B-IncStrDB
Home
(current)
Explore the database
Validate CIF
Report an error
About us
Log in
Download CIF
#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_III _publ_contact_author_name 'Jana, Patha Pratim' _publ_contact_author_address ;CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 SE-22100 ; _publ_contact_author_email Partha.Jana@polymat.lth.se _publ_contact_author_fax +46462224012 _publ_contact_author_phone 0046462224769 loop_ _publ_author_name _publ_author_address 'Jana, Partha P.' ;CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 SE-22100 ; 'Lidin, Sven' ;CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 SE-22100 ; _publ_section_title ;Structural Impact of Platinum on the Incommensurably Modulated \g-Brass Related Composite Structure Pd~15~Zn~54~ ; _journal_name_full 'Inorganic Chemistry' _journal_volume 51 _journal_page_first 9893 _journal_page_last 9901 _journal_year 2012 _journal_paper_doi https://doi.org/10.1021/ic301326p _chemical_formula_sum 'Ho3.736 Pd1.992 Pt2.008 Zn26.772' _chemical_formula_weight 2970.2 _chemical_absolute_configuration ? _space_group_crystal_system orthorhombic _space_group_ssg_name Fmmm(\a00)0s0 loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,-x2,x3,-x4 3 -x1,x2,-x3,-x4+1/2 4 x1,-x2,-x3,x4+1/2 5 -x1,-x2,-x3,-x4 6 x1,x2,-x3,x4 7 x1,-x2,x3,x4+1/2 8 -x1,x2,x3,-x4+1/2 9 x1,x2+1/2,x3+1/2,x4 10 -x1,-x2+1/2,x3+1/2,-x4 11 -x1,x2+1/2,-x3+1/2,-x4+1/2 12 x1,-x2+1/2,-x3+1/2,x4+1/2 13 -x1,-x2+1/2,-x3+1/2,-x4 14 x1,x2+1/2,-x3+1/2,x4 15 x1,-x2+1/2,x3+1/2,x4+1/2 16 -x1,x2+1/2,x3+1/2,-x4+1/2 17 x1+1/2,x2,x3+1/2,x4 18 -x1+1/2,-x2,x3+1/2,-x4 19 -x1+1/2,x2,-x3+1/2,-x4+1/2 20 x1+1/2,-x2,-x3+1/2,x4+1/2 21 -x1+1/2,-x2,-x3+1/2,-x4 22 x1+1/2,x2,-x3+1/2,x4 23 x1+1/2,-x2,x3+1/2,x4+1/2 24 -x1+1/2,x2,x3+1/2,-x4+1/2 25 x1+1/2,x2+1/2,x3,x4 26 -x1+1/2,-x2+1/2,x3,-x4 27 -x1+1/2,x2+1/2,-x3,-x4+1/2 28 x1+1/2,-x2+1/2,-x3,x4+1/2 29 -x1+1/2,-x2+1/2,-x3,-x4 30 x1+1/2,x2+1/2,-x3,x4 31 x1+1/2,-x2+1/2,x3,x4+1/2 32 -x1+1/2,x2+1/2,x3,-x4+1/2 _cell_length_a 4.2881(13) _cell_length_b 9.14(4) _cell_length_c 12.926(7) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 506.6(4) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.627 0 0 _cell_subsystems_number 2 loop_ _cell_subsystem_code _cell_subsystem_description _cell_subsystem_matrix_W_1_1 _cell_subsystem_matrix_W_1_2 _cell_subsystem_matrix_W_1_3 _cell_subsystem_matrix_W_1_4 _cell_subsystem_matrix_W_2_1 _cell_subsystem_matrix_W_2_2 _cell_subsystem_matrix_W_2_3 _cell_subsystem_matrix_W_2_4 _cell_subsystem_matrix_W_3_1 _cell_subsystem_matrix_W_3_2 _cell_subsystem_matrix_W_3_3 _cell_subsystem_matrix_W_3_4 _cell_subsystem_matrix_W_4_1 _cell_subsystem_matrix_W_4_2 _cell_subsystem_matrix_W_4_3 _cell_subsystem_matrix_W_4_4 1 '1st subsystem' 1 0 0 0 0 1 0 0 0 0 1 0 0 0 0 1 2 '2nd subsystem' 1 0 0 1 0 1 0 0 0 0 1 0 0 0 0 1 _cell_formula_units_Z 1 _cell_measurement_temperature 293 _exptl_crystal_type_of_structure comp _exptl_crystal_density_diffrn 9.7326 _exptl_crystal_F_000 1302 _exptl_absorpt_coefficient_mu 60.856 _exptl_crystal_size_max 0.06 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.04 _exptl_absorpt_correction_type multi-scan _diffrn_ambient_temperature 293 _diffrn_radiation_type 'Mo K\a' _diffrn_source 'x-ray tube' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-cycle diffractometer' _diffrn_measurement_device_type 'Oxford Diffraction CCD' _diffrn_reflns_number 26583 _diffrn_reflns_theta_min 2.99 _diffrn_reflns_theta_max 29.04 _diffrn_reflns_theta_full 24.72 _diffrn_measured_fraction_theta_max 0.93 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0664 _diffrn_reflns_av_unetI/netI 0.0181 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_index_m_1_min -3 _diffrn_reflns_limit_index_m_1_max 3 loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? _reflns_number_total 1161 _reflns_number_gt 991 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.044 _refine_ls_wR_factor_gt 0.0992 _refine_ls_R_factor_all 0.0513 _refine_ls_wR_factor_ref 0.1011 _refine_ls_goodness_of_fit_ref 2.27 _refine_ls_goodness_of_fit_gt 2.43 _refine_ls_number_reflns 1161 _refine_ls_number_parameters 79 _refine_ls_number_constraints 48 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(I)+0.0004I^2^) _refine_ls_shift/su_max 0.0296 _refine_ls_shift/su_mean 0.0065 _refine_diff_density_max 4.27 _refine_diff_density_min -4.27 _refine_ls_extinction_method 'B-C type 1 gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 85(12) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ho -0.2175 4.6783 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Pd -0.9988 1.0072 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Pt -1.7033 8.3905 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Zn 0.2839 1.4301 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_subsystem_code Pt1 Pt 0.5 0 0 Uani 0.0096(2) 4 0.502(7) d ? ? ? 1 Pd1 Pd 0.5 0 0 Uani 0.0096(2) 4 0.498(7) d ? ? ? 1 Ho2 Ho 0.5 0.15099(7) 0.17961(5) Uani 0.0138(3) 16 0.233(4) d ? ? ? 1 Zn2 Zn 0.5 0.15099(7) 0.17961(5) Uani 0.0138(3) 16 0.767(4) d ? ? ? 1 Zn1 Zn 0 0 0.12341(9) Uani 0.0165(4) 8 1 d ? ? ? 1 Zn3 Zn 0.75 0.25 0 Uani 0.0155(4) 4 1 d ? ? ? 2 loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pt1 Pt 0.009(4) 0.0116(4) 0.0082(4) 0 0 0 Pd1 Pd 0.009(4) 0.0116(4) 0.0082(4) 0 0 0 Ho2 Ho 0.0134(5) 0.016(5) 0.0119(4) 0 0 -0.003(2) Zn2 Zn 0.0134(5) 0.016(5) 0.0119(4) 0 0 -0.003(2) Zn1 Zn 0.009(6) 0.0216(7) 0.0189(6) 0 0 0 Zn3 Zn 0.0169(7) 0.0153(6) 0.0142(6) 0 0 0 loop_ _atom_site_Fourier_wave_vector_seq_id _jana_atom_site_Fourier_wave_vector_q1_coeff 1 1 2 2 3 3 loop_ _atom_site_occ_Fourier_id _atom_site_occ_Fourier_atom_site_label _atom_site_occ_Fourier_wave_vector_seq_id Pt1o1 Pt1 1 Pt1o2 Pt1 2 Pt1o3 Pt1 3 Pd1o1 Pd1 1 Pd1o2 Pd1 2 Pd1o3 Pd1 3 Ho2o1 Ho2 1 Ho2o2 Ho2 2 Ho2o3 Ho2 3 Zn2o1 Zn2 1 Zn2o2 Zn2 2 Zn2o3 Zn2 3 loop_ _atom_site_occ_Fourier_param_id _atom_site_occ_Fourier_param_cos _atom_site_occ_Fourier_param_sin Pt1o1 0 0 Pt1o2 0.395(6) 0 Pt1o3 0 0 Pd1o1 0 0 Pd1o2 -0.395(6) 0 Pd1o3 0 0 Ho2o1 0 -0.407(4) Ho2o2 -0.263(3) 0 Ho2o3 0 0.124(2) Zn2o1 0 0.407(4) Zn2o2 0.263(3) 0 Zn2o3 0 -0.124(2) loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Pt1x1 Pt1 x 1 Pt1y1 Pt1 y 1 Pt1z1 Pt1 z 1 Pt1x2 Pt1 x 2 Pt1y2 Pt1 y 2 Pt1z2 Pt1 z 2 Pt1x3 Pt1 x 3 Pt1y3 Pt1 y 3 Pt1z3 Pt1 z 3 Pd1x1 Pd1 x 1 Pd1y1 Pd1 y 1 Pd1z1 Pd1 z 1 Pd1x2 Pd1 x 2 Pd1y2 Pd1 y 2 Pd1z2 Pd1 z 2 Pd1x3 Pd1 x 3 Pd1y3 Pd1 y 3 Pd1z3 Pd1 z 3 Ho2x1 Ho2 x 1 Ho2y1 Ho2 y 1 Ho2z1 Ho2 z 1 Ho2x2 Ho2 x 2 Ho2y2 Ho2 y 2 Ho2z2 Ho2 z 2 Ho2x3 Ho2 x 3 Ho2y3 Ho2 y 3 Ho2z3 Ho2 z 3 Zn2x1 Zn2 x 1 Zn2y1 Zn2 y 1 Zn2z1 Zn2 z 1 Zn2x2 Zn2 x 2 Zn2y2 Zn2 y 2 Zn2z2 Zn2 z 2 Zn2x3 Zn2 x 3 Zn2y3 Zn2 y 3 Zn2z3 Zn2 z 3 Zn1x1 Zn1 x 1 Zn1y1 Zn1 y 1 Zn1z1 Zn1 z 1 Zn1x2 Zn1 x 2 Zn1y2 Zn1 y 2 Zn1z2 Zn1 z 2 Zn1x3 Zn1 x 3 Zn1y3 Zn1 y 3 Zn1z3 Zn1 z 3 Zn3x1 Zn3 x 1 Zn3y1 Zn3 y 1 Zn3z1 Zn3 z 1 Zn3x2 Zn3 x 2 Zn3y2 Zn3 y 2 Zn3z2 Zn3 z 2 Zn3x3 Zn3 x 3 Zn3y3 Zn3 y 3 Zn3z3 Zn3 z 3 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Pt1x1 0 0 Pt1y1 0 0.02497(11) Pt1z1 0 0 Pt1x2 0 0.0039(2) Pt1y2 0 0 Pt1z2 0 0 Pt1x3 0 0 Pt1y3 0 0.00077(10) Pt1z3 0 0 Pd1x1 0 0 Pd1y1 0 0.02497(11) Pd1z1 0 0 Pd1x2 0 0.0039(2) Pd1y2 0 0 Pd1z2 0 0 Pd1x3 0 0 Pd1y3 0 0.00077(10) Pd1z3 0 0 Ho2x1 -0.0677(3) 0 Ho2y1 0 -0.0192(9) Ho2z1 0 0.00344(6) Ho2x2 0 -0.0131(2) Ho2y2 0.00548(9) 0 Ho2z2 -0.00334(7) 0 Ho2x3 0.0065(2) 0 Ho2y3 0 0.00483(9) Ho2z3 0 -0.0015(6) Zn2x1 -0.0677(3) 0 Zn2y1 0 -0.0192(9) Zn2z1 0 0.00344(6) Zn2x2 0 -0.0131(2) Zn2y2 0.00548(9) 0 Zn2z2 -0.00334(7) 0 Zn2x3 0.0065(2) 0 Zn2y3 0 0.00483(9) Zn2z3 0 -0.0015(6) Zn1x1 0 0 Zn1y1 0 0.05187(17) Zn1z1 0 0 Zn1x2 0 0.0129(4) Zn1y2 0 0 Zn1z2 0.00867(11) 0 Zn1x3 0 0 Zn1y3 0 0.0032(2) Zn1z3 0 0 Zn3x1 0 0 Zn3y1 0 0.0567(18) Zn3z1 0 0 Zn3x2 0 -0.0385(7) Zn3y2 0 0 Zn3z2 0 0 Zn3x3 0 0 Zn3y3 0 0.00184(18) Zn3z3 0 0 loop_ _atom_site_U_Fourier_id _atom_site_U_Fourier_atom_site_label _atom_site_U_Fourier_tens_elem _atom_site_U_Fourier_wave_vector_seq_id Pt1U111 Pt1 U11 1 Pt1U221 Pt1 U22 1 Pt1U331 Pt1 U33 1 Pt1U121 Pt1 U12 1 Pt1U131 Pt1 U13 1 Pt1U231 Pt1 U23 1 Pt1U112 Pt1 U11 2 Pt1U222 Pt1 U22 2 Pt1U332 Pt1 U33 2 Pt1U122 Pt1 U12 2 Pt1U132 Pt1 U13 2 Pt1U232 Pt1 U23 2 Pt1U113 Pt1 U11 3 Pt1U223 Pt1 U22 3 Pt1U333 Pt1 U33 3 Pt1U123 Pt1 U12 3 Pt1U133 Pt1 U13 3 Pt1U233 Pt1 U23 3 Pd1U111 Pd1 U11 1 Pd1U221 Pd1 U22 1 Pd1U331 Pd1 U33 1 Pd1U121 Pd1 U12 1 Pd1U131 Pd1 U13 1 Pd1U231 Pd1 U23 1 Pd1U112 Pd1 U11 2 Pd1U222 Pd1 U22 2 Pd1U332 Pd1 U33 2 Pd1U122 Pd1 U12 2 Pd1U132 Pd1 U13 2 Pd1U232 Pd1 U23 2 Pd1U113 Pd1 U11 3 Pd1U223 Pd1 U22 3 Pd1U333 Pd1 U33 3 Pd1U123 Pd1 U12 3 Pd1U133 Pd1 U13 3 Pd1U233 Pd1 U23 3 Ho2U111 Ho2 U11 1 Ho2U221 Ho2 U22 1 Ho2U331 Ho2 U33 1 Ho2U121 Ho2 U12 1 Ho2U131 Ho2 U13 1 Ho2U231 Ho2 U23 1 Ho2U112 Ho2 U11 2 Ho2U222 Ho2 U22 2 Ho2U332 Ho2 U33 2 Ho2U122 Ho2 U12 2 Ho2U132 Ho2 U13 2 Ho2U232 Ho2 U23 2 Ho2U113 Ho2 U11 3 Ho2U223 Ho2 U22 3 Ho2U333 Ho2 U33 3 Ho2U123 Ho2 U12 3 Ho2U133 Ho2 U13 3 Ho2U233 Ho2 U23 3 Zn2U111 Zn2 U11 1 Zn2U221 Zn2 U22 1 Zn2U331 Zn2 U33 1 Zn2U121 Zn2 U12 1 Zn2U131 Zn2 U13 1 Zn2U231 Zn2 U23 1 Zn2U112 Zn2 U11 2 Zn2U222 Zn2 U22 2 Zn2U332 Zn2 U33 2 Zn2U122 Zn2 U12 2 Zn2U132 Zn2 U13 2 Zn2U232 Zn2 U23 2 Zn2U113 Zn2 U11 3 Zn2U223 Zn2 U22 3 Zn2U333 Zn2 U33 3 Zn2U123 Zn2 U12 3 Zn2U133 Zn2 U13 3 Zn2U233 Zn2 U23 3 Zn1U111 Zn1 U11 1 Zn1U221 Zn1 U22 1 Zn1U331 Zn1 U33 1 Zn1U121 Zn1 U12 1 Zn1U131 Zn1 U13 1 Zn1U231 Zn1 U23 1 Zn1U112 Zn1 U11 2 Zn1U222 Zn1 U22 2 Zn1U332 Zn1 U33 2 Zn1U122 Zn1 U12 2 Zn1U132 Zn1 U13 2 Zn1U232 Zn1 U23 2 Zn1U113 Zn1 U11 3 Zn1U223 Zn1 U22 3 Zn1U333 Zn1 U33 3 Zn1U123 Zn1 U12 3 Zn1U133 Zn1 U13 3 Zn1U233 Zn1 U23 3 Zn3U111 Zn3 U11 1 Zn3U221 Zn3 U22 1 Zn3U331 Zn3 U33 1 Zn3U121 Zn3 U12 1 Zn3U131 Zn3 U13 1 Zn3U231 Zn3 U23 1 Zn3U112 Zn3 U11 2 Zn3U222 Zn3 U22 2 Zn3U332 Zn3 U33 2 Zn3U122 Zn3 U12 2 Zn3U132 Zn3 U13 2 Zn3U232 Zn3 U23 2 Zn3U113 Zn3 U11 3 Zn3U223 Zn3 U22 3 Zn3U333 Zn3 U33 3 Zn3U123 Zn3 U12 3 Zn3U133 Zn3 U13 3 Zn3U233 Zn3 U23 3 loop_ _atom_site_U_Fourier_param_id _atom_site_U_Fourier_param_cos _atom_site_U_Fourier_param_sin Pt1U111 0 0 Pt1U221 0 0 Pt1U331 0 0 Pt1U121 0.0005(3) 0 Pt1U131 0 0 Pt1U231 0 0 Pt1U112 -0.002(6) 0 Pt1U222 -0.0014(5) 0 Pt1U332 0.0002(5) 0 Pt1U122 0 0 Pt1U132 0 0 Pt1U232 0 0 Pt1U113 0 0 Pt1U223 0 0 Pt1U333 0 0 Pt1U123 0.0011(4) 0 Pt1U133 0 0 Pt1U233 0 0 Pd1U111 0 0 Pd1U221 0 0 Pd1U331 0 0 Pd1U121 0.0005(3) 0 Pd1U131 0 0 Pd1U231 0 0 Pd1U112 -0.002(6) 0 Pd1U222 -0.0014(5) 0 Pd1U332 0.0002(5) 0 Pd1U122 0 0 Pd1U132 0 0 Pd1U232 0 0 Pd1U113 0 0 Pd1U223 0 0 Pd1U333 0 0 Pd1U123 0.0011(4) 0 Pd1U133 0 0 Pd1U233 0 0 Ho2U111 0 0.0066(6) Ho2U221 0 0.0019(5) Ho2U331 0 0.0015(4) Ho2U121 -0.0009(4) 0 Ho2U131 0.0024(4) 0 Ho2U231 0 -0.0017(3) Ho2U112 0.0003(7) 0 Ho2U222 0.0046(6) 0 Ho2U332 -0.0006(5) 0 Ho2U122 0 0.0001(4) Ho2U132 0 0.0009(3) Ho2U232 -0.0009(4) 0 Ho2U113 0 0.0019(6) Ho2U223 0 0.0022(5) Ho2U333 0 -0.0018(4) Ho2U123 0.0009(4) 0 Ho2U133 0.001(4) 0 Ho2U233 0 -0.0006(4) Zn2U111 0 0.0066(6) Zn2U221 0 0.0019(5) Zn2U331 0 0.0015(4) Zn2U121 -0.0009(4) 0 Zn2U131 0.0024(4) 0 Zn2U231 0 -0.0017(3) Zn2U112 0.0003(7) 0 Zn2U222 0.0046(6) 0 Zn2U332 -0.0006(5) 0 Zn2U122 0 0.0001(4) Zn2U132 0 0.0009(3) Zn2U232 -0.0009(4) 0 Zn2U113 0 0.0019(6) Zn2U223 0 0.0022(5) Zn2U333 0 -0.0018(4) Zn2U123 0.0009(4) 0 Zn2U133 0.001(4) 0 Zn2U233 0 -0.0006(4) Zn1U111 0 0 Zn1U221 0 0 Zn1U331 0 0 Zn1U121 0.0051(7) 0 Zn1U131 0 0 Zn1U231 0 -0.0063(6) Zn1U112 0.0019(8) 0 Zn1U222 0.0022(9) 0 Zn1U332 -0.003(7) 0 Zn1U122 0 0 Zn1U132 0 0.004(6) Zn1U232 0 0 Zn1U113 0 0 Zn1U223 0 0 Zn1U333 0 0 Zn1U123 0.0051(8) 0 Zn1U133 0 0 Zn1U233 0 0.0043(8) Zn3U111 0 0 Zn3U221 0 0 Zn3U331 0 0 Zn3U121 -0.008(8) 0 Zn3U131 0 0 Zn3U231 0 0 Zn3U112 0.0068(10) 0 Zn3U222 0.0063(8) 0 Zn3U332 -0.0035(7) 0 Zn3U122 0 0 Zn3U132 0 0 Zn3U232 0 0 Zn3U113 0 0 Zn3U223 0 0 Zn3U333 0 0 Zn3U123 0.001(8) 0 Zn3U133 0 0 Zn3U233 0 0 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_ssg_symmetry_1 _geom_bond_site_ssg_symmetry_2 _geom_bond_distance_av _geom_bond_distance_min _geom_bond_distance_max _geom_bond_publ_flag Pt1 Pd1 ? ? 2.887(15) 2.286(5) 3.63(3) ? Pt1 Pd1 ? 1_6555 4.015(14) 2.48(3) 5.75(3) ? Pt1 Pd1 ? 25_4455 4.015(14) 2.48(3) 5.75(3) ? Pt1 Pd1 ? 25_5455 2.887(15) 2.286(5) 3.63(3) ? Pt1 Pd1 ? 3_4555 4.022(14) 2.48(3) 5.75(3) ? Pt1 Pd1 ? 3_5555 2.895(15) 2.286(5) 3.63(3) ? Pt1 Pd1 ? 27_4455 2.895(15) 2.286(5) 3.63(3) ? Pt1 Pd1 ? 27_5455 4.022(14) 2.48(3) 5.75(3) ? #Pt1 Pd2 ? ? 2.721(9) 2.549(12) 2.895(13) ? #Pt1 Pd2 ? 2_5555 2.721(9) 2.549(12) 2.895(13) ? #Pt1 Pd2 ? 3_5555 2.721(9) 2.549(12) 2.895(13) ? #Pt1 Pd2 ? 4_5555 2.721(9) 2.549(12) 2.895(13) ? Pt1 Zn1 ? ? 2.666(9) 2.629(8) 2.702(9) ? Pt1 Zn1 ? 1_6555 2.666(9) 2.629(8) 2.702(9) ? Pt1 Zn1 ? 3_4555 2.666(9) 2.629(8) 2.702(9) ? Pt1 Zn1 ? 3_5555 2.666(9) 2.629(8) 2.702(9) ? Pd1 Pd1 ? 1_4555 4.34(2) 0.73(3) 8.04(4) ? Pd1 Pd1 ? 1_6555 4.29(2) 0.73(3) 8.04(4) ? Pd1 Pd1 ? 3_3555 6.43(2) 2.4(4) 10.4(4) ? Pd1 Pd1 ? 3_4555 2.22(2) 0.118(13) 4.386(13) ? Pd1 Pd1 ? 3_5555 2.2(2) 0.118(13) 4.386(13) ? Pd1 Pd1 ? 3_6555 6.36(2) 2.4(4) 10.4(4) ? #Pd1 Pd2 ? 1_4555 4.163(15) 2.643(17) 5.86(3) ? #Pd1 Pd2 ? ? 3.11(14) 2.476(12) 4.15(3) ? #Pd1 Pd2 ? 26_4555 3.12(14) 2.476(11) 4.15(3) ? #Pd1 Pd2 ? 26_5555 4.137(15) 2.643(17) 5.86(3) ? #Pd1 Pd2 ? 3_4555 4.163(15) 2.643(17) 5.86(3) ? #Pd1 Pd2 ? 3_5555 3.11(14) 2.476(12) 4.15(3) ? #Pd1 Pd2 ? 28_4555 3.12(14) 2.476(11) 4.15(3) ? #Pd1 Pd2 ? 28_5555 4.137(15) 2.643(17) 5.86(3) ? Pd1 Zn1 ? ? 3.238(17) 2.221(19) 4.51(3) ? Pd1 Zn1 ? 1_6555 4.3(16) 2.82(3) 6.01(3) ? Pd1 Zn1 ? 25_4555 4.327(16) 2.82(3) 6(3) ? Pd1 Zn1 ? 25_5555 3.221(17) 2.221(19) 4.51(3) ? Pd1 Zn1 ? 3_4555 3.238(17) 2.221(19) 4.51(3) ? Pd1 Zn1 ? 3_5555 4.3(16) 2.82(3) 6.01(3) ? Pd1 Zn1 ? 27_3555 4.327(16) 2.82(3) 6(3) ? Pd1 Zn1 ? 27_4555 3.221(17) 2.221(19) 4.51(3) ? #Pd2 Pd2 ? 2_5555 2.792(13) 2.76(17) 2.824(10) ? #Pd2 Pd2 ? 26_4555 2.809(11) 2.747(11) 2.902(8) ? #Pd2 Pd2 ? 26_5555 2.809(11) 2.747(11) 2.902(8) ? #Pd2 Pd2 ? 19_4555 2.808(11) 2.446(11) 3.183(11) ? #Pd2 Pd2 ? 19_5555 2.814(11) 2.446(11) 3.183(11) ? #Pd2 Pd2 ? 12_5555 2.587(13) 2.552(17) 2.621(11) ? #Pd2 Zn1 ? ? 2.69(11) 2.636(8) 2.729(17) ? #Pd2 Zn1 ? 1_6555 2.689(11) 2.636(8) 2.729(17) ? #Pd2 Zn1 ? 25_5555 3.288(15) 2.62(2) 3.94(2) ? #Pd2 Zn1 ? 19_4555 2.974(17) 2.674(19) 3.32(2) ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 0 2 2743.17 3358.47 84.01 o 2 0 0 -2 2237.80 2828.88 71.32 o 2 0 0 0 378169.00 389469.00 2596.78 o 2 0 0 2 41441.40 39980.90 861.13 o 4 0 0 -2 1335.97 1666.88 140.40 o 4 0 0 0 130200.00 129097.00 1854.85 o 4 0 0 2 21639.00 18453.10 634.25 o 0 2 0 0 3431.45 2875.30 62.07 o 0 2 0 1 8663.96 9595.30 96.84 o 0 2 0 2 1499.77 1632.65 45.98 o 0 2 0 3 1776.80 1835.76 66.67 o 2 2 0 -3 1070.52 903.26 18.97 o 2 2 0 -2 3452.82 3905.83 62.63 o 2 2 0 -1 11207.70 10398.20 119.72 o 2 2 0 0 30876.70 30900.80 294.37 o 2 2 0 1 37166.60 38253.30 425.36 o 2 2 0 2 19716.10 18824.50 302.03 o 2 2 0 3 3984.36 3810.55 179.66 o 4 2 0 -3 202.01 230.09 33.87 o 4 2 0 -2 3226.04 3963.74 135.71 o 4 2 0 -1 11361.30 10298.90 261.06 o 4 2 0 0 21970.70 19632.00 411.70 o 4 2 0 1 15846.80 15935.60 394.97 o 4 2 0 2 5009.11 4052.91 208.05 o 0 4 0 0 1517.64 1379.85 43.08 o 0 4 0 1 141071.00 139584.00 692.18 o 0 4 0 2 9496.59 9212.63 136.71 o 0 4 0 3 439.98 390.02 32.33 o 2 4 0 -3 586.67 439.23 19.33 o 2 4 0 -2 10192.80 9594.01 128.26 o 2 4 0 -1 37944.40 39128.60 320.41 o 2 4 0 0 18.09 66.89 20.70 o 2 4 0 1 139985.00 149135.00 993.99 o 2 4 0 2 460.33 438.79 54.91 o 2 4 0 3 4303.83 4282.71 187.19 o 4 4 0 -3 0.83 24.98 24.64 < 4 4 0 -2 12276.80 12318.10 232.47 o 4 4 0 -1 7359.73 8378.77 224.28 o 4 4 0 0 6299.89 6606.13 234.63 o 4 4 0 1 51138.50 52636.50 818.99 o 4 4 0 2 4412.52 3517.71 417.51 o 0 6 0 0 169886.00 157780.00 1375.12 o 0 6 0 1 845.23 880.36 42.08 o 0 6 0 2 222.85 302.12 32.16 o 0 6 0 3 180.72 320.26 52.52 o 2 6 0 -3 2685.92 2185.21 65.30 o 2 6 0 -2 3523.67 3243.02 79.64 o 2 6 0 -1 1226.81 1095.61 53.87 o 2 6 0 0 138610.00 158285.00 1125.97 o 2 6 0 1 4999.53 6160.03 186.80 o 2 6 0 2 1049.06 1277.24 105.88 o 2 6 0 3 1590.42 2178.01 165.57 o 4 6 0 -3 4277.27 4541.68 155.87 o 4 6 0 -2 2169.28 2454.65 111.15 o 4 6 0 -1 89.16 113.77 47.22 < 4 6 0 0 36725.20 41641.00 771.75 o 4 6 0 1 11121.30 11755.60 508.10 o 0 8 0 0 1912.96 1907.66 165.71 o 0 8 0 1 275.14 323.50 45.85 o 0 8 0 2 19206.50 18690.90 362.62 o 0 8 0 3 5978.67 6334.08 215.49 o 2 8 0 -3 3393.16 2780.46 127.54 o 2 8 0 -2 3749.58 3486.65 140.18 o 2 8 0 -1 1109.49 1262.66 89.97 o 2 8 0 0 124.39 169.37 43.28 o 2 8 0 1 724.67 1097.71 103.83 o 2 8 0 2 14985.50 18563.70 442.18 o 2 8 0 3 1718.65 1970.20 224.06 o 4 8 0 -3 1771.53 1530.70 119.21 o 4 8 0 -2 1180.28 1494.63 123.84 o 4 8 0 -1 4123.65 6119.36 280.05 o 4 8 0 0 642.04 773.40 153.28 o 0 10 0 0 4941.66 4881.65 278.12 o 0 10 0 1 33687.60 30594.10 530.16 o 0 10 0 2 971.96 1043.11 118.37 o 0 10 0 3 156.22 81.95 54.57 < 2 10 0 -3 137.49 267.06 53.55 o 2 10 0 -2 3276.81 3245.20 167.91 o 2 10 0 -1 31679.10 28486.00 613.13 o 2 10 0 0 1296.54 1180.07 134.10 o 2 10 0 1 25113.60 30977.50 791.74 o 2 10 0 2 2555.73 3697.61 767.53 o 4 10 0 -3 7.88 10.09 54.40 < 4 10 0 -2 2159.87 2602.71 238.41 o 0 12 0 1 1081.19 1032.33 311.67 o 0 12 0 2 562.41 788.64 191.94 o 2 12 0 -2 931.64 847.61 192.44 o 2 12 0 -1 77.50 278.52 165.44 < 1 1 1 -3 472.00 564.70 15.73 o 1 1 1 -2 152.40 150.35 13.34 o 1 1 1 -1 2167.08 2083.63 32.58 o 1 1 1 0 25458.40 26497.10 119.35 o 1 1 1 1 1338.87 1516.32 34.54 o 1 1 1 2 884.96 938.61 41.90 o 1 1 1 3 1913.97 1979.22 70.62 o 3 1 1 -3 61.16 76.81 10.44 o 3 1 1 -2 17.06 53.38 13.17 o 3 1 1 -1 74.07 248.24 26.35 o 3 1 1 0 11033.30 11181.90 163.57 o 3 1 1 1 5226.36 5001.11 143.37 o 3 1 1 2 268.76 256.44 40.55 o 3 1 1 3 490.68 603.03 59.02 o 5 1 1 -3 61.46 149.18 31.48 o 5 1 1 -2 16.37 146.79 36.61 o 5 1 1 -1 129.02 300.59 44.48 o 5 1 1 0 3128.49 2738.70 117.65 o 5 1 1 1 2475.52 1742.19 232.08 o 1 3 1 -3 9.59 34.39 8.90 o 1 3 1 -2 1976.12 1809.45 25.12 o 1 3 1 -1 634.86 653.13 16.42 o 1 3 1 0 753.04 830.13 25.48 o 1 3 1 1 12616.50 12749.60 120.51 o 1 3 1 2 167.99 199.99 24.46 o 1 3 1 3 339.60 359.25 34.90 o 3 3 1 -3 76.44 57.65 13.86 o 3 3 1 -2 1310.54 1211.70 37.28 o 3 3 1 -1 325.63 232.14 23.95 o 3 3 1 0 341.57 279.53 29.94 o 3 3 1 1 806.30 691.41 53.37 o 3 3 1 2 674.63 778.34 62.95 o 3 3 1 3 1498.67 1311.05 85.18 o 5 3 1 -3 133.70 152.77 28.74 o 5 3 1 -2 957.49 837.64 59.70 o 5 3 1 -1 126.19 131.90 34.39 o 5 3 1 0 693.21 785.71 68.08 o 5 3 1 1 222.77 263.98 117.70 < 1 5 1 -3 296.93 368.31 20.36 o 1 5 1 -2 251.79 211.10 13.17 o 1 5 1 -1 352.87 407.47 17.79 o 1 5 1 0 2192.05 2255.31 49.41 o 1 5 1 1 10521.40 11266.80 136.10 o 1 5 1 2 772.30 863.30 41.22 o 1 5 1 3 227.04 304.69 32.68 o 3 5 1 -3 12.00 39.86 12.49 o 3 5 1 -2 186.74 262.77 23.44 o 3 5 1 -1 320.20 316.83 26.17 o 3 5 1 0 8542.71 9067.09 159.84 o 3 5 1 1 2905.42 3038.35 112.51 o 3 5 1 2 752.12 756.10 69.62 o 3 5 1 3 612.91 607.12 102.47 o 5 5 1 -3 91.94 107.10 28.57 o 5 5 1 -2 258.48 400.15 47.56 o 5 5 1 -1 104.90 67.58 40.20 < 5 5 1 0 4407.03 3360.07 284.32 o 1 7 1 -3 820.94 902.12 38.49 o 1 7 1 -2 411.76 346.58 25.49 o 1 7 1 -1 40.46 42.94 13.86 o 1 7 1 0 57306.60 54319.10 347.68 o 1 7 1 1 3381.28 3356.55 89.07 o 1 7 1 2 1288.72 1410.23 69.27 o 1 7 1 3 6.36 84.52 33.53 < 3 7 1 -3 299.63 454.71 35.75 o 3 7 1 -2 28.87 126.60 24.81 o 3 7 1 -1 255.93 294.42 37.98 o 3 7 1 0 14079.90 17377.70 277.64 o 3 7 1 1 448.49 497.48 53.37 o 3 7 1 2 2774.56 2766.11 179.73 o 5 7 1 -3 157.56 232.33 39.52 o 5 7 1 -2 13.43 79.21 37.98 < 5 7 1 -1 21.16 95.29 55.26 < 1 9 1 -3 162.63 157.05 29.60 o 1 9 1 -2 136.68 143.20 25.49 o 1 9 1 -1 160.80 159.62 27.03 o 1 9 1 0 14.85 83.83 27.37 o 1 9 1 1 3.89 54.41 32.16 < 1 9 1 2 1314.68 1445.86 104.00 o 1 9 1 3 235.67 358.41 56.46 o 3 9 1 -3 18.01 9.41 26.52 < 3 9 1 -2 70.74 216.08 41.23 o 3 9 1 -1 3309.93 3785.88 168.94 o 3 9 1 0 2012.57 2406.22 127.07 o 3 9 1 1 547.20 853.99 147.80 o 5 9 1 -3 60.55 86.06 43.63 < 5 9 1 -2 75.97 275.44 114.28 < 1 11 1 -3 47.24 46.19 28.57 < 1 11 1 -2 362.10 308.96 45.16 o 1 11 1 -1 9288.70 8331.76 210.80 o 1 11 1 0 3444.11 3137.36 136.45 o 1 11 1 1 12584.00 11097.60 333.99 o 1 11 1 2 70.05 21.04 59.71 < 3 11 1 -3 34.24 -2.57 34.73 < 3 11 1 -2 124.94 128.14 54.23 < 3 11 1 -1 1704.76 1850.50 238.95 o 0 0 2 0 2865.46 2758.65 80.26 o 0 0 2 2 5538.35 5934.51 74.84 o 2 0 2 -2 4723.63 4831.05 49.74 o 2 0 2 0 1190.31 1255.66 53.18 o 2 0 2 2 369.41 401.50 37.29 o 4 0 2 -2 4689.96 4194.22 121.81 o 4 0 2 0 1570.95 2008.76 127.25 o 4 0 2 2 2913.74 2955.51 177.16 o 0 2 2 0 31826.50 29167.30 143.21 o 0 2 2 1 3499.98 3546.12 38.91 o 0 2 2 2 872.77 809.21 22.23 o 0 2 2 3 1177.78 1248.00 41.55 o 2 2 2 -3 93.12 157.56 6.84 o 2 2 2 -2 64.63 115.99 10.09 o 2 2 2 -1 30.74 92.04 13.00 o 2 2 2 0 57002.10 57242.50 320.96 o 2 2 2 1 12277.60 12399.00 145.75 o 2 2 2 2 2713.13 2559.82 82.58 o 2 2 2 3 204.38 363.54 47.22 o 4 2 2 -3 445.50 474.17 31.13 o 4 2 2 -2 184.90 309.99 28.40 o 4 2 2 -1 428.38 481.04 41.06 o 4 2 2 0 21568.50 19167.10 284.67 o 4 2 2 1 11601.20 10370.70 228.80 o 4 2 2 2 145.78 231.30 54.75 o 0 4 2 0 168197.00 156002.00 756.76 o 0 4 2 1 294.56 319.04 16.08 o 0 4 2 2 1140.28 1101.16 38.99 o 0 4 2 3 2238.97 2338.48 62.74 o 2 4 2 -3 912.34 1188.05 28.73 o 2 4 2 -2 72.38 121.64 11.46 o 2 4 2 -1 9.77 59.02 16.94 o 2 4 2 0 66668.60 70685.30 392.82 o 2 4 2 1 125.58 197.43 26.52 o 2 4 2 2 2660.83 2608.92 87.37 o 2 4 2 3 151.18 281.08 49.44 o 4 4 2 -3 264.46 392.10 34.21 o 4 4 2 -2 192.85 336.68 33.02 o 4 4 2 -1 758.87 940.99 58.16 o 4 4 2 0 20743.00 21649.50 327.24 o 4 4 2 1 1739.46 1625.02 98.52 o 4 4 2 2 498.43 380.12 103.50 o 0 6 2 0 5134.73 4976.22 102.33 o 0 6 2 1 1102.24 1116.49 34.89 o 0 6 2 2 432.34 403.71 27.03 o 0 6 2 3 231.48 275.26 30.28 o 2 6 2 -3 12.20 21.56 10.27 < 2 6 2 -2 2045.66 1912.14 46.51 o 2 6 2 -1 15272.60 14601.40 160.52 o 2 6 2 0 78.03 160.30 26.00 o 2 6 2 1 265.60 322.14 35.07 o 2 6 2 2 6627.31 7726.53 172.58 o 2 6 2 3 423.40 382.52 48.41 o 4 6 2 -3 271.68 228.04 27.89 o 4 6 2 -2 1338.35 1754.17 73.03 o 4 6 2 -1 6979.11 7080.86 180.09 o 4 6 2 0 646.33 678.62 63.98 o 4 6 2 1 191.94 391.60 75.28 o 0 8 2 0 2633.60 2605.69 115.42 o 0 8 2 1 25964.90 24792.80 274.09 o 0 8 2 2 1602.46 1636.75 67.73 o 0 8 2 3 122.60 101.62 29.77 o 2 8 2 -3 48.87 117.53 20.19 o 2 8 2 -2 863.48 883.84 50.63 o 2 8 2 -1 3428.79 3532.69 99.33 o 2 8 2 0 1135.16 1166.04 69.10 o 2 8 2 1 31712.80 38057.70 470.05 o 2 8 2 2 28.98 79.21 32.33 < 2 8 2 3 426.24 531.70 88.96 o 4 8 2 -3 56.98 66.04 29.08 < 4 8 2 -2 2214.27 2518.95 119.54 o 4 8 2 -1 1299.54 1918.83 111.01 o 4 8 2 0 3964.98 4815.18 305.37 o 0 10 2 0 24323.60 21192.90 426.77 o 0 10 2 1 1150.83 1127.06 71.33 o 0 10 2 2 165.54 165.43 34.39 o 0 10 2 3 283.03 365.08 63.13 o 2 10 2 -3 1605.24 1569.62 80.39 o 2 10 2 -2 2435.60 2164.70 102.44 o 2 10 2 -1 8.89 19.16 32.16 < 2 10 2 0 17684.50 19361.60 377.87 o 2 10 2 1 858.43 1035.27 93.40 o 2 10 2 2 49.86 239.35 143.54 < 4 10 2 -3 1206.71 1309.58 98.70 o 4 10 2 -2 903.13 799.20 104.86 o 0 12 2 0 1636.25 1327.64 206.62 o 0 12 2 1 648.55 390.04 86.56 o 2 12 2 -3 104.88 -18.65 62.10 < 2 12 2 -2 278.79 267.05 80.75 o 1 1 3 -3 1466.53 1368.61 22.05 o 1 1 3 -2 4600.54 4672.74 37.50 o 1 1 3 -1 13069.50 13676.90 69.77 o 1 1 3 0 1386.16 1365.15 22.22 o 1 1 3 1 124684.00 132922.00 479.61 o 1 1 3 2 5049.86 4970.31 80.95 o 1 1 3 3 573.93 578.69 36.26 o 3 1 3 -3 33.56 74.08 8.04 o 3 1 3 -2 8622.14 9143.08 90.17 o 3 1 3 -1 10.76 188.54 23.10 o 3 1 3 0 9836.12 9707.42 145.73 o 3 1 3 1 55551.40 54354.70 442.11 o 3 1 3 2 5532.38 4905.11 142.20 o 3 1 3 3 8884.38 7747.20 210.81 o 5 1 3 -3 651.76 636.67 41.05 o 5 1 3 -2 6293.14 6582.52 153.43 o 5 1 3 -1 222.24 170.22 37.98 o 5 1 3 0 12254.10 10327.20 245.70 o 5 1 3 1 17120.10 11346.90 1368.23 o 1 3 3 -3 810.50 873.58 29.24 o 1 3 3 -2 5.45 34.73 5.65 o 1 3 3 -1 1441.79 1334.53 23.25 o 1 3 3 0 359407.00 365358.00 1049.50 o 1 3 3 1 665.58 671.69 30.62 o 1 3 3 2 8161.14 8472.27 117.25 o 1 3 3 3 57.23 571.76 57.65 o 3 3 3 -3 1786.40 2001.72 47.35 o 3 3 3 -2 9.49 42.77 14.88 < 3 3 3 -1 11.79 114.80 21.56 o 3 3 3 0 153031.00 158467.00 824.67 o 3 3 3 1 4504.00 4549.43 121.36 o 3 3 3 2 17534.60 16770.50 291.47 o 3 3 3 3 1681.74 2110.79 116.48 o 5 3 3 -3 1883.79 2193.38 84.65 o 5 3 3 -2 11.09 83.32 30.62 < 5 3 3 -1 6.64 102.31 43.63 < 5 3 3 0 33487.60 32046.10 444.17 o 1 5 3 -3 2476.02 2323.23 52.14 o 1 5 3 -2 2959.44 2891.38 50.59 o 1 5 3 -1 197.14 213.67 15.91 o 1 5 3 0 2345.36 2464.74 55.05 o 1 5 3 1 958.48 973.73 43.96 o 1 5 3 2 16999.90 18619.20 223.02 o 1 5 3 3 5533.82 5723.73 127.99 o 3 5 3 -3 1179.12 1018.62 37.80 o 3 5 3 -2 1515.64 1812.41 62.93 o 3 5 3 -1 10434.90 11685.20 179.88 o 3 5 3 0 8435.84 8719.93 164.47 o 3 5 3 1 12059.70 13382.80 240.87 o 3 5 3 2 15442.10 15738.90 305.12 o 3 5 3 3 1214.23 1101.24 160.11 o 5 5 3 -3 2.16 51.84 25.66 < 5 5 3 -2 750.96 947.68 66.54 o 5 5 3 -1 5256.98 5515.51 185.47 o 5 5 3 0 4701.40 3311.73 395.78 o 1 7 3 -3 1.66 67.07 21.90 o 1 7 3 -2 6029.28 5754.45 98.40 o 1 7 3 -1 69316.20 66869.00 404.50 o 1 7 3 0 1104.26 1038.56 48.23 o 1 7 3 1 66082.70 67049.30 502.62 o 1 7 3 2 896.06 1020.00 62.95 o 1 7 3 3 1539.29 1686.26 90.14 o 3 7 3 -3 76.57 52.86 19.33 < 3 7 3 -2 5385.92 5227.83 126.63 o 3 7 3 -1 19308.00 22276.00 293.49 o 3 7 3 0 278.20 296.65 37.64 o 3 7 3 1 51613.10 62890.40 645.07 o 3 7 3 2 1361.87 1452.04 143.85 o 5 7 3 -3 4.62 16.25 26.35 < 5 7 3 -2 4431.29 4951.92 180.02 o 5 7 3 -1 4561.07 5076.33 301.41 o 1 9 3 -3 605.00 519.53 54.74 o 1 9 3 -2 286.73 288.26 32.50 o 1 9 3 -1 28.22 106.59 26.35 o 1 9 3 0 29246.70 27667.00 373.17 o 1 9 3 1 2761.29 2977.32 126.03 o 1 9 3 2 17.60 74.42 41.06 < 1 9 3 3 2253.50 2931.52 147.08 o 3 9 3 -3 1966.47 1503.13 84.14 o 3 9 3 -2 3140.42 3309.20 136.79 o 3 9 3 -1 14.23 90.16 41.06 < 3 9 3 0 21923.80 27453.50 441.06 o 3 9 3 1 3640.14 4105.15 442.35 o 5 9 3 -3 2180.49 2685.12 147.94 o 5 9 3 -2 2057.86 2426.27 344.29 o 1 11 3 -3 3312.24 3087.85 141.24 o 1 11 3 -2 8246.23 7434.37 207.43 o 1 11 3 -1 17.62 62.96 33.87 < 1 11 3 0 357.47 415.37 58.85 o 1 11 3 1 1061.86 1232.64 121.28 o 1 11 3 2 7993.41 8827.47 533.14 o 3 11 3 -3 1887.30 1716.34 118.01 o 3 11 3 -2 1468.14 1332.97 147.61 o 3 11 3 -1 0.96 -75.62 80.92 < 0 0 4 0 4858.69 4951.16 82.36 o 0 0 4 2 2182.58 2197.67 48.37 o 2 0 4 -2 300.92 256.41 13.17 o 2 0 4 0 1497.43 1560.48 56.94 o 2 0 4 2 1118.28 1108.68 81.24 o 4 0 4 -2 257.03 197.76 39.35 o 4 0 4 0 20.24 102.65 48.76 < 4 0 4 2 1088.54 1082.10 155.32 o 0 2 4 0 3985.17 4379.30 52.75 o 0 2 4 1 1101.08 1089.55 22.40 o 0 2 4 2 39.70 48.93 9.41 o 0 2 4 3 167.72 201.53 17.11 o 2 2 4 -3 168.77 190.23 8.38 o 2 2 4 -2 111.27 155.68 10.78 o 2 2 4 -1 336.39 384.20 18.30 o 2 2 4 0 2385.80 2758.78 57.78 o 2 2 4 1 136.08 198.11 24.81 o 2 2 4 2 6801.77 6578.15 132.39 o 2 2 4 3 119.24 142.00 32.33 o 4 2 4 -3 73.52 68.77 16.77 o 4 2 4 -2 32.72 89.99 23.10 o 4 2 4 -1 316.39 442.40 39.35 o 4 2 4 0 1448.38 1138.43 66.88 o 4 2 4 1 177.85 156.54 40.89 o 4 2 4 2 443.03 265.51 69.11 o 0 4 4 0 34334.70 31817.90 213.59 o 0 4 4 1 119.53 132.93 12.49 o 0 4 4 2 1219.04 1150.09 40.53 o 0 4 4 3 517.95 594.26 38.49 o 2 4 4 -3 35.86 81.61 10.44 o 2 4 4 -2 23.71 37.47 12.15 o 2 4 4 -1 1659.15 1504.75 47.88 o 2 4 4 0 5933.64 5899.94 115.12 o 2 4 4 1 296.07 304.85 29.42 o 2 4 4 2 1608.60 1586.46 75.59 o 2 4 4 3 36.93 43.28 37.13 < 4 4 4 -3 5.17 18.31 21.21 < 4 4 4 -2 14.89 75.11 25.15 < 4 4 4 -1 114.61 115.31 29.77 o 4 4 4 0 2986.66 3258.48 122.43 o 4 4 4 1 1823.84 1594.56 95.27 o 0 6 4 0 87.01 178.10 22.24 o 0 6 4 1 5675.12 5355.66 93.27 o 0 6 4 2 1015.03 1042.33 43.96 o 0 6 4 3 340.87 354.80 34.39 o 2 6 4 -3 10.77 29.77 12.49 < 2 6 4 -2 17.48 43.63 18.48 < 2 6 4 -1 37.88 37.64 18.82 < 2 6 4 0 4011.95 4391.26 103.58 o 2 6 4 1 6787.05 7264.12 155.99 o 2 6 4 2 596.52 776.13 58.33 o 2 6 4 3 372.46 499.37 56.97 o 4 6 4 -3 43.12 45.34 28.23 < 4 6 4 -2 25.31 79.04 25.66 o 4 6 4 -1 52.45 81.78 32.33 < 4 6 4 0 2137.66 2180.24 114.42 o 4 6 4 1 582.02 646.82 158.41 o 0 8 4 0 7408.64 6930.18 189.79 o 0 8 4 1 3911.03 3736.79 97.27 o 0 8 4 2 117.38 147.64 28.74 o 0 8 4 3 137.80 97.00 27.89 o 2 8 4 -3 169.87 257.99 26.35 o 2 8 4 -2 280.09 283.30 29.94 o 2 8 4 -1 2.43 83.15 26.52 o 2 8 4 0 3417.45 3432.90 117.80 o 2 8 4 1 5150.34 5929.88 169.57 o 2 8 4 2 66.72 54.23 37.81 < 2 8 4 3 161.69 291.18 106.24 < 4 8 4 -3 46.26 86.57 30.97 < 4 8 4 -2 8.93 12.66 34.73 < 4 8 4 -1 127.18 307.95 52.52 o 4 8 4 0 4855.53 4554.36 347.05 o 0 10 4 0 17827.40 15638.50 405.45 o 0 10 4 1 3.85 62.62 29.77 < 0 10 4 2 405.13 450.27 53.89 o 0 10 4 3 149.30 181.18 51.15 o 2 10 4 -3 50.55 93.75 30.80 o 2 10 4 -2 274.78 260.21 42.43 o 2 10 4 -1 1430.28 1424.81 91.17 o 2 10 4 0 14354.50 15196.80 361.02 o 2 10 4 1 50.93 84.52 55.60 < 4 10 4 -3 9.21 79.21 46.88 < 4 10 4 -2 71.36 91.87 80.92 < 0 12 4 0 22.35 8.55 74.76 < 0 12 4 1 980.45 942.88 355.63 < 2 12 4 -3 41.12 86.40 71.86 < 2 12 4 -2 23.76 -18.48 99.91 < 1 1 5 -3 953.08 1064.55 27.02 o 1 1 5 -2 780.10 733.84 21.38 o 1 1 5 -1 100.06 176.04 14.20 o 1 1 5 0 190982.00 191110.00 621.24 o 1 1 5 1 341.14 432.11 18.82 o 1 1 5 2 376.86 379.77 23.26 o 1 1 5 3 3106.25 3146.74 86.33 o 3 1 5 -3 19.62 135.33 13.86 o 3 1 5 -2 530.73 498.96 22.41 o 3 1 5 -1 2651.54 3142.32 72.66 o 3 1 5 0 95365.00 97629.70 576.95 o 3 1 5 1 8730.57 8965.82 170.61 o 3 1 5 2 985.95 1014.19 69.11 o 3 1 5 3 23.78 342.00 61.25 o 5 1 5 -3 382.57 593.78 53.37 o 5 1 5 -2 79.29 103.33 27.54 o 5 1 5 -1 1517.11 1713.48 89.97 o 5 1 5 0 27692.50 24634.30 410.68 o 1 3 5 -3 10.01 22.07 11.63 < 1 3 5 -2 5571.18 5110.44 54.97 o 1 3 5 -1 25491.00 23661.00 135.82 o 1 3 5 0 204.63 265.16 17.45 o 1 3 5 1 392.73 445.79 26.69 o 1 3 5 2 1376.97 1334.83 45.15 o 1 3 5 3 548.38 513.02 35.75 o 3 3 5 -3 250.40 166.28 16.94 o 3 3 5 -2 5954.41 5509.70 92.22 o 3 3 5 -1 14552.50 13206.80 146.75 o 3 3 5 0 1242.56 1406.96 57.81 o 3 3 5 1 2421.36 2543.36 96.62 o 3 3 5 2 2293.26 2516.87 120.74 o 3 3 5 3 748.21 679.13 71.33 o 5 3 5 -3 376.59 365.24 34.04 o 5 3 5 -2 4177.52 3728.44 117.96 o 5 3 5 -1 4494.51 3846.68 147.36 o 5 3 5 0 5627.62 5399.03 276.58 o 1 5 5 -3 385.08 412.95 22.92 o 1 5 5 -2 622.54 626.91 25.49 o 1 5 5 -1 13007.80 11829.10 107.54 o 1 5 5 0 14658.30 13822.20 138.70 o 1 5 5 1 64909.30 66165.30 430.69 o 1 5 5 2 1451.18 1601.00 64.31 o 1 5 5 3 8.61 99.06 30.62 o 3 5 5 -3 142.42 71.34 15.57 o 3 5 5 -2 3844.08 4090.18 97.08 o 3 5 5 -1 3110.23 3542.97 93.69 o 3 5 5 0 21204.10 21968.40 266.12 o 3 5 5 1 37045.90 37998.50 409.44 o 3 5 5 2 558.47 550.33 59.19 o 3 5 5 3 1916.35 1735.33 490.87 o 5 5 5 -3 1078.83 1005.09 58.16 o 5 5 5 -2 3005.34 2980.98 114.57 o 5 5 5 -1 701.90 748.41 68.94 o 1 7 5 -3 3446.86 3461.71 96.59 o 1 7 5 -2 4439.84 4188.63 89.39 o 1 7 5 -1 739.26 883.85 43.62 o 1 7 5 0 78583.80 73887.40 523.26 o 1 7 5 1 374.66 466.51 44.31 o 1 7 5 2 105.82 209.23 40.55 o 1 7 5 3 597.55 736.79 58.85 o 3 7 5 -3 2669.25 2589.10 88.57 o 3 7 5 -2 1007.56 796.58 54.57 o 3 7 5 -1 191.41 209.91 35.58 o 3 7 5 0 20588.70 23626.30 326.29 o 3 7 5 1 117.68 167.83 49.27 o 3 7 5 2 661.64 580.95 132.07 o 5 7 5 -3 1625.41 1605.19 92.53 o 5 7 5 -2 428.50 447.70 62.27 o 5 7 5 -1 662.82 450.77 134.29 o 1 9 5 -3 113.05 90.16 37.12 < 1 9 5 -2 1964.24 2140.72 102.44 o 1 9 5 -1 4698.45 4179.34 143.93 o 1 9 5 0 5962.73 5910.10 171.42 o 1 9 5 1 1800.37 1876.74 94.07 o 1 9 5 2 9749.87 11325.80 292.77 o 1 9 5 3 906.72 1065.20 101.95 o 3 9 5 -3 232.56 150.89 34.39 o 3 9 5 -2 1854.63 2221.36 112.20 o 3 9 5 -1 10273.30 11878.50 301.81 o 3 9 5 0 180.29 336.52 89.48 o 3 9 5 1 31.23 151.07 159.79 < 5 9 5 -3 13.44 22.24 60.22 < 1 11 5 -3 456.56 351.21 76.81 o 1 11 5 -2 1781.99 1751.94 144.53 o 1 11 5 -1 15614.80 13583.50 401.42 o 1 11 5 0 129.57 265.52 74.25 o 1 11 5 1 22775.60 21279.50 776.95 o 3 11 5 -3 99.58 67.75 43.11 < 3 11 5 -2 1397.37 1278.08 208.00 o 0 0 6 0 349354.00 345332.00 2162.38 o 0 0 6 2 18.60 55.26 13.00 o 2 0 6 -2 18.69 45.00 14.88 o 2 0 6 0 181329.00 189125.00 978.85 o 2 0 6 2 18244.20 18594.10 339.29 o 4 0 6 -2 63.98 260.73 39.18 o 4 0 6 0 45249.40 46738.50 639.12 o 0 2 6 0 9085.36 8519.90 114.21 o 0 2 6 1 20212.10 19680.50 141.25 o 0 2 6 2 2603.81 2467.10 49.40 o 0 2 6 3 1658.26 1560.91 44.46 o 2 2 6 -3 1374.03 1210.63 28.56 o 2 2 6 -2 3541.59 3581.39 56.90 o 2 2 6 -1 225.49 210.76 16.08 o 2 2 6 0 930.55 1150.42 38.48 o 2 2 6 1 42333.10 42302.50 313.91 o 2 2 6 2 19239.10 18318.90 232.59 o 2 2 6 3 3372.59 2944.79 114.39 o 4 2 6 -3 4.77 31.65 16.77 < 4 2 6 -2 2613.29 2875.37 80.36 o 4 2 6 -1 1982.89 1668.78 71.48 o 4 2 6 0 3002.67 2318.50 108.24 o 4 2 6 1 18244.20 17551.70 331.44 o 4 2 6 2 5991.43 5097.50 482.54 o 0 4 6 0 182.96 161.32 16.77 o 0 4 6 1 49305.50 46496.60 245.50 o 0 4 6 2 4569.58 4446.80 84.58 o 0 4 6 3 48.23 111.38 24.29 o 2 4 6 -3 200.56 166.63 13.34 o 2 4 6 -2 3436.48 3147.30 63.58 o 2 4 6 -1 6310.60 6947.84 110.84 o 2 4 6 0 1734.00 1729.45 60.88 o 2 4 6 1 57173.00 57405.60 421.51 o 2 4 6 2 221.45 221.20 33.36 o 2 4 6 3 2024.05 1868.80 88.25 o 4 4 6 -3 0.82 58.51 25.49 < 4 4 6 -2 4931.16 4488.70 109.38 o 4 4 6 -1 561.72 883.39 54.40 o 4 4 6 0 1431.51 1584.72 88.26 o 4 4 6 1 19795.90 20491.50 407.46 o 0 6 6 0 110776.00 107187.00 719.20 o 0 6 6 1 1713.81 1597.46 54.73 o 0 6 6 2 1765.14 1736.00 63.28 o 0 6 6 3 102.67 274.59 43.45 o 2 6 6 -3 1153.22 1334.95 51.31 o 2 6 6 -2 301.92 279.36 25.49 o 2 6 6 -1 428.47 469.93 34.21 o 2 6 6 0 93207.90 98151.90 615.82 o 2 6 6 1 12.08 63.81 27.89 < 2 6 6 2 2199.62 2321.60 105.01 o 2 6 6 3 1457.97 1781.10 108.61 o 4 6 6 -3 1689.59 1962.36 78.33 o 4 6 6 -2 187.91 245.50 33.36 o 4 6 6 -1 557.13 834.82 66.55 o 4 6 6 0 25561.70 27498.50 421.72 o 4 6 6 1 1939.49 1971.36 514.47 o 0 8 6 0 3275.00 3427.42 146.19 o 0 8 6 1 467.05 444.10 41.23 o 0 8 6 2 6929.96 6876.71 154.63 o 0 8 6 3 3063.50 3408.24 130.64 o 2 8 6 -3 1252.01 1208.77 64.65 o 2 8 6 -2 526.44 512.35 42.60 o 2 8 6 -1 15.00 53.21 27.72 < 2 8 6 0 825.48 745.14 61.41 o 2 8 6 1 2862.62 3434.80 147.06 o 2 8 6 2 5471.10 5993.46 209.06 o 2 8 6 3 862.41 817.68 294.40 < 4 8 6 -3 556.90 553.41 54.57 o 4 8 6 -2 113.01 151.92 41.23 o 4 8 6 -1 1195.64 1701.30 125.21 o 0 10 6 0 305.81 356.01 76.47 o 0 10 6 1 19202.30 17878.90 359.02 o 0 10 6 2 11.74 111.21 47.56 < 0 10 6 3 547.31 447.01 114.45 o 2 10 6 -3 9.09 22.75 33.19 < 2 10 6 -2 612.33 622.86 72.19 o 2 10 6 -1 18938.00 18222.80 370.31 o 2 10 6 0 51.82 134.30 88.96 < 2 10 6 1 14678.70 16193.20 999.49 o 4 10 6 -3 70.84 110.52 62.10 < 4 10 6 -2 500.80 505.52 215.89 < 1 1 7 -3 2.19 17.62 10.27 < 1 1 7 -2 130.57 158.93 16.25 o 1 1 7 -1 248.43 270.29 18.13 o 1 1 7 0 1423.21 1570.67 41.04 o 1 1 7 1 7728.67 7802.30 89.10 o 1 1 7 2 558.59 628.14 31.99 o 1 1 7 3 128.32 216.25 27.37 o 3 1 7 -3 69.90 54.92 13.17 o 3 1 7 -2 104.67 127.63 13.34 o 3 1 7 -1 22.64 36.78 17.11 < 3 1 7 0 2402.16 2403.02 81.39 o 3 1 7 1 52.73 91.87 33.19 < 3 1 7 2 441.48 477.12 56.97 o 3 1 7 3 1713.63 1665.24 168.65 o 5 1 7 -3 86.32 100.43 27.72 o 5 1 7 -2 41.64 126.77 37.64 o 5 1 7 -1 0.52 113.09 44.48 < 5 1 7 0 1926.59 1666.73 261.68 o 1 3 7 -3 3.79 33.53 15.23 < 1 3 7 -2 84.40 92.55 14.37 o 1 3 7 -1 5.35 47.73 12.83 o 1 3 7 0 18272.60 18177.20 163.53 o 1 3 7 1 7061.88 6896.36 103.82 o 1 3 7 2 909.41 946.93 45.16 o 1 3 7 3 491.03 477.28 40.20 o 3 3 7 -3 0.99 25.32 18.14 < 3 3 7 -2 211.79 247.03 21.38 o 3 3 7 -1 12.30 130.54 23.95 o 3 3 7 0 5796.99 6097.17 145.42 o 3 3 7 1 66.87 91.36 27.89 o 3 3 7 2 395.50 426.32 55.09 o 3 3 7 3 776.59 709.92 99.39 o 5 3 7 -3 6.12 13.17 28.06 < 5 3 7 -2 25.28 43.46 31.14 < 5 3 7 -1 12.51 22.93 38.67 < 5 3 7 0 3075.59 3047.50 329.02 o 1 5 7 -3 170.44 230.44 24.81 o 1 5 7 -2 212.00 212.31 18.48 o 1 5 7 -1 25.41 102.99 14.88 o 1 5 7 0 1283.13 1339.01 53.19 o 1 5 7 1 2360.38 2555.18 74.90 o 1 5 7 2 1327.45 1388.66 63.97 o 1 5 7 3 461.93 464.80 45.50 o 3 5 7 -3 289.49 406.64 30.96 o 3 5 7 -2 38.03 36.78 22.07 < 3 5 7 -1 399.40 486.70 38.32 o 3 5 7 0 5053.96 4963.04 138.45 o 3 5 7 1 6.54 14.54 29.08 < 3 5 7 2 1728.18 1643.00 110.66 o 5 5 7 -3 222.63 236.09 38.49 o 5 5 7 -2 13.33 72.54 33.53 < 5 5 7 -1 344.62 368.50 72.37 o 1 7 7 -3 3.69 9.41 20.87 < 1 7 7 -2 1035.90 852.68 50.97 o 1 7 7 -1 4133.74 4257.14 111.28 o 1 7 7 0 11605.60 10878.30 187.59 o 1 7 7 1 481.48 494.22 48.93 o 1 7 7 2 272.99 369.87 49.78 o 1 7 7 3 463.46 553.93 59.19 o 3 7 7 -3 82.98 107.95 30.97 o 3 7 7 -2 345.98 273.21 40.03 o 3 7 7 -1 1188.15 1239.77 80.05 o 3 7 7 0 2422.31 2653.67 124.50 o 3 7 7 1 1066.82 1292.16 99.73 o 5 7 7 -3 46.18 42.09 36.95 < 5 7 7 -2 273.62 244.13 53.55 o 1 9 7 -3 88.71 131.22 34.22 o 1 9 7 -2 17.33 31.14 32.68 < 1 9 7 -1 41.35 90.33 34.56 < 1 9 7 0 737.45 628.15 62.27 o 1 9 7 1 1.87 72.37 41.92 < 1 9 7 2 358.25 449.93 64.15 o 1 9 7 3 169.23 281.94 91.87 o 3 9 7 -3 26.09 15.74 40.38 < 3 9 7 -2 539.40 603.54 72.36 o 3 9 7 -1 695.97 615.16 86.39 o 3 9 7 0 3267.39 3548.10 287.28 o 5 9 7 -3 40.77 58.17 127.97 < 1 11 7 -3 344.41 234.55 151.74 < 1 11 7 0 2870.60 2228.11 427.19 o 3 11 7 -3 64.43 52.86 110.52 < 0 0 8 0 3690.62 3861.08 113.64 o 0 0 8 2 6536.58 6395.25 126.71 o 2 0 8 -2 7610.78 7005.68 135.35 o 2 0 8 0 115.88 216.07 30.79 o 2 0 8 2 110.51 228.74 51.84 o 4 0 8 -2 8646.98 8115.87 184.77 o 4 0 8 0 5717.76 6360.39 278.94 o 0 2 8 0 79714.20 76497.50 542.50 o 0 2 8 1 11902.90 11466.00 117.46 o 0 2 8 2 487.45 469.05 26.69 o 0 2 8 3 1175.97 1282.77 50.28 o 2 2 8 -3 26.11 210.95 26.00 o 2 2 8 -2 415.07 439.29 24.80 o 2 2 8 -1 1095.16 1159.62 43.10 o 2 2 8 0 95150.80 96347.40 528.83 o 2 2 8 1 27609.40 27752.70 285.72 o 2 2 8 2 603.51 582.48 45.67 o 2 2 8 3 614.45 585.56 61.76 o 4 2 8 -3 851.54 937.36 47.38 o 4 2 8 -2 889.98 1029.57 57.13 o 4 2 8 -1 67.68 115.65 28.06 o 4 2 8 0 40178.00 37141.30 444.70 o 4 2 8 1 22573.70 21309.10 567.54 o 0 4 8 0 197713.00 188963.00 1023.13 o 0 4 8 1 751.22 789.58 34.89 o 0 4 8 2 1396.93 1402.78 53.19 o 0 4 8 3 3600.11 3772.19 104.79 o 2 4 8 -3 2289.41 2390.54 61.73 o 2 4 8 -2 83.90 104.19 20.87 o 2 4 8 -1 709.89 849.30 44.82 o 2 4 8 0 96215.70 99987.20 605.25 o 2 4 8 1 16.79 60.39 28.91 < 2 4 8 2 1623.17 1604.32 84.32 o 2 4 8 3 820.15 900.82 75.27 o 4 4 8 -3 984.61 1002.18 61.06 o 4 4 8 -2 10.84 49.10 29.08 < 4 4 8 -1 1851.91 2012.68 96.80 o 4 4 8 0 32885.90 31690.20 445.36 o 4 4 8 1 890.77 969.92 140.10 o 0 6 8 0 7080.15 6989.27 169.97 o 0 6 8 1 8248.93 7997.59 150.81 o 0 6 8 2 3161.79 3144.77 99.85 o 0 6 8 3 2.37 46.36 30.80 < 2 6 8 -3 158.64 181.17 23.10 o 2 6 8 -2 4950.86 5020.29 121.52 o 2 6 8 -1 25059.50 24452.20 287.35 o 2 6 8 0 170.15 138.06 33.70 o 2 6 8 1 1252.12 1449.29 80.73 o 2 6 8 2 11249.30 12067.20 256.84 o 2 6 8 3 455.61 465.66 67.75 o 4 6 8 -3 13.18 53.72 30.97 < 4 6 8 -2 3200.81 3517.45 126.02 o 4 6 8 -1 11797.50 11563.70 253.58 o 4 6 8 0 334.56 339.07 78.52 o 0 8 8 0 1902.24 1931.41 134.77 o 0 8 8 1 37434.90 34757.70 459.72 o 0 8 8 2 2203.10 2263.63 110.14 o 0 8 8 3 192.65 270.31 48.07 o 2 8 8 -3 28.71 15.91 30.97 < 2 8 8 -2 2155.44 2078.24 105.18 o 2 8 8 -1 7807.42 7522.68 195.80 o 2 8 8 0 1042.09 1161.13 83.99 o 2 8 8 1 47001.50 52793.50 598.24 o 2 8 8 2 159.40 105.56 58.17 < 4 8 8 -3 412.21 381.67 50.81 o 4 8 8 -2 3842.72 4583.36 181.58 o 4 8 8 -1 2348.62 2604.19 289.37 o 0 10 8 0 20471.30 18271.20 739.12 o 0 10 8 1 1358.39 1447.25 185.07 o 0 10 8 2 1121.05 1262.91 196.88 o 0 10 8 3 1239.75 1657.68 571.32 < 2 10 8 -3 3003.49 2760.88 200.25 o 2 10 8 -2 3724.49 3755.55 328.12 o 2 10 8 -1 62.69 122.84 85.54 < 1 1 9 -3 661.10 596.13 29.93 o 1 1 9 -2 1955.63 1841.08 46.34 o 1 1 9 -1 2725.19 2784.20 58.30 o 1 1 9 0 9232.12 8874.46 117.93 o 1 1 9 1 45752.50 46211.60 305.02 o 1 1 9 2 4199.58 4233.05 97.09 o 1 1 9 3 97.03 166.63 28.74 o 3 1 9 -3 222.18 286.89 22.41 o 3 1 9 -2 2308.93 2434.58 69.25 o 3 1 9 -1 55.56 94.10 21.56 o 3 1 9 0 478.82 487.55 43.79 o 3 1 9 1 19190.50 18966.10 321.76 o 3 1 9 2 5465.33 5349.11 199.31 o 3 1 9 3 4153.52 3272.36 615.01 o 5 1 9 -3 17.30 45.51 27.89 < 5 1 9 -2 1711.53 1691.03 98.86 o 5 1 9 -1 190.22 113.25 50.98 < 1 3 9 -3 186.37 360.63 33.87 o 1 3 9 -2 98.63 61.76 15.74 o 1 3 9 -1 709.28 706.97 34.72 o 1 3 9 0 112308.00 113352.00 595.66 o 1 3 9 1 6441.19 6382.52 123.18 o 1 3 9 2 2578.83 2686.67 88.40 o 1 3 9 3 13.61 154.49 40.03 o 3 3 9 -3 179.65 387.15 37.29 o 3 3 9 -2 7.59 32.51 22.93 < 3 3 9 -1 1317.19 1523.62 65.51 o 3 3 9 0 34966.00 34664.50 387.40 o 3 3 9 1 19.27 -6.16 39.01 < 3 3 9 2 7096.04 6637.43 258.05 o 5 3 9 -3 224.77 250.46 39.52 o 5 3 9 -2 20.28 51.67 38.84 < 5 3 9 -1 343.83 606.12 101.28 o 1 5 9 -3 792.73 773.18 49.26 o 1 5 9 -2 419.60 381.66 29.94 o 1 5 9 -1 5947.48 5820.56 114.31 o 1 5 9 0 399.45 396.71 37.12 o 1 5 9 1 9113.56 9018.38 166.51 o 1 5 9 2 5725.11 5902.87 140.48 o 1 5 9 3 2536.90 2561.74 104.15 o 3 5 9 -3 439.44 383.71 36.10 o 3 5 9 -2 251.18 322.99 35.58 o 3 5 9 -1 22.92 108.47 30.28 o 3 5 9 0 1031.49 840.05 64.15 o 3 5 9 1 17681.40 17922.70 327.56 o 3 5 9 2 6547.27 5940.89 608.46 o 5 5 9 -3 1.66 38.67 26.69 < 5 5 9 -2 126.98 193.84 44.99 o 5 5 9 -1 210.05 321.97 224.80 < 1 7 9 -3 46.88 80.07 35.24 < 1 7 9 -2 271.95 385.09 47.22 o 1 7 9 -1 12958.70 12873.30 241.34 o 1 7 9 0 222.64 278.35 40.55 o 1 7 9 1 12146.80 12298.70 224.85 o 1 7 9 2 155.57 236.78 40.89 o 1 7 9 3 1012.81 1038.15 79.71 o 3 7 9 -3 187.80 137.04 30.62 o 3 7 9 -2 228.07 177.24 37.47 o 3 7 9 -1 2162.03 2428.72 116.98 o 3 7 9 0 139.07 239.86 54.92 o 3 7 9 1 12669.90 13751.10 487.18 o 5 7 9 -3 58.01 29.77 35.76 < 5 7 9 -2 515.51 416.73 116.84 o 1 9 9 -3 5.69 87.42 50.98 < 1 9 9 -2 665.28 717.97 74.07 o 1 9 9 -1 443.05 481.57 63.13 o 1 9 9 0 25563.60 24625.70 440.12 o 1 9 9 1 141.87 160.47 53.38 o 1 9 9 2 781.62 837.53 137.71 o 3 9 9 -3 151.03 211.97 55.26 o 3 9 9 -2 51.00 55.26 54.58 < 3 9 9 -1 12.48 -10.78 56.97 < 0 0 10 0 107243.00 106792.00 832.76 o 0 0 10 2 735.90 794.38 60.21 o 2 0 10 -2 2068.10 2031.30 82.93 o 2 0 10 0 44125.40 46157.20 488.09 o 2 0 10 2 6663.44 7022.00 266.58 o 4 0 10 -2 1047.51 1141.60 84.33 o 4 0 10 0 18363.10 19201.10 504.92 o 0 2 10 0 1464.25 1646.63 73.20 o 0 2 10 1 41.56 69.97 18.82 o 0 2 10 2 148.74 183.57 23.10 o 0 2 10 3 0.97 48.76 19.85 < 2 2 10 -3 139.48 199.65 23.78 o 2 2 10 -2 16.20 33.02 20.70 < 2 2 10 -1 2346.45 2356.84 75.24 o 2 2 10 0 11002.80 11576.10 169.33 o 2 2 10 1 375.15 401.17 40.72 o 2 2 10 2 2981.78 2872.75 114.40 o 2 2 10 3 368.10 262.60 43.97 o 4 2 10 -3 586.04 582.13 40.03 o 4 2 10 -2 13.73 84.52 27.72 o 4 2 10 -1 1621.08 1455.88 86.37 o 4 2 10 0 7136.94 6024.13 196.35 o 0 4 10 0 8907.26 8596.40 197.74 o 0 4 10 1 12874.30 12903.10 179.66 o 0 4 10 2 1663.38 1656.91 65.33 o 0 4 10 3 82.22 121.81 28.74 o 2 4 10 -3 186.51 217.44 26.52 o 2 4 10 -2 1022.95 936.66 50.97 o 2 4 10 -1 3874.94 4110.36 102.74 o 2 4 10 0 1740.68 1601.34 70.29 o 2 4 10 1 11235.50 11437.40 210.70 o 2 4 10 2 277.78 218.64 44.82 o 2 4 10 3 930.00 860.09 94.94 o 4 4 10 -3 21.46 57.31 23.95 < 4 4 10 -2 1066.02 881.44 64.32 o 4 4 10 -1 2013.65 2056.97 109.12 o 4 4 10 0 2928.52 2849.51 189.82 o 0 6 10 0 9438.96 8597.19 270.18 o 0 6 10 1 13.15 97.01 32.68 < 0 6 10 2 156.37 139.94 28.40 o 0 6 10 3 190.48 217.10 39.86 o 2 6 10 -3 59.79 119.42 31.82 o 2 6 10 -2 384.67 419.47 41.06 o 2 6 10 -1 891.60 747.01 55.25 o 2 6 10 0 13970.00 14455.10 278.89 o 2 6 10 1 10.13 111.89 35.41 o 2 6 10 2 135.27 219.50 50.30 o 4 6 10 -3 226.24 196.91 39.35 o 4 6 10 -2 428.03 440.34 52.01 o 4 6 10 -1 421.93 235.91 67.57 o 0 8 10 0 3112.20 2912.61 196.82 o 0 8 10 1 2335.00 1986.06 111.85 o 0 8 10 2 2602.00 2520.74 122.45 o 0 8 10 3 750.86 649.36 70.99 o 2 8 10 -3 78.03 87.77 37.30 < 2 8 10 -2 263.27 274.58 50.47 o 2 8 10 -1 426.11 413.31 55.09 o 2 8 10 0 1031.03 946.98 90.49 o 2 8 10 1 1834.00 1588.43 149.66 o 4 8 10 -3 51.09 36.78 53.55 < 4 8 10 -2 201.25 266.03 59.36 o 1 1 11 -3 1391.07 1609.43 63.11 o 1 1 11 -2 253.08 221.71 20.19 o 1 1 11 -1 1527.22 1554.98 48.91 o 1 1 11 0 97937.80 98701.20 570.85 o 1 1 11 1 1224.27 1319.42 57.47 o 1 1 11 2 75.73 139.95 26.86 o 1 1 11 3 3041.80 2899.21 117.30 o 3 1 11 -3 284.87 417.77 39.18 o 3 1 11 -2 268.84 266.54 28.91 o 3 1 11 -1 340.98 490.64 39.86 o 3 1 11 0 50439.90 49805.70 524.03 o 3 1 11 1 11075.50 11213.30 269.15 o 3 1 11 2 226.09 248.75 102.65 < 5 1 11 -3 51.24 130.71 40.72 o 5 1 11 -2 279.07 267.57 52.35 o 5 1 11 -1 458.10 534.09 229.92 < 1 3 11 -3 232.73 238.65 28.06 o 1 3 11 -2 6216.02 6140.47 120.80 o 1 3 11 -1 6722.38 6997.49 127.79 o 1 3 11 0 1536.26 1624.12 65.33 o 1 3 11 1 40.44 115.82 25.83 o 1 3 11 2 3394.56 3462.18 115.58 o 1 3 11 3 16.28 53.38 34.05 < 3 3 11 -3 34.38 44.82 21.39 < 3 3 11 -2 6244.69 5992.31 131.75 o 3 3 11 -1 4252.58 4129.94 123.60 o 3 3 11 0 7.63 57.14 34.56 < 3 3 11 1 371.26 479.18 56.11 o 3 3 11 2 4288.46 3683.33 458.39 o 5 3 11 -3 9.84 64.16 34.90 < 5 3 11 -2 4538.00 3806.70 172.33 o 1 5 11 -3 37.82 61.08 27.03 < 1 5 11 -2 151.76 210.09 31.65 o 1 5 11 -1 5276.58 5119.45 129.04 o 1 5 11 0 14306.10 14642.50 236.67 o 1 5 11 1 35059.30 36390.70 408.57 o 1 5 11 2 279.74 369.53 45.16 o 1 5 11 3 6.16 3.76 31.99 < 3 5 11 -3 300.83 319.06 39.18 o 3 5 11 -2 1854.20 2118.38 98.17 o 3 5 11 -1 585.09 737.82 67.23 o 3 5 11 0 17437.30 17567.50 349.59 o 3 5 11 1 24826.00 23100.90 707.50 o 5 5 11 -3 1138.13 1125.20 91.34 o 5 5 11 -2 1850.57 1547.38 192.42 o 1 7 11 -3 3321.08 3496.26 146.88 o 1 7 11 -2 1664.82 1631.19 94.75 o 1 7 11 -1 78.42 66.38 34.39 < 1 7 11 0 60922.60 60496.90 628.15 o 1 7 11 1 1896.85 2028.28 110.49 o 1 7 11 2 3.70 17.11 42.77 < 1 7 11 3 1217.70 1272.47 221.86 o 3 7 11 -3 2403.24 2643.60 126.38 o 3 7 11 -2 265.81 317.86 53.55 o 3 7 11 -1 84.07 59.54 50.47 < 3 7 11 0 19568.30 18181.70 713.21 o 5 7 11 -3 1397.65 1038.10 211.42 o 1 9 11 -3 104.91 17.96 51.50 < 1 9 11 -2 1100.21 1098.87 144.37 o 1 9 11 -1 3327.02 3097.30 241.96 o 1 9 11 0 3546.93 3336.09 310.70 o 1 9 11 1 1199.92 1315.75 245.98 o 3 9 11 -3 169.71 278.01 83.15 o 3 9 11 -2 874.59 1094.46 223.75 o 0 0 12 0 78548.00 79832.80 990.17 o 0 0 12 2 47.72 32.16 26.18 < 2 0 12 -2 16.87 16.77 23.95 < 2 0 12 0 27977.50 28900.50 430.62 o 2 0 12 2 6300.61 5873.72 257.73 o 4 0 12 -2 60.94 194.52 53.04 o 4 0 12 0 7312.78 6142.51 636.76 o 0 2 12 0 8596.68 8442.90 193.85 o 0 2 12 1 10363.10 10306.40 163.39 o 0 2 12 2 222.81 233.52 31.31 o 0 2 12 3 177.66 225.65 30.97 o 2 2 12 -3 342.79 359.25 28.91 o 2 2 12 -2 247.21 321.28 31.65 o 2 2 12 -1 465.89 531.00 40.71 o 2 2 12 0 172.91 235.24 32.16 o 2 2 12 1 16789.50 16998.90 269.04 o 2 2 12 2 6594.73 6257.37 194.15 o 2 2 12 3 707.39 539.89 123.00 o 4 2 12 -3 66.15 101.62 27.72 o 4 2 12 -2 163.25 226.51 38.84 o 4 2 12 -1 37.48 81.26 37.81 < 4 2 12 0 190.26 245.33 171.76 < 0 4 12 0 101.12 195.72 48.76 o 0 4 12 1 9279.31 9298.02 176.43 o 0 4 12 2 490.07 471.81 41.74 o 0 4 12 3 100.30 95.12 27.03 o 2 4 12 -3 440.61 428.88 36.27 o 2 4 12 -2 22.35 89.65 24.12 o 2 4 12 -1 599.22 659.81 49.10 o 2 4 12 0 316.81 442.92 45.68 o 2 4 12 1 12749.60 12799.30 257.29 o 2 4 12 2 14.32 -1.37 59.37 < 4 4 12 -3 216.05 249.26 39.35 o 4 4 12 -2 164.33 179.12 44.14 o 4 4 12 -1 44.34 93.24 51.33 < 0 6 12 0 29700.50 29509.10 567.03 o 0 6 12 1 1046.74 1014.36 77.83 o 0 6 12 2 1183.64 1159.05 78.51 o 0 6 12 3 59.34 234.56 54.23 o 2 6 12 -3 4.04 181.18 42.94 o 2 6 12 -2 4.69 -9.92 26.35 < 2 6 12 -1 23.06 111.38 44.82 < 2 6 12 0 28069.30 29752.00 435.69 o 2 6 12 1 551.79 537.68 89.81 o 4 6 12 -3 2.78 143.37 47.22 o 4 6 12 -2 10.55 -53.38 91.53 < 0 8 12 0 553.53 593.61 126.25 o 0 8 12 1 310.07 334.63 66.72 o 0 8 12 2 2038.04 1802.85 148.46 o 0 8 12 3 478.55 362.50 146.95 < 2 8 12 -3 58.63 44.82 50.47 < 2 8 12 -2 222.51 199.48 50.30 o 2 8 12 -1 80.59 82.46 69.29 < 2 8 12 0 85.64 -59.71 156.54 < 1 1 13 -3 135.80 106.07 23.95 o 1 1 13 -2 356.15 445.65 35.24 o 1 1 13 -1 591.60 622.34 42.42 o 1 1 13 0 7130.24 7179.44 146.77 o 1 1 13 1 12464.50 12541.50 210.14 o 1 1 13 2 304.36 382.36 42.94 o 1 1 13 3 68.26 71.68 30.97 < 3 1 13 -3 36.33 56.12 25.83 < 3 1 13 -2 831.97 922.87 56.45 o 3 1 13 -1 49.73 140.63 35.41 o 3 1 13 0 8573.39 7977.83 211.69 o 3 1 13 1 4399.16 4029.97 425.38 o 5 1 13 -3 266.78 303.66 48.93 o 5 1 13 -2 697.96 608.83 272.00 < 1 3 13 -3 37.58 247.04 47.39 o 1 3 13 -2 166.34 125.40 25.49 o 1 3 13 -1 1122.06 1097.29 59.35 o 1 3 13 0 66515.10 66825.30 535.09 o 1 3 13 1 32.36 58.51 29.08 < 1 3 13 2 1392.21 1378.98 83.64 o 1 3 13 3 173.30 371.42 71.85 o 3 3 13 -3 186.08 395.54 45.34 o 3 3 13 -2 141.59 135.84 33.19 o 3 3 13 -1 256.50 223.43 43.45 o 3 3 13 0 30293.90 29771.90 513.91 o 3 3 13 1 1551.35 1107.18 488.51 < 5 3 13 -3 317.41 441.55 85.71 o 1 5 13 -3 127.64 94.09 37.81 < 1 5 13 -2 253.72 327.44 50.81 o 1 5 13 -1 1506.72 1621.99 100.40 o 1 5 13 0 4138.47 4110.78 157.63 o 1 5 13 1 2449.44 2539.62 121.42 o 1 5 13 2 2535.73 2661.04 147.42 o 1 5 13 3 1021.25 849.48 119.91 o 3 5 13 -3 8.40 24.81 30.62 < 3 5 13 -2 193.58 252.68 42.09 o 3 5 13 -1 3648.84 3769.96 218.87 o 3 5 13 0 6085.10 5511.44 378.61 o 5 5 13 -3 39.07 217.11 137.04 < 1 7 13 -3 2.89 39.86 45.34 < 1 7 13 -2 2634.10 2728.89 171.36 o 1 7 13 -1 15255.40 15494.90 416.46 o 1 7 13 0 818.82 746.01 107.09 o 1 7 13 1 10541.30 9193.64 563.68 o 3 7 13 -3 4.73 -11.98 56.12 < 3 7 13 -2 1905.61 1231.46 213.97 o 0 0 14 0 3665.25 4120.16 230.47 o 0 0 14 2 6248.11 6424.43 221.15 o 2 0 14 -2 5205.58 4952.54 172.64 o 2 0 14 0 5419.48 5690.91 212.47 o 2 0 14 2 1795.44 1654.46 360.04 o 4 0 14 -2 5112.90 4308.26 266.68 o 0 2 14 0 16314.40 15943.70 320.73 o 0 2 14 1 3629.17 3427.96 106.69 o 0 2 14 2 5.01 19.16 24.64 < 0 2 14 3 550.27 537.50 51.66 o 2 2 14 -3 89.21 95.12 24.81 o 2 2 14 -2 597.30 599.59 45.85 o 2 2 14 -1 105.20 122.15 29.43 o 2 2 14 0 23648.70 23989.40 340.01 o 2 2 14 1 10668.20 10769.40 330.16 o 2 2 14 2 647.28 544.68 171.92 o 4 2 14 -3 113.57 190.41 41.06 o 4 2 14 -2 713.03 865.42 117.18 o 0 4 14 0 66475.90 67078.10 863.42 o 0 4 14 1 2204.67 2345.76 101.76 o 0 4 14 2 810.13 705.46 59.87 o 0 4 14 3 2611.22 2499.22 119.37 o 2 4 14 -3 1544.11 1877.01 98.01 o 2 4 14 -2 155.74 138.75 35.07 o 2 4 14 -1 1170.23 1265.79 81.25 o 2 4 14 0 31746.70 31263.90 567.57 o 2 4 14 1 3840.48 4659.54 382.50 o 4 4 14 -3 628.89 635.01 106.92 o 4 4 14 -2 28.98 86.91 125.23 < 0 6 14 0 4890.76 5253.47 343.45 o 0 6 14 1 159.57 111.03 78.01 < 0 6 14 2 1060.49 1083.65 169.18 o 0 6 14 3 26.64 -40.03 79.90 < 2 6 14 -3 188.71 267.74 66.89 o 2 6 14 -2 1521.23 1616.38 153.60 o 2 6 14 -1 3673.62 3742.97 314.79 o 2 6 14 0 460.67 673.86 207.68 o 1 1 15 -3 269.95 321.97 35.07 o 1 1 15 -2 154.00 123.52 27.20 o 1 1 15 -1 1455.26 1518.87 77.65 o 1 1 15 0 351.02 460.19 44.14 o 1 1 15 1 12990.50 13196.10 240.90 o 1 1 15 2 91.78 107.61 44.14 < 3 1 15 -3 350.43 457.46 43.28 o 3 1 15 -2 128.83 173.13 35.24 o 3 1 15 -1 218.68 399.30 87.25 o 1 3 15 -3 50.58 167.49 35.24 o 1 3 15 -2 11.51 10.44 22.58 < 1 3 15 -1 643.56 718.48 53.72 o 1 3 15 0 25262.40 25143.70 360.40 o 1 3 15 1 309.80 257.98 51.32 o 1 3 15 2 935.98 1025.17 126.07 o 3 3 15 -3 131.56 250.29 48.42 o 3 3 15 -2 9.52 50.47 34.73 < 3 3 15 -1 259.21 210.77 78.87 < 1 5 15 -3 2.36 -19.85 64.50 < 1 5 15 -2 168.39 238.32 71.34 o 1 5 15 -1 395.68 408.53 90.50 o 1 5 15 0 161.04 215.56 101.45 < 1 5 15 1 330.49 258.50 94.43 < 3 5 15 -3 22.72 -31.14 81.61 < 3 5 15 -2 277.96 302.98 99.74 o 0 0 16 0 94044.60 96603.00 1427.24 o 0 0 16 2 79.63 96.66 46.19 < 2 0 16 -2 148.04 157.05 40.03 o 2 0 16 0 50631.10 49620.20 2240.46 o 0 2 16 0 2292.83 2171.84 143.66 o 0 2 16 1 218.81 211.45 39.86 o 0 2 16 2 366.61 409.04 63.81 o 0 2 16 3 449.99 200.50 73.90 < 2 2 16 -3 154.68 116.68 34.73 o 2 2 16 -2 836.72 912.45 83.82 o 2 2 16 -1 713.03 732.68 84.34 o 2 2 16 0 7415.00 6872.20 465.86 o 4 2 16 -3 21.71 187.17 155.69 < 0 4 16 0 2707.42 1897.93 295.00 o 0 4 16 1 11150.10 10940.70 1164.15 o 0 4 16 2 1679.45 1859.91 297.10 o 2 4 16 -3 0.42 -39.52 42.94 < 2 4 16 -2 1657.09 1466.18 401.95 o 2 4 16 -1 3528.09 3735.22 524.44 o 1 1 17 -3 620.13 796.84 275.93 < 1 1 17 -2 131.26 94.78 56.46 < 1 1 17 -1 2141.35 2009.94 236.53 o 1 1 17 0 16547.20 15309.90 1186.77 o 3 1 17 -3 239.59 446.00 140.97 o