 0.01023 0.00945 0.00201 0.00329 0.0014 T2mzal 0.00925 0.0119 0.00977 0.00062 0.00373 0.00176 Odmo 0.01815 0.02104 0.01428 0.00038 -0.00233 -0.00543 Odmz 0.0191 0.02537 0.01524 0.00209 -0.00241 -0.00118 Oa2o 0.01196 0.01324 0.01429 -0.00126 0.00456 -0.00016 Oa2z 0.01349 0.01291 0.01345 0.00365 0.00403 0.00435 Odoo 0.0153 0.0182 0.01099 0.00225 0.00009 0.00041 Odoz 0.01848 0.02284 0.01076 -0.00146 -0.00004 0.00189 Oa1o 0.02559 0.02317 0.0088 -0.00053 0.00951 0.00158 Oa1z 0.02903 0.0291 0.00909 0.0066 0.00998 0.00568 Obmo 0.02194 0.02133 0.03688 0.00334 0.02062 -0.00139 Obmz 0.01808 0.02763 0.03719 0.00444 0.01719 -0.00359 Oboo 0.01536 0.01633 0.0257 -0.00204 0.01259 -0.00137 Oboz 0.01646 0.01864 0.02113 -0.00666 0.011 -0.00338 Ocmo 0.01476 0.02337 0.01491 0.00842 0.00221 -0.00088 Ocmz 0.0218 0.01741 0.01535 0.00649 0.00228 -0.00321 Ocoo 0.01995 0.01987 0.01853 -0.00425 0.00896 -0.00214 Ocoz 0.01567 0.01499 0.01728 -0.00469 0.00525 -0.00157 data_section_2_I_1_t0.25 _exptl_crystal_type_of_structure cryst _pd_phase_name 'Ca0.43 Na0.57 Si2.59 Al1.41 O8' _cell_length_a 8.1668(1) _cell_length_b 12.8509(15) _cell_length_c 14.2086(19) _cell_angle_alpha 93.5804(14) _cell_angle_beta 116.23(17) _cell_angle_gamma 89.8396(13) _space_group_name_H-M_alt 'I 1' _space_group_IT_number 1 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 'x, y, z' 2 'x+1/2, y+1/2, z+1/2' loop_ _atom_type_symbol Ca Na Si Al O loop_ _atom_site_label _atom_site_occupancy _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_type_symbol Moz0 0.3237 0.267036 0.030428 0.549726 Uiso 0.019159 Ca Moo0 0.1466 0.272087 0.018525 0.051383 Uiso 0.057116 Ca Miz0 0.1354 0.729618 0.983434 0.448346 Uiso 0.057544 Ca Mio0 0.4007 0.7336 0.969499 0.949936 Uiso 0.018481 Ca Moz1Ca 0.1314 0.269401 0.022389 0.564903 Uiso 0.038063 Ca Moo1Ca 0.2509 0.27291 0.964369 0.089854 Uiso 0.014076 Ca Miz1Ca 0.2165 0.729092 0.034301 0.411981 Uiso 0.015938 Ca Mio1Ca 0.1182 0.729947 0.978638 0.935157 Uiso 0.034903 Ca Moz1Na 0.545 0.269401 0.022389 0.564903 Uiso 0.038063 Na Moo1Na 0.6025 0.27291 0.964369 0.089854 Uiso 0.014076 Na Miz1Na 0.6481 0.729092 0.034301 0.411981 Uiso 0.015938 Na Mio1Na 0.4811 0.729947 0.978638 0.935157 Uiso 0.034903 Na T1ozoSi 0.4039 0.499766 0.324923 0.392473 Uiso 0.009085 Si T1oooSi 0.3233 0.98828 0.843768 0.394734 Uiso 0.00902 Si T1oizSi 0.3353 0.512005 0.656135 0.605208 Uiso 0.00897 Si T1oioSi 0.4217 0.00016 0.174985 0.607336 Uiso 0.009099 Si T1mozSi 0.4029 0.496537 0.308642 0.618002 Uiso 0.008105 Si T1mooSi 0.8982 0.008703 0.826127 0.615933 Uiso 0.009378 Si T1mizSi 0.9378 0.489141 0.673103 0.384832 Uiso 0.009408 Si T1mioSi 0.5714 0.003674 0.191272 0.383435 Uiso 0.008002 Si T2ozoSi 0.7255 0.684445 0.104624 0.658677 Uiso 0.009618 Si T2oooSi 0.5727 0.691112 0.115802 0.156695 Uiso 0.008889 Si T2oizSi 0.7968 0.314297 0.885894 0.344303 Uiso 0.009355 Si T2oioSi 0.8844 0.316328 0.896982 0.839287 Uiso 0.009482 Si T2mozSi 0.782 0.678594 0.887397 0.179515 Uiso 0.009094 Si T2mooSi 0.9034 0.684484 0.874607 0.679222 Uiso 0.00922 Si T2mizSi 0.7294 0.310947 0.127391 0.821935 Uiso 0.009412 Si T2mioSi 0.667 0.321811 0.112876 0.321401 Uiso 0.00914 Si T1ozoAl 0.5961 0.499766 0.324923 0.392473 Uiso 0.009085 Al T1oooAl 0.6767 0.98828 0.843768 0.394734 Uiso 0.00902 Al T1oizAl 0.6647 0.512005 0.656135 0.605208 Uiso 0.00897 Al T1oioAl 0.5783 0.00016 0.174985 0.607336 Uiso 0.009099 Al T1mozAl 0.5971 0.496537 0.308642 0.618002 Uiso 0.008105 Al T1mooAl 0.1018 0.008703 0.826127 0.615933 Uiso 0.009378 Al T1mizAl 0.0622 0.489141 0.673103 0.384832 Uiso 0.009408 Al T1mioAl 0.4286 0.003674 0.191272 0.383435 Uiso 0.008002 Al T2ozoAl 0.2745 0.684445 0.104624 0.658677 Uiso 0.009618 Al T2oooAl 0.4273 0.691112 0.115802 0.156695 Uiso 0.008889 Al T2oizAl 0.2032 0.314297 0.885894 0.344303 Uiso 0.009355 Al T2oioAl 0.1156 0.316328 0.896982 0.839287 Uiso 0.009482 Al T2mozAl 0.218 0.678594 0.887397 0.179515 Uiso 0.009094 Al T2mooAl 0.0966 0.684484 0.874607 0.679222 Uiso 0.00922 Al T2mizAl 0.2706 0.310947 0.127391 0.821935 Uiso 0.009412 Al T2mioAl 0.333 0.321811 0.112876 0.321401 Uiso 0.00914 Al Odmoz 1 0.192508 0.860536 0.219644 Uiso 0.018807 O Odmoo 1 0.192962 0.876322 0.714344 Uiso 0.021142 O Odmiz 1 0.810255 0.124275 0.784974 Uiso 0.022778 O Odmio 1 0.814913 0.142294 0.284186 Uiso 0.017737 O Oa2oz 1 0.588844 0.985186 0.639358 Uiso 0.013538 O Oa2oo 1 0.581352 0.000573 0.140098 Uiso 0.012991 O Oa2iz 1 0.420029 0.998514 0.360833 Uiso 0.012931 O Oa2io 1 0.412039 0.014268 0.859691 Uiso 0.01353 O Odooz 1 0.797327 0.902382 0.307157 Uiso 0.01679 O Odooo 1 0.804795 0.883109 0.806871 Uiso 0.015778 O Odoiz 1 0.19039 0.117864 0.692556 Uiso 0.016928 O Odoio 1 0.202653 0.097631 0.192389 Uiso 0.016105 O Oa1oz 1 0.498021 0.357127 0.509827 Uiso 0.014054 O Oa1oo 1 0.9929 0.883836 0.513483 Uiso 0.019546 O Oa1iz 1 0.501051 0.615409 0.485872 Uiso 0.020647 O Oa1io 1 0.001389 0.144227 0.489979 Uiso 0.013959 O Obmoz 1 0.306556 0.353139 0.620566 Uiso 0.021309 O Obmoo 1 0.82839 0.850522 0.631505 Uiso 0.026754 O Obmiz 1 0.671564 0.648301 0.372665 Uiso 0.028501 O Obmio 1 0.190913 0.147179 0.38153 Uiso 0.019699 O Obooz 1 0.806612 0.114003 0.593064 Uiso 0.018261 O Obooo 1 0.312639 0.601449 0.593464 Uiso 0.018087 O Oboiz 1 0.187899 0.89851 0.406546 Uiso 0.01815 O Oboio 1 0.693496 0.386044 0.406675 Uiso 0.018208 O Ocmoz 1 0.505433 0.17662 0.614707 Uiso 0.014312 O Ocmoo 1 0.028792 0.700455 0.604226 Uiso 0.017693 O Ocmiz 1 0.468911 0.797819 0.396671 Uiso 0.01766 O Ocmio 1 0.996689 0.32128 0.386804 Uiso 0.014923 O Ocooz 1 0.495893 0.195862 0.358575 Uiso 0.016967 O Ocooo 1 0.973541 0.714393 0.362001 Uiso 0.017399 O Ocoiz 1 0.5266 0.785375 0.637931 Uiso 0.017486 O Ocoio 1 0.003888 0.303833 0.641129 Uiso 0.016979 O loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Moz0 0.01625 0.02074 0.0167 0.00098 0.00418 -0.00126 Moo0 0.02741 0.08048 0.04809 0.00935 0.00716 -0.02993 Miz0 0.0289 0.08211 0.04747 0.00964 0.00822 -0.028 Mio0 0.01501 0.01994 0.01652 0.00079 0.00382 -0.00226 Moz1Ca 0.01128 0.04993 0.03647 0.00939 -0.00012 -0.03051 Moo1Ca 0.00883 0.01579 0.01685 -0.00353 0.00633 -0.00955 Miz1Ca 0.00858 0.01904 0.0185 -0.00388 0.00611 -0.01193 Mio1Ca 0.01084 0.04512 0.03343 0.01046 -0.0004 -0.02609 Moz1Na 0.01128 0.04993 0.03647 0.00939 -0.00012 -0.03051 Moo1Na 0.00883 0.01579 0.01685 -0.00353 0.00633 -0.00955 Miz1Na 0.00858 0.01904 0.0185 -0.00388 0.00611 -0.01193 Mio1Na 0.01084 0.04512 0.03343 0.01046 -0.0004 -0.02609 T1ozoSi 0.00948 0.01082 0.00698 -0.00023 0.00364 0.00077 T1oooSi 0.01029 0.00886 0.00768 -0.00008 0.00379 0.00037 T1oizSi 0.01031 0.00879 0.00762 -0.00008 0.00382 0.00035 T1oioSi 0.00946 0.01092 0.00691 -0.00031 0.0036 0.00073 T1mozSi 0.00925 0.00802 0.00699 0.00213 0.00348 0.0011 T1mooSi 0.01022 0.01095 0.0074 0.00227 0.00426 0.00099 T1mizSi 0.00997 0.01091 0.0077 0.00255 0.00416 0.00132 T1mioSi 0.00936 0.0082 0.00629 0.00245 0.00326 0.00109 T2ozoSi 0.00983 0.00843 0.00949 0.00098 0.00315 0.00164 T2oooSi 0.0087 0.00878 0.00837 0.00018 0.00301 0.00079 T2oizSi 0.00871 0.00916 0.0096 0.00047 0.00356 0.00028 T2oioSi 0.00912 0.00773 0.01001 0.00035 0.00281 0.00048 T2mozSi 0.00854 0.00858 0.00943 0.00137 0.00325 0.00117 T2mooSi 0.00933 0.00813 0.00993 0.00189 0.00391 0.00153 T2mizSi 0.00926 0.00859 0.01031 0.00143 0.00412 0.00183 T2mioSi 0.00857 0.00881 0.00945 0.00111 0.0034 0.00107 T1ozoAl 0.00948 0.01082 0.00698 -0.00023 0.00364 0.00077 T1oooAl 0.01029 0.00886 0.00768 -0.00008 0.00379 0.00037 T1oizAl 0.01031 0.00879 0.00762 -0.00008 0.00382 0.00035 T1oioAl 0.00946 0.01092 0.00691 -0.00031 0.0036 0.00073 T1mozAl 0.00925 0.00802 0.00699 0.00213 0.00348 0.0011 T1mooAl 0.01022 0.01095 0.0074 0.00227 0.00426 0.00099 T1mizAl 0.00997 0.01091 0.0077 0.00255 0.00416 0.00132 T1mioAl 0.00936 0.0082 0.00629 0.00245 0.00326 0.00109 T2ozoAl 0.00983 0.00843 0.00949 0.00098 0.00315 0.00164 T2oooAl 0.0087 0.00878 0.00837 0.00018 0.00301 0.00079 T2oizAl 0.00871 0.00916 0.0096 0.00047 0.00356 0.00028 T2oioAl 0.00912 0.00773 0.01001 0.00035 0.00281 0.00048 T2mozAl 0.00854 0.00858 0.00943 0.00137 0.00325 0.00117 T2mooAl 0.00933 0.00813 0.00993 0.00189 0.00391 0.00153 T2mizAl 0.00926 0.00859 0.01031 0.00143 0.00412 0.00183 T2mioAl 0.00857 0.00881 0.00945 0.00111 0.0034 0.00107 Odmoz 0.01577 0.01799 0.01446 -0.00033 -0.00034 -0.00219 Odmoo 0.02113 0.017 0.01377 0.00031 -0.00219 -0.00327 Odmiz 0.02144 0.0192 0.01531 0.0011 -0.00274 -0.00169 Odmio 0.01635 0.01837 0.01218 -0.00003 0.00078 -0.00052 Oa2oz 0.01505 0.01015 0.01324 -0.00021 0.00419 0.00155 Oa2oo 0.01185 0.01128 0.01458 0.0009 0.00446 0.00282 Oa2iz 0.01145 0.01169 0.01377 0.0005 0.00369 0.00232 Oa2io 0.01494 0.00992 0.01405 -0.00118 0.00489 0.00075 Odooz 0.01771 0.01485 0.01122 0.00285 0.00049 0.00046 Odooo 0.01563 0.01566 0.01118 0.00097 0.00132 0.00251 Odoiz 0.01694 0.01724 0.01083 0.00006 0.00068 0.00271 Odoio 0.01677 0.01451 0.0118 0.00286 0.00165 0.00039 Oa1oz 0.01867 0.01607 0.0099 -0.00098 0.00856 0.00092 Oa1oo 0.0327 0.01719 0.01269 0.00104 0.01349 0.00211 Oa1iz 0.03358 0.01945 0.01267 0.00227 0.01336 0.00344 Oa1io 0.01902 0.01559 0.01007 0.00063 0.00898 0.00091 Obmoz 0.01656 0.02475 0.02377 0.00191 0.01045 -0.00206 Obmoo 0.02233 0.02948 0.03889 0.0049 0.023 0.00272 Obmiz 0.0218 0.03247 0.04087 0.0046 0.02289 0.00054 Obmio 0.01556 0.02336 0.02098 0.00288 0.00901 0.0001 Obooz 0.01862 0.0165 0.02291 -0.00155 0.01227 0.00023 Obooo 0.01939 0.01537 0.02411 -0.00126 0.01394 0.00026 Oboiz 0.01938 0.01538 0.0244 -0.00123 0.0141 0.00022 Oboio 0.01858 0.01641 0.02281 -0.0014 0.01216 0.00034 Ocmoz 0.01247 0.01301 0.01591 0.0004 0.00506 -0.00044 Ocmoo 0.01632 0.01829 0.01526 0.00541 0.00412 0.00103 Ocmiz 0.01706 0.01606 0.01599 0.00372 0.00402 -0.00047 Ocmio 0.01467 0.01353 0.01501 0.002 0.0052 0.00069 Ocooz 0.01437 0.01946 0.01898 -0.00088 0.00902 0.002 Ocooo 0.01757 0.01461 0.01936 0.00082 0.00759 0.00108 Ocoiz 0.01776 0.01473 0.01941 0.00097 0.00772 0.00119 Ocoio 0.01434 0.01953 0.01898 -0.001 0.00903 0.00188 data_section_3_I-1_t0.50 _exptl_crystal_type_of_structure cryst _pd_phase_name 'Ca0.595 Na0.405 Si2.305 Al1.695 O8' _cell_length_a 8.1668(1) _cell_length_b 12.8509(15) _cell_length_c 14.2086(19) _cell_angle_alpha 93.5804(14) _cell_angle_beta 116.23(17) _cell_angle_gamma 89.8396(13) _space_group_name_H-M_alt 'I -1' _space_group_IT_number 2 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 'x, y, z' 2 '-x, -y, -z' 3 'x+1/2, y+1/2, z+1/2' 4 '-x+1/2, -y+1/2, -z+1/2' loop_ _atom_type_symbol Ca Na Si Al O loop_ _atom_site_label _atom_site_occupancy _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_type_symbol Mo2ca-1 0.3666 0.27647 0.033452 0.546723 Uiso 0.016647 Ca Mz2ca-2 0.538 0.26826 0.026262 0.048672 Uiso 0.016344 Ca Mo1ca-1 0.2272 0.268974 0.977948 0.587175 Uiso 0.033921 Ca Mz1ca-2 0.0616 0.263205 0.980168 0.080048 Uiso 0.032291 Ca Mo1na-1 0.4061 0.268974 0.977948 0.587175 Uiso 0.033921 Na Mz1na-2 0.4004 0.263205 0.980168 0.080048 Uiso 0.032291 Na T1oosi-1 0.0466 0.496426 0.334557 0.389187 Uiso 0.011578 Si T1ozsi-2 0.9011 0.990856 0.8394 0.395517 Uiso 0.011097 Si T1mosi-1 0.9731 0.503904 0.317042 0.612777 Uiso 0.011051 Si T1mzsi-2 0.2953 0.000053 0.815166 0.6188 Uiso 0.010921 Si T2oosi-1 0.3432 0.690905 0.113605 0.658131 Uiso 0.009827 Si T2ozsi-2 0.9492 0.680425 0.10919 0.157986 Uiso 0.010899 Si T2mosi-1 0.152 0.680331 0.878704 0.176199 Uiso 0.010497 Si T2mzsi-2 0.9536 0.678117 0.8813 0.680973 Uiso 0.010099 Si T1ooal-1 0.9534 0.496426 0.334557 0.389187 Uiso 0.011578 Al T1ozal-2 0.0989 0.990856 0.8394 0.395517 Uiso 0.011097 Al T1moal-1 0.0269 0.503904 0.317042 0.612777 Uiso 0.011051 Al T1mzal-2 0.7047 0.000053 0.815166 0.6188 Uiso 0.010921 Al T2ooal-1 0.6568 0.690905 0.113605 0.658131 Uiso 0.009827 Al T2ozal-2 0.0508 0.680425 0.10919 0.157986 Uiso 0.010899 Al T2moal-1 0.848 0.680331 0.878704 0.176199 Uiso 0.010497 Al T2mzal-2 0.0464 0.678117 0.8813 0.680973 Uiso 0.010099 Al Odmo-1 1 0.181374 0.860515 0.212492 Uiso 0.020959 O Odmz-2 1 0.197434 0.866148 0.718861 Uiso 0.021565 O Oa2o-1 1 0.580868 0.991646 0.638828 Uiso 0.013795 O Oa2z-2 1 0.573186 0.996576 0.137962 Uiso 0.01355 O Odoo-1 1 0.806938 0.892794 0.311345 Uiso 0.018494 O Odoz-2 1 0.793577 0.895555 0.808087 Uiso 0.017897 O Oa1o-1 1 0.506238 0.368629 0.511037 Uiso 0.019875 O Oa1z-2 1 0.991828 0.871219 0.509155 Uiso 0.017888 O Obmo-1 1 0.317079 0.355983 0.612096 Uiso 0.023053 O Obmz-2 1 0.809261 0.854501 0.627247 Uiso 0.024375 O Oboo-1 1 0.822176 0.103271 0.592236 Uiso 0.017897 O Oboz-2 1 0.305505 0.603179 0.598488 Uiso 0.018032 O Ocmo-1 1 0.508994 0.191131 0.604266 Uiso 0.020316 O Ocmz-2 1 0.010692 0.681101 0.610781 Uiso 0.018482 O Ocoo-1 1 0.485893 0.203506 0.355389 Uiso 0.01681 O Ocoz-2 1 0.987604 0.717162 0.364542 Uiso 0.019487 O loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Mo2ca-1 0.00719 0.02095 0.01508 0.00652 -0.00006 -0.00726 Mz2ca-2 0.00935 0.02492 0.01216 0.00712 0.00294 -0.00271 Mo1ca-1 0.01111 0.06454 0.025 -0.01305 0.01046 -0.02497 Mz1ca-2 0.00897 0.06368 0.02286 -0.01139 0.00888 -0.02179 Mo1na-1 0.01111 0.06454 0.025 -0.01305 0.01046 -0.02497 Mz1na-2 0.00897 0.06368 0.02286 -0.01139 0.00888 -0.02179 T1oosi-1 0.00981 0.01444 0.01 -0.00076 0.00386 0.00145 T1ozsi-2 0.01041 0.01548 0.00729 -0.00293 0.0039 -0.00002 T1mosi-1 0.01073 0.01504 0.00655 0.00533 0.00313 0.00048 T1mzsi-2 0.01048 0.01418 0.00769 0.00373 0.00379 -0.00023 T2oosi-1 0.00905 0.01009 0.00924 0.00029 0.0031 0.00026 T2ozsi-2 0.00884 0.01054 0.01224 0.00033 0.00399 -0.0016 T2mosi-1 0.00907 0.01265 0.00923 0.00029 0.00349 0.00129 T2mzsi-2 0.00941 0.01048 0.00935 0.00198 0.00311 0.00141 T1ooal-1 0.00981 0.01444 0.01 -0.00076 0.00386 0.00145 T1ozal-2 0.01041 0.01548 0.00729 -0.00293 0.0039 -0.00002 T1moal-1 0.01073 0.01504 0.00655 0.00533 0.00313 0.00048 T1mzal-2 0.01048 0.01418 0.00769 0.00373 0.00379 -0.00023 T2ooal-1 0.00905 0.01009 0.00924 0.00029 0.0031 0.00026 T2ozal-2 0.00884 0.01054 0.01224 0.00033 0.00399 -0.0016 T2moal-1 0.00907 0.01265 0.00923 0.00029 0.00349 0.00129 T2mzal-2 0.00941 0.01048 0.00935 0.00198 0.00311 0.00141 Odmo-1 0.01731 0.02443 0.01292 0.00149 -0.00051 -0.00072 Odmz-2 0.01604 0.02199 0.01573 0.00037 -0.0021 -0.00498 Oa2o-1 0.01313 0.01285 0.01435 0.00357 0.0047 0.00442 Oa2z-2 0.01131 0.01373 0.01357 -0.00075 0.00374 0.00021 Odoo-1 0.01655 0.02199 0.01192 -0.00022 0.00181 0.00058 Odoz-2 0.01655 0.0189 0.01061 0.00217 -0.00081 0.00024 Oa1o-1 0.026 0.02725 0.00867 0.00643 0.00935 0.00468 Oa1z-2 0.0231 0.02406 0.00818 -0.00108 0.00834 0.00184 Obmo-1 0.01674 0.0241 0.03139 0.0046 0.01395 -0.00194 Obmz-2 0.02099 0.02217 0.03584 0.00223 0.01869 -0.00407 Oboo-1 0.01646 0.01856 0.02095 -0.00659 0.0109 -0.0033 Oboz-2 0.01539 0.01637 0.02593 -0.0021 0.01276 -0.00145 Ocmo-1 0.02189 0.01808 0.01451 0.00749 0.00261 -0.00194 Ocmz-2 0.01343 0.02122 0.0157 0.00613 0.00229 -0.00219 Ocoo-1 0.01562 0.01488 0.01725 -0.00479 0.00517 -0.00171 Ocoz-2 0.02012 0.0198 0.01857 -0.00408 0.00899 -0.00204 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 2 0 0 56.22 61.58 1.12 o 4 0 0 17222.70 17140.80 42.23 o 6 0 0 10518.00 10368.30 28.84 o 8 0 0 9.66 11.52 3.44 o 10 0 0 2306.45 2361.86 26.08 o -9 1 0 180.49 169.96 7.46 o -7 1 0 1764.68 1706.65 12.94 o -5 1 0 227.60 217.12 3.37 o -3 1 0 2561.79 2247.19 6.89 o -1 1 0 472.29 523.08 2.78 o 1 1 0 58.28 61.81 0.98 o 3 1 0 2116.21 1837.93 7.45 o 5 1 0 140.99 141.36 3.05 o 7 1 0 1284.64 1292.42 11.48 o 9 1 0 46.39 48.95 6.25 o -10 2 0 138.84 140.95 8.19 o -8 2 0 530.46 518.72 9.42 o -6 2 0 3122.40 3183.01 15.84 o -4 2 0 865.09 887.52 5.22 o -2 2 0 16520.80 17056.70 50.80 o 0 2 0 30.62 31.09 0.81 o 2 2 0 14772.20 14495.80 41.50 o 4 2 0 1480.14 1590.89 8.20 o 6 2 0 4266.98 4264.18 18.92 o 8 2 0 555.19 576.72 11.99 o 10 2 0 429.25 444.62 13.51 o -9 3 0 1270.14 1231.09 15.06 o -7 3 0 299.68 291.95 5.77 o -5 3 0 1696.86 1737.34 7.93 o -3 3 0 913.26 707.20 4.09 o -1 3 0 9673.66 9992.39 27.79 o 1 3 0 7837.52 7934.04 26.76 o 3 3 0 1214.16 945.71 5.76 o 5 3 0 2676.08 2732.68 13.23 o 7 3 0 19.42 24.94 4.13 o 9 3 0 1935.81 1991.69 23.04 o -10 4 0 1189.89 1158.72 16.10 o -8 4 0 1617.30 1559.83 15.30 o -6 4 0 8979.58 9128.56 18.96 o -4 4 0 161.56 157.57 2.29 o -2 4 0 1775.41 1942.60 6.67 o 0 4 0 20779.00 20362.20 48.77 o 2 4 0 2620.56 2956.74 9.71 o 4 4 0 2.51 3.67 1.27 < 6 4 0 8534.61 8472.06 30.50 o 8 4 0 1589.41 1626.52 19.65 o 10 4 0 757.37 778.91 17.11 o -9 5 0 54.37 60.96 5.57 o -7 5 0 257.83 260.26 5.66 o -5 5 0 1320.89 1402.89 7.07 o -3 5 0 71.60 60.51 1.51 o -1 5 0 518.09 889.35 4.34 o 1 5 0 167.05 378.57 3.50 o 3 5 0 65.83 49.38 2.04 o 5 5 0 195.51 240.51 4.70 o 7 5 0 1376.81 1385.69 17.04 o 9 5 0 127.50 112.14 8.39 o -8 6 0 2459.37 2482.34 17.05 o -6 6 0 92.43 140.11 3.03 o -4 6 0 2941.49 3038.99 9.95 o -2 6 0 6605.30 6733.46 16.10 o 0 6 0 6601.70 6967.26 19.78 o 2 6 0 6134.81 6054.00 15.97 o 4 6 0 4948.43 4776.78 17.90 o 6 6 0 287.57 325.97 6.98 o 8 6 0 1422.89 1467.00 19.51 o -9 7 0 1.10 -0.74 4.01 < -7 7 0 489.41 537.73 7.21 o -5 7 0 711.78 702.46 5.39 o -3 7 0 581.88 597.44 4.70 o -1 7 0 2881.21 3155.12 9.69 o 1 7 0 100.33 129.97 2.66 o 3 7 0 1687.15 1655.24 9.50 o 5 7 0 694.26 659.71 7.81 o 7 7 0 396.78 407.69 10.46 o 9 7 0 202.69 221.55 10.87 o -8 8 0 1856.00 1826.10 16.55 o -6 8 0 75.92 78.23 2.78 o -4 8 0 786.13 747.50 5.44 o -2 8 0 10165.20 10322.90 24.93 o 0 8 0 3014.44 3220.64 12.16 o 2 8 0 7269.94 7385.10 19.76 o 4 8 0 2068.18 1969.43 12.61 o 6 8 0 10.23 9.32 3.15 < 8 8 0 3540.43 3800.24 31.79 o -9 9 0 2.97 6.91 7.28 < -7 9 0 34.86 41.25 6.52 o -5 9 0 1706.92 1793.24 9.48 o -3 9 0 90.58 130.75 2.83 o -1 9 0 1272.68 1291.75 8.23 o 1 9 0 7197.44 7165.19 21.46 o 3 9 0 40.69 62.57 3.18 o 5 9 0 1648.23 1699.51 14.30 o 7 9 0 678.96 688.55 16.74 o -8 10 0 166.70 172.18 8.08 o -6 10 0 27.34 25.11 2.91 o -4 10 0 124.89 122.50 3.75 o -2 10 0 496.65 527.01 6.76 o 0 10 0 2101.31 1985.12 11.62 o 2 10 0 82.77 70.81 3.26 o 4 10 0 83.59 87.98 4.33 o 6 10 0 446.22 418.31 12.62 o 8 10 0 218.58 254.20 13.41 o -7 11 0 5.78 3.07 4.67 < -5 11 0 739.67 724.98 8.92 o -3 11 0 278.50 277.73 5.64 o -1 11 0 94.30 93.87 3.79 o 1 11 0 157.49 154.48 4.80 o 3 11 0 162.96 163.40 4.74 o 5 11 0 264.99 252.48 6.87 o 7 11 0 342.97 337.34 13.47 o -8 12 0 557.74 512.47 17.40 o -6 12 0 14.38 12.92 3.39 o -4 12 0 4.28 9.60 2.64 o -2 12 0 2101.97 2156.09 14.54 o 0 12 0 455.21 526.07 8.31 o 2 12 0 1819.14 1897.29 15.67 o 4 12 0 218.80 214.95 6.47 o 6 12 0 112.11 97.11 8.74 o -7 13 0 367.97 347.13 14.82 o -5 13 0 1334.66 1413.09 15.07 o -3 13 0 647.32 674.28 10.47 o -1 13 0 4.80 6.50 3.43 < 1 13 0 416.81 431.71 9.92 o 3 13 0 701.61 736.26 13.10 o 5 13 0 342.28 346.55 12.42 o -6 14 0 385.65 368.62 9.44 o -4 14 0 1322.17 1299.22 15.02 o -2 14 0 365.17 373.98 8.65 o 0 14 0 1933.65 1977.38 20.59 o 2 14 0 18.99 24.45 4.83 o 4 14 0 31.58 37.02 6.82 o -5 15 0 25.66 46.51 5.54 o -3 15 0 263.34 284.98 8.55 o -1 15 0 85.78 82.34 6.74 o 1 15 0 442.06 442.34 11.30 o 3 15 0 427.55 414.71 14.20 o 5 15 0 90.72 86.50 13.39 o -4 16 0 14.60 16.67 5.00 o -2 16 0 5.95 5.18 4.47 < 0 16 0 129.92 134.91 7.93 o 2 16 0 171.80 156.97 9.05 o 4 16 0 54.42 82.81 9.87 o -3 17 0 574.84 554.68 13.71 o -1 17 0 177.96 169.14 9.45 o 1 17 0 54.79 97.39 8.40 o 3 17 0 695.46 680.69 19.26 o -2 18 0 176.73 183.60 9.95 o 0 18 0 282.44 297.36 12.05 o -2 -18 1 173.33 157.03 10.61 o 0 -18 1 833.16 819.12 17.05 o -3 -17 1 417.75 409.70 15.46 o -1 -17 1 433.29 390.72 12.43 o 1 -17 1 92.66 93.04 7.86 o 3 -17 1 1170.84 1183.09 16.78 o -4 -16 1 105.01 134.63 11.11 o -2 -16 1 575.79 523.88 13.08 o 0 -16 1 1277.34 1258.01 18.45 o 2 -16 1 141.06 127.38 6.77 o 4 -16 1 3.64 5.25 4.40 < -5 -15 1 9.24 17.24 9.94 < -3 -15 1 553.50 580.21 13.12 o -1 -15 1 106.78 106.13 7.11 o 1 -15 1 770.32 795.05 12.48 o 3 -15 1 678.94 672.36 11.84 o 5 -15 1 374.59 380.18 10.21 o -6 -14 1 714.50 811.21 19.25 o -4 -14 1 318.60 324.27 9.81 o -2 -14 1 7.93 5.50 3.37 < 0 -14 1 627.07 640.37 9.32 o 2 -14 1 29.26 21.73 3.32 o 4 -14 1 0.01 -0.54 3.17 < 6 -14 1 602.57 599.99 13.34 o -7 -13 1 234.76 253.62 18.29 o -5 -13 1 731.30 798.96 17.19 o -3 -13 1 46.71 66.07 4.82 o -1 -13 1 18.24 14.55 3.26 o 1 -13 1 482.39 480.79 7.74 o 3 -13 1 116.22 110.66 4.84 o 5 -13 1 26.65 30.77 4.08 o 7 -13 1 849.38 857.41 13.61 o -8 -12 1 1482.57 1553.48 39.21 o -6 -12 1 527.13 558.86 14.79 o -4 -12 1 2.89 4.94 3.37 < -2 -12 1 2190.38 2217.94 16.92 o 0 -12 1 809.47 772.34 9.07 o 2 -12 1 1961.94 1982.29 14.38 o 4 -12 1 508.06 506.53 8.08 o 6 -12 1 142.29 126.52 6.49 o -7 -11 1 4.35 3.49 5.58 < -5 -11 1 276.90 269.32 6.87 o -3 -11 1 749.87 690.05 9.58 o -1 -11 1 70.58 72.13 3.48 o 1 -11 1 59.26 61.48 3.55 o 3 -11 1 631.61 640.59 8.27 o 5 -11 1 1.01 0.96 2.69 < 7 -11 1 608.55 590.50 11.03 o -8 -10 1 4.89 9.13 6.59 < -6 -10 1 0.02 1.55 3.45 < -4 -10 1 227.20 234.85 5.50 o -2 -10 1 316.56 319.56 5.33 o 0 -10 1 1146.18 1086.94 9.43 o 2 -10 1 421.35 396.36 6.17 o 4 -10 1 104.51 110.35 4.59 o 6 -10 1 548.19 578.26 10.87 o 8 -10 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