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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_I _publ_contact_author_name 'Jana,Partha Pratim' _publ_contact_author_address ;CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 ; _publ_contact_author_email Partha.Jana@polymat.lth.se _publ_contact_author_fax +46462224012 _publ_contact_author_phone 0046462224769 loop_ _publ_author_name _publ_author_address 'Jana,Partha Pratim' ;CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 ; 'Lidin, Sven' ;CAS Chemical Centre Lund University Getingevagen 60 Lund Sweden Box 124 ; _publ_section_title ;Structural Impact of Platinum on the Incommensurably Modulated \g-Brass Related Composite Structure Pd~15~Zn~54~ ; _journal_name_full 'Inorganic Chemistry' _journal_volume 51 _journal_page_first 9893 _journal_page_last 9901 _journal_year 2012 _journal_paper_doi https://doi.org/10.1021/ic301326p _chemical_formula_sum 'Nd3.626 Pd2.861 Pt1.139 Zn26.89' _chemical_formula_weight 2807.7 _chemical_absolute_configuration ? _space_group_crystal_system orthorhombic _space_group_ssg_name Fmmm(\a00)0s0 _cell_length_a 4.2652(6) _cell_length_b 9.1319(12) _cell_length_c 12.928(15) _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_volume 503.54(11) _cell_modulation_dimension 1 _cell_subsystems_number 2 _cell_formula_units_Z 1 _cell_measurement_temperature 293.0 _exptl_crystal_type_of_structure comp _exptl_crystal_density_diffrn 9.2561 _exptl_crystal_F_000 1245.0 _exptl_absorpt_coefficient_mu 50.788 _exptl_crystal_size_max 0.06 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.04 _exptl_absorpt_correction_type multi-scan _diffrn_ambient_temperature 293.0 _diffrn_radiation_type 'Mo K\a' _diffrn_source 'x-ray tube' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-cycle diffractometer' _diffrn_measurement_device_type 'Oxford Diffraction CCD' _diffrn_reflns_number 19491 _diffrn_reflns_theta_min 3.0 _diffrn_reflns_theta_max 28.92 _diffrn_reflns_theta_full 20.84 _diffrn_measured_fraction_theta_max 0.89 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.058 _diffrn_reflns_av_unetI/netI 0.0255 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_index_m_1_min -3 _diffrn_reflns_limit_index_m_1_max 3 _reflns_number_total 1156 _reflns_number_gt 848 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0319 _refine_ls_wR_factor_gt 0.0938 _refine_ls_R_factor_all 0.0527 _refine_ls_wR_factor_ref 0.1043 _refine_ls_goodness_of_fit_ref 1.36 _refine_ls_goodness_of_fit_gt 1.45 _refine_ls_number_reflns 1156 _refine_ls_number_parameters 79 _refine_ls_number_constraints 48 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(I)+0.0016I^2^) _refine_ls_shift/su_max 0.0454 _refine_ls_shift/su_mean 0.0074 _refine_diff_density_max 3.14 _refine_diff_density_min -3.03 _refine_ls_extinction_method 'B-C type 1 gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 128.0(16) loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,-x2,x3,-x4 3 -x1,x2,-x3,-x4+1/2 4 x1,-x2,-x3,x4+1/2 5 -x1,-x2,-x3,-x4 6 x1,x2,-x3,x4 7 x1,-x2,x3,x4+1/2 8 -x1,x2,x3,-x4+1/2 9 x1,x2+1/2,x3+1/2,x4 10 -x1,-x2+1/2,x3+1/2,-x4 11 -x1,x2+1/2,-x3+1/2,-x4+1/2 12 x1,-x2+1/2,-x3+1/2,x4+1/2 13 -x1,-x2+1/2,-x3+1/2,-x4 14 x1,x2+1/2,-x3+1/2,x4 15 x1,-x2+1/2,x3+1/2,x4+1/2 16 -x1,x2+1/2,x3+1/2,-x4+1/2 17 x1+1/2,x2,x3+1/2,x4 18 -x1+1/2,-x2,x3+1/2,-x4 19 -x1+1/2,x2,-x3+1/2,-x4+1/2 20 x1+1/2,-x2,-x3+1/2,x4+1/2 21 -x1+1/2,-x2,-x3+1/2,-x4 22 x1+1/2,x2,-x3+1/2,x4 23 x1+1/2,-x2,x3+1/2,x4+1/2 24 -x1+1/2,x2,x3+1/2,-x4+1/2 25 x1+1/2,x2+1/2,x3,x4 26 -x1+1/2,-x2+1/2,x3,-x4 27 -x1+1/2,x2+1/2,-x3,-x4+1/2 28 x1+1/2,-x2+1/2,-x3,x4+1/2 29 -x1+1/2,-x2+1/2,-x3,-x4 30 x1+1/2,x2+1/2,-x3,x4 31 x1+1/2,-x2+1/2,x3,x4+1/2 32 -x1+1/2,x2+1/2,x3,-x4+1/2 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.629 0.0 0.0 loop_ _cell_subsystem_code _cell_subsystem_description _cell_subsystem_matrix_W_1_1 _cell_subsystem_matrix_W_1_2 _cell_subsystem_matrix_W_1_3 _cell_subsystem_matrix_W_1_4 _cell_subsystem_matrix_W_2_1 _cell_subsystem_matrix_W_2_2 _cell_subsystem_matrix_W_2_3 _cell_subsystem_matrix_W_2_4 _cell_subsystem_matrix_W_3_1 _cell_subsystem_matrix_W_3_2 _cell_subsystem_matrix_W_3_3 _cell_subsystem_matrix_W_3_4 _cell_subsystem_matrix_W_4_1 _cell_subsystem_matrix_W_4_2 _cell_subsystem_matrix_W_4_3 _cell_subsystem_matrix_W_4_4 1 '1st subsystem' 1 0 0 0 0 1 0 0 0 0 1 0 0 0 0 1 2 '2nd subsystem' 1 0 0 1 0 1 0 0 0 0 1 0 0 0 0 1 loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Nd -0.1943 3.0179 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Pd -0.9988 1.0072 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Pt -1.7033 8.3905 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Zn 0.2839 1.4301 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_subsystem_code Pd1 Pd 0.5 0.0 0.0 Uani 0.0096(2) 4 0.715(7) d ? ? ? 1 Pt1 Pt 0.5 0.0 0.0 Uani 0.0096(2) 4 0.285(7) d ? ? ? 1 Nd1 Nd 0.5 0.1512(6) 0.17947(5) Uani 0.0136(2) 16 0.227(4) d ? ? ? 1 Zn1 Zn 0.5 0.1512(6) 0.17947(5) Uani 0.0136(2) 16 0.773(4) d ? ? ? 1 Zn2 Zn 0.0 0.0 0.12349(8) Uani 0.0158(3) 8 1.0 d ? ? ? 1 Zn3 Zn 0.75 0.25 0.0 Uani 0.0156(3) 4 1.0 d ? ? ? 2 loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pd1 Pd 0.0106(4) 0.0099(4) 0.0082(4) 0.0 0.0 0.0 Pt1 Pt 0.0106(4) 0.0099(4) 0.0082(4) 0.0 0.0 0.0 Nd1 Nd 0.0156(4) 0.0138(4) 0.0114(4) 0.0 0.0 -0.0033(2) Zn1 Zn 0.0156(4) 0.0138(4) 0.0114(4) 0.0 0.0 -0.0033(2) Zn2 Zn 0.0106(5) 0.0185(6) 0.0183(6) 0.0 0.0 0.0 Zn3 Zn 0.0185(6) 0.0135(5) 0.0147(6) 0.0 0.0 0.0 loop_ _atom_site_Fourier_wave_vector_seq_id _jana_atom_site_Fourier_wave_vector_q1_coeff 1 1.0 2 2.0 3 3.0 loop_ _atom_site_occ_Fourier_id _atom_site_occ_Fourier_atom_site_label _atom_site_occ_Fourier_wave_vector_seq_id Pd1o1 Pd1 1 Pd1o2 Pd1 2 Pd1o3 Pd1 3 Pt1o1 Pt1 1 Pt1o2 Pt1 2 Pt1o3 Pt1 3 Nd1o1 Nd1 1 Nd1o2 Nd1 2 Nd1o3 Nd1 3 Zn1o1 Zn1 1 Zn1o2 Zn1 2 Zn1o3 Zn1 3 loop_ _atom_site_occ_Fourier_param_id _atom_site_occ_Fourier_param_cos _atom_site_occ_Fourier_param_sin Pd1o1 0.0 0.0 Pd1o2 -0.293(5) 0.0 Pd1o3 0.0 0.0 Pt1o1 0.0 0.0 Pt1o2 0.293(5) 0.0 Pt1o3 0.0 0.0 Nd1o1 0.0 -0.381(4) Nd1o2 -0.246(3) 0.0 Nd1o3 0.0 0.103(3) Zn1o1 0.0 0.381(4) Zn1o2 0.246(3) 0.0 Zn1o3 0.0 -0.103(3) loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Pd1x1 Pd1 x 1 Pd1y1 Pd1 y 1 Pd1z1 Pd1 z 1 Pd1x2 Pd1 x 2 Pd1y2 Pd1 y 2 Pd1z2 Pd1 z 2 Pd1x3 Pd1 x 3 Pd1y3 Pd1 y 3 Pd1z3 Pd1 z 3 Pt1x1 Pt1 x 1 Pt1y1 Pt1 y 1 Pt1z1 Pt1 z 1 Pt1x2 Pt1 x 2 Pt1y2 Pt1 y 2 Pt1z2 Pt1 z 2 Pt1x3 Pt1 x 3 Pt1y3 Pt1 y 3 Pt1z3 Pt1 z 3 Nd1x1 Nd1 x 1 Nd1y1 Nd1 y 1 Nd1z1 Nd1 z 1 Nd1x2 Nd1 x 2 Nd1y2 Nd1 y 2 Nd1z2 Nd1 z 2 Nd1x3 Nd1 x 3 Nd1y3 Nd1 y 3 Nd1z3 Nd1 z 3 Zn1x1 Zn1 x 1 Zn1y1 Zn1 y 1 Zn1z1 Zn1 z 1 Zn1x2 Zn1 x 2 Zn1y2 Zn1 y 2 Zn1z2 Zn1 z 2 Zn1x3 Zn1 x 3 Zn1y3 Zn1 y 3 Zn1z3 Zn1 z 3 Zn2x1 Zn2 x 1 Zn2y1 Zn2 y 1 Zn2z1 Zn2 z 1 Zn2x2 Zn2 x 2 Zn2y2 Zn2 y 2 Zn2z2 Zn2 z 2 Zn2x3 Zn2 x 3 Zn2y3 Zn2 y 3 Zn2z3 Zn2 z 3 Zn3x1 Zn3 x 1 Zn3y1 Zn3 y 1 Zn3z1 Zn3 z 1 Zn3x2 Zn3 x 2 Zn3y2 Zn3 y 2 Zn3z2 Zn3 z 2 Zn3x3 Zn3 x 3 Zn3y3 Zn3 y 3 Zn3z3 Zn3 z 3 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Pd1x1 0.0 0.0 Pd1y1 0.0 0.02422(11) Pd1z1 0.0 0.0 Pd1x2 0.0 0.0035(2) Pd1y2 0.0 0.0 Pd1z2 0.0 0.0 Pd1x3 0.0 0.0 Pd1y3 0.0 0.00149(10) Pd1z3 0.0 0.0 Pt1x1 0.0 0.0 Pt1y1 0.0 0.02422(11) Pt1z1 0.0 0.0 Pt1x2 0.0 0.0035(2) Pt1y2 0.0 0.0 Pt1z2 0.0 0.0 Pt1x3 0.0 0.0 Pt1y3 0.0 0.00149(10) Pt1z3 0.0 0.0 Nd1x1 -0.0666(2) 0.0 Nd1y1 0.0 -0.01885(8) Nd1z1 0.0 0.00347(6) Nd1x2 0.0 -0.0138(2) Nd1y2 0.00519(8) 0.0 Nd1z2 -0.00307(6) 0.0 Nd1x3 0.0062(2) 0.0 Nd1y3 0.0 0.00525(8) Nd1z3 0.0 -0.00151(7) Zn1x1 -0.0666(2) 0.0 Zn1y1 0.0 -0.01885(8) Zn1z1 0.0 0.00347(6) Zn1x2 0.0 -0.0138(2) Zn1y2 0.00519(8) 0.0 Zn1z2 -0.00307(6) 0.0 Zn1x3 0.0062(2) 0.0 Zn1y3 0.0 0.00525(8) Zn1z3 0.0 -0.00151(7) Zn2x1 0.0 0.0 Zn2y1 0.0 0.05131(15) Zn2z1 0.0 0.0 Zn2x2 0.0 0.0131(3) Zn2y2 0.0 0.0 Zn2z2 0.00851(10) 0.0 Zn2x3 0.0 0.0 Zn2y3 0.0 0.004(18) Zn2z3 0.0 0.0 Zn3x1 0.0 0.0 Zn3y1 0.0 0.05665(15) Zn3z1 0.0 0.0 Zn3x2 0.0 -0.0388(6) Zn3y2 0.0 0.0 Zn3z2 0.0 0.0 Zn3x3 0.0 0.0 Zn3y3 0.0 0.00178(15) Zn3z3 0.0 0.0 loop_ _atom_site_U_Fourier_id _atom_site_U_Fourier_atom_site_label _atom_site_U_Fourier_tens_elem _atom_site_U_Fourier_wave_vector_seq_id Pd1U111 Pd1 U11 1 Pd1U221 Pd1 U22 1 Pd1U331 Pd1 U33 1 Pd1U121 Pd1 U12 1 Pd1U131 Pd1 U13 1 Pd1U231 Pd1 U23 1 Pd1U112 Pd1 U11 2 Pd1U222 Pd1 U22 2 Pd1U332 Pd1 U33 2 Pd1U122 Pd1 U12 2 Pd1U132 Pd1 U13 2 Pd1U232 Pd1 U23 2 Pd1U113 Pd1 U11 3 Pd1U223 Pd1 U22 3 Pd1U333 Pd1 U33 3 Pd1U123 Pd1 U12 3 Pd1U133 Pd1 U13 3 Pd1U233 Pd1 U23 3 Pt1U111 Pt1 U11 1 Pt1U221 Pt1 U22 1 Pt1U331 Pt1 U33 1 Pt1U121 Pt1 U12 1 Pt1U131 Pt1 U13 1 Pt1U231 Pt1 U23 1 Pt1U112 Pt1 U11 2 Pt1U222 Pt1 U22 2 Pt1U332 Pt1 U33 2 Pt1U122 Pt1 U12 2 Pt1U132 Pt1 U13 2 Pt1U232 Pt1 U23 2 Pt1U113 Pt1 U11 3 Pt1U223 Pt1 U22 3 Pt1U333 Pt1 U33 3 Pt1U123 Pt1 U12 3 Pt1U133 Pt1 U13 3 Pt1U233 Pt1 U23 3 Nd1U111 Nd1 U11 1 Nd1U221 Nd1 U22 1 Nd1U331 Nd1 U33 1 Nd1U121 Nd1 U12 1 Nd1U131 Nd1 U13 1 Nd1U231 Nd1 U23 1 Nd1U112 Nd1 U11 2 Nd1U222 Nd1 U22 2 Nd1U332 Nd1 U33 2 Nd1U122 Nd1 U12 2 Nd1U132 Nd1 U13 2 Nd1U232 Nd1 U23 2 Nd1U113 Nd1 U11 3 Nd1U223 Nd1 U22 3 Nd1U333 Nd1 U33 3 Nd1U123 Nd1 U12 3 Nd1U133 Nd1 U13 3 Nd1U233 Nd1 U23 3 Zn1U111 Zn1 U11 1 Zn1U221 Zn1 U22 1 Zn1U331 Zn1 U33 1 Zn1U121 Zn1 U12 1 Zn1U131 Zn1 U13 1 Zn1U231 Zn1 U23 1 Zn1U112 Zn1 U11 2 Zn1U222 Zn1 U22 2 Zn1U332 Zn1 U33 2 Zn1U122 Zn1 U12 2 Zn1U132 Zn1 U13 2 Zn1U232 Zn1 U23 2 Zn1U113 Zn1 U11 3 Zn1U223 Zn1 U22 3 Zn1U333 Zn1 U33 3 Zn1U123 Zn1 U12 3 Zn1U133 Zn1 U13 3 Zn1U233 Zn1 U23 3 Zn2U111 Zn2 U11 1 Zn2U221 Zn2 U22 1 Zn2U331 Zn2 U33 1 Zn2U121 Zn2 U12 1 Zn2U131 Zn2 U13 1 Zn2U231 Zn2 U23 1 Zn2U112 Zn2 U11 2 Zn2U222 Zn2 U22 2 Zn2U332 Zn2 U33 2 Zn2U122 Zn2 U12 2 Zn2U132 Zn2 U13 2 Zn2U232 Zn2 U23 2 Zn2U113 Zn2 U11 3 Zn2U223 Zn2 U22 3 Zn2U333 Zn2 U33 3 Zn2U123 Zn2 U12 3 Zn2U133 Zn2 U13 3 Zn2U233 Zn2 U23 3 Zn3U111 Zn3 U11 1 Zn3U221 Zn3 U22 1 Zn3U331 Zn3 U33 1 Zn3U121 Zn3 U12 1 Zn3U131 Zn3 U13 1 Zn3U231 Zn3 U23 1 Zn3U112 Zn3 U11 2 Zn3U222 Zn3 U22 2 Zn3U332 Zn3 U33 2 Zn3U122 Zn3 U12 2 Zn3U132 Zn3 U13 2 Zn3U232 Zn3 U23 2 Zn3U113 Zn3 U11 3 Zn3U223 Zn3 U22 3 Zn3U333 Zn3 U33 3 Zn3U123 Zn3 U12 3 Zn3U133 Zn3 U13 3 Zn3U233 Zn3 U23 3 loop_ _atom_site_U_Fourier_param_id _atom_site_U_Fourier_param_cos _atom_site_U_Fourier_param_sin Pd1U111 0.0 0.0 Pd1U221 0.0 0.0 Pd1U331 0.0 0.0 Pd1U121 0.0006(3) 0.0 Pd1U131 0.0 0.0 Pd1U231 0.0 0.0 Pd1U112 -0.0013(6) 0.0 Pd1U222 -0.0004(5) 0.0 Pd1U332 0.0007(5) 0.0 Pd1U122 0.0 0.0 Pd1U132 0.0 0.0 Pd1U232 0.0 0.0 Pd1U113 0.0 0.0 Pd1U223 0.0 0.0 Pd1U333 0.0 0.0 Pd1U123 0.0014(4) 0.0 Pd1U133 0.0 0.0 Pd1U233 0.0 0.0 Pt1U111 0.0 0.0 Pt1U221 0.0 0.0 Pt1U331 0.0 0.0 Pt1U121 0.0006(3) 0.0 Pt1U131 0.0 0.0 Pt1U231 0.0 0.0 Pt1U112 -0.0013(6) 0.0 Pt1U222 -0.0004(5) 0.0 Pt1U332 0.0007(5) 0.0 Pt1U122 0.0 0.0 Pt1U132 0.0 0.0 Pt1U232 0.0 0.0 Pt1U113 0.0 0.0 Pt1U223 0.0 0.0 Pt1U333 0.0 0.0 Pt1U123 0.0014(4) 0.0 Pt1U133 0.0 0.0 Pt1U233 0.0 0.0 Nd1U111 0.0 0.0077(5) Nd1U221 0.0 0.0018(4) Nd1U331 0.0 0.0011(4) Nd1U121 -0.0016(3) 0.0 Nd1U131 0.0028(3) 0.0 Nd1U231 0.0 -0.0021(3) Nd1U112 -0.0013(6) 0.0 Nd1U222 0.0039(4) 0.0 Nd1U332 -0.0007(5) 0.0 Nd1U122 0.0 -0.0005(3) Nd1U132 0.0 0.0013(3) Nd1U232 -0.0006(3) 0.0 Nd1U113 0.0 0.0013(6) Nd1U223 0.0 0.0017(4) Nd1U333 0.0 -0.0015(5) Nd1U123 0.0014(4) 0.0 Nd1U133 0.0005(4) 0.0 Nd1U233 0.0 -0.0006(4) Zn1U111 0.0 0.0077(5) Zn1U221 0.0 0.0018(4) Zn1U331 0.0 0.0011(4) Zn1U121 -0.0016(3) 0.0 Zn1U131 0.0028(3) 0.0 Zn1U231 0.0 -0.0021(3) Zn1U112 -0.0013(6) 0.0 Zn1U222 0.0039(4) 0.0 Zn1U332 -0.0007(5) 0.0 Zn1U122 0.0 -0.0005(3) Zn1U132 0.0 0.0013(3) Zn1U232 -0.0006(3) 0.0 Zn1U113 0.0 0.0013(6) Zn1U223 0.0 0.0017(4) Zn1U333 0.0 -0.0015(5) Zn1U123 0.0014(4) 0.0 Zn1U133 0.0005(4) 0.0 Zn1U233 0.0 -0.0006(4) Zn2U111 0.0 0.0 Zn2U221 0.0 0.0 Zn2U331 0.0 0.0 Zn2U121 0.0052(6) 0.0 Zn2U131 0.0 0.0 Zn2U231 0.0 -0.007(6) Zn2U112 0.0015(7) 0.0 Zn2U222 0.0007(8) 0.0 Zn2U332 -0.0039(8) 0.0 Zn2U122 0.0 0.0 Zn2U132 0.0 0.004(5) Zn2U232 0.0 0.0 Zn2U113 0.0 0.0 Zn2U223 0.0 0.0 Zn2U333 0.0 0.0 Zn2U123 0.0052(7) 0.0 Zn2U133 0.0 0.0 Zn2U233 0.0 0.0044(7) Zn3U111 0.0 0.0 Zn3U221 0.0 0.0 Zn3U331 0.0 0.0 Zn3U121 -0.0099(7) 0.0 Zn3U131 0.0 0.0 Zn3U231 0.0 0.0 Zn3U112 0.0093(9) 0.0 Zn3U222 0.0045(7) 0.0 Zn3U332 -0.0031(7) 0.0 Zn3U122 0.0 0.0 Zn3U132 0.0 0.0 Zn3U232 0.0 0.0 Zn3U113 0.0 0.0 Zn3U223 0.0 0.0 Zn3U333 0.0 0.0 Zn3U123 0.0001(6) 0.0 Zn3U133 0.0 0.0 Zn3U233 0.0 0.0 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_ssg_symmetry_1 _geom_bond_site_ssg_symmetry_2 _geom_bond_distance_av _geom_bond_distance_min _geom_bond_distance_max _geom_bond_publ_flag #Pd1 Pd2 ? ? 2.89(4) 2.56(3) 3.45(5) ? #Pd1 Pd2 ? 25_4455 3.37(8) 2.65(4) 4.32(14) ? #Pd1 Pd2 ? 25_5455 2.61(6) 1.63(3) 3.7(9) ? #Pd1 Pd2 ? 2_6555 2.88(4) 2.56(3) 3.45(5) ? #Pd1 Pd2 ? 26_5555 2.62(6) 1.63(3) 3.7(9) ? #Pd1 Pd2 ? 26_6555 3.39(9) 2.65(4) 4.32(14) ? #Pd1 Pd2 ? 3_6555 2.88(4) 2.56(3) 3.45(5) ? #Pd1 Pd2 ? 27_5455 2.6(6) 1.63(3) 3.7(9) ? #Pd1 Pd2 ? 27_6455 3.37(8) 2.65(4) 4.32(14) ? #Pd1 Pd2 ? 4_5555 2.88(4) 2.56(3) 3.45(5) ? #Pd1 Pd2 ? 28_4555 3.39(9) 2.65(4) 4.32(14) ? #Pd1 Pd2 ? 28_5555 2.61(6) 1.63(3) 3.7(9) ? Pd1 Zn2 ? ? 2.715(9) 2.553(12) 2.888(13) ? Pd1 Zn2 ? 2_6555 2.718(9) 2.553(12) 2.888(13) ? Pd1 Zn2 ? 3_6555 2.715(9) 2.553(12) 2.888(13) ? Pd1 Zn2 ? 4_5555 2.718(9) 2.553(12) 2.888(13) ? Pd1 Zn3 ? 1_4555 2.66(6) 2.62(6) 2.71(6) ? Pd1 Zn3 ? ? 2.66(6) 2.62(6) 2.71(6) ? Pd1 Zn3 ? 3_6555 2.66(6) 2.62(6) 2.71(6) ? Pd1 Zn3 ? 3_7555 2.66(6) 2.62(6) 2.71(6) ? #Pd2 Pd2 ? 1_4555 4.28(16) 1.69(8) 6.9(2) ? #Pd2 Pd2 ? 1_6555 4.32(16) 1.69(8) 6.9(2) ? #Pd2 Pd2 ? 26_5555 1.35(7) 1.01(7) 1.69(7) ? #Pd2 Pd2 ? 26_6555 3.27(13) 0.6(6) 5.9(19) ? #Pd2 Pd2 ? 3_5555 3.28(13) 1.48(9) 5.01(18) ? #Pd2 Pd2 ? 3_6555 1.21(8) 0.22(4) 2.43(10) ? #Pd2 Pd2 ? 3_7555 5.32(19) 2.41(10) 8.2(3) ? #Pd2 Pd2 ? 28_4555 2.31(10) 0.7(6) 3.87(14) ? #Pd2 Pd2 ? 28_5555 2.32(10) 0.7(6) 3.87(14) ? #Pd2 Zn2 ? ? 2.97(3) 2.442(15) 3.63(5) ? #Pd2 Zn2 ? 26_5555 3.05(5) 2.302(9) 4.16(10) ? #Pd2 Zn2 ? 26_6555 3.64(8) 2.65(3) 4.74(12) ? #Pd2 Zn2 ? 3_6555 2.97(3) 2.442(15) 3.63(5) ? #Pd2 Zn2 ? 28_4555 3.05(5) 2.302(9) 4.16(10) ? #Pd2 Zn2 ? 28_5555 3.64(8) 2.65(3) 4.74(12) ? #Pd2 Zn3 ? 1_4555 3.59(5) 2.7(3) 4.46(8) ? #Pd2 Zn3 ? ? 4.1(7) 2.63(4) 5.62(11) ? #Pd2 Zn3 ? 25_4555 2.68(3) 2.18(2) 3.14(5) ? #Pd2 Zn3 ? 3_6555 3.59(5) 2.7(3) 4.46(8) ? #Pd2 Zn3 ? 3_7555 4.1(7) 2.63(4) 5.62(11) ? #Pd2 Zn3 ? 27_6555 2.68(3) 2.18(2) 3.14(5) ? Zn2 Zn2 ? 2_6555 2.766(11) 2.735(15) 2.797(10) ? Zn2 Zn2 ? 26_5555 2.82(5) 2.78(4) 2.89(7) ? Zn2 Zn2 ? 26_6555 2.82(5) 2.78(4) 2.89(7) ? Zn2 Zn2 ? 19_5555 2.81(6) 2.47(4) 3.16(7) ? Zn2 Zn2 ? 19_6555 2.81(6) 2.47(4) 3.16(7) ? Zn2 Zn2 ? 12_5555 2.595(12) 2.562(15) 2.629(10) ? Zn2 Zn3 ? 1_4555 2.7(6) 2.62(6) 2.78(4) ? Zn2 Zn3 ? ? 2.7(6) 2.62(6) 2.78(4) ? Zn2 Zn3 ? 25_4555 3.306(12) 2.543(19) 4.045(19) ? Zn2 Zn3 ? 19_6555 2.988(14) 2.643(17) 3.399(17) ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 0 2 1135.28 1166.46 75.78 o 2 0 0 -2 1456.31 1377.43 77.74 o 2 0 0 0 287423.00 289497.00 3020.83 o 2 0 0 2 31554.20 31325.60 733.09 o 4 0 0 -2 1133.84 1600.97 160.44 o 4 0 0 0 101128.00 100979.00 1664.98 o 4 0 0 2 16059.90 16155.20 716.82 o 0 2 0 0 2265.24 2090.33 43.11 o 0 2 0 1 4989.50 5325.60 61.16 o 0 2 0 2 399.74 468.24 31.22 o 0 2 0 3 711.82 758.82 54.33 o 2 2 0 -3 540.64 517.27 17.10 o 2 2 0 -2 1961.54 2233.62 42.24 o 2 2 0 -1 14238.90 13602.10 161.40 o 2 2 0 0 26843.00 26153.20 307.65 o 2 2 0 1 28974.00 27798.80 343.64 o 2 2 0 2 14532.90 14725.00 295.62 o 2 2 0 3 1960.14 1759.67 128.76 o 4 2 0 -3 245.69 258.11 45.79 o 4 2 0 -2 2170.60 2634.41 106.76 o 4 2 0 -1 11973.10 11659.00 281.45 o 4 2 0 0 17976.30 16575.40 417.78 o 4 2 0 1 12153.00 13185.50 512.10 o 4 2 0 2 3292.90 3226.57 330.52 o 0 4 0 0 1155.60 1196.74 49.46 o 0 4 0 1 116327.00 116646.00 620.95 o 0 4 0 2 6245.14 5980.59 113.39 o 0 4 0 3 74.60 64.07 31.23 < 2 4 0 -3 301.18 218.77 20.35 o 2 4 0 -2 7228.27 6629.18 99.68 o 2 4 0 -1 28756.80 29369.60 281.63 o 2 4 0 0 69.60 101.77 32.38 o 2 4 0 1 117796.00 116778.00 953.43 o 2 4 0 2 19.07 211.42 62.92 o 2 4 0 3 2357.75 2253.29 161.35 o 4 4 0 -3 6.23 33.54 34.47 < 4 4 0 -2 9423.26 9136.23 228.41 o 4 4 0 -1 5013.61 5744.09 210.85 o 4 4 0 0 4862.29 5474.37 249.71 o 4 4 0 1 41186.50 43402.50 911.06 o 4 4 0 2 2610.09 3028.57 717.55 o 0 6 0 0 140851.00 140110.00 1282.63 o 0 6 0 1 488.93 463.68 43.48 o 0 6 0 2 9.32 71.47 33.54 < 0 6 0 3 232.27 436.91 59.21 o 2 6 0 -3 2882.52 2356.25 83.39 o 2 6 0 -2 4097.30 4095.79 113.60 o 2 6 0 -1 898.63 821.55 64.05 o 2 6 0 0 115552.00 116520.00 1013.22 o 2 6 0 1 3917.50 4234.09 179.96 o 2 6 0 2 307.04 328.66 91.82 o 2 6 0 3 1572.38 1951.70 171.56 o 4 6 0 -3 4063.30 4334.47 170.46 o 4 6 0 -2 1817.57 1833.24 132.46 o 4 6 0 -1 23.85 3.24 71.94 < 4 6 0 0 27638.10 28996.40 628.39 o 4 6 0 1 9499.33 9006.90 452.58 o 0 8 0 0 2025.61 2264.39 166.20 o 0 8 0 1 886.11 916.65 81.17 o 0 8 0 2 15470.90 16151.10 359.31 o 0 8 0 3 4514.02 4087.82 190.58 o 2 8 0 -3 2700.15 2533.35 117.40 o 2 8 0 -2 2315.21 2291.02 123.89 o 2 8 0 -1 1857.93 2153.88 133.39 o 2 8 0 0 86.23 125.37 59.91 < 2 8 0 1 267.96 260.21 72.63 o 2 8 0 2 11665.90 11720.90 435.89 o 2 8 0 3 793.40 883.90 167.44 o 4 8 0 -3 1484.36 1102.42 104.28 o 4 8 0 -2 688.40 705.14 105.69 o 4 8 0 -1 4659.52 5469.94 309.83 o 4 8 0 0 557.26 337.90 117.95 < 0 10 0 0 5795.69 5965.34 345.97 o 0 10 0 1 29902.60 29288.40 523.91 o 0 10 0 2 283.20 297.67 78.18 o 0 10 0 3 86.53 171.17 86.28 < 2 10 0 -3 143.73 305.78 72.63 o 2 10 0 -2 2287.78 2035.24 139.40 o 2 10 0 -1 28784.00 28585.60 593.29 o 2 10 0 0 1468.16 1402.16 148.22 o 2 10 0 1 21587.20 21251.40 706.48 o 2 10 0 2 1387.82 1399.45 398.19 o 4 10 0 -3 1.95 60.60 71.01 < 4 10 0 -2 1513.69 1394.54 251.81 o 4 10 0 -1 7326.01 6431.71 823.71 o 0 12 0 0 2772.91 2813.25 405.92 o 0 12 0 1 929.29 825.83 184.32 o 0 12 0 2 946.17 536.99 254.16 < 2 12 0 -3 670.88 471.34 131.36 o 2 12 0 -2 1048.87 1643.99 342.49 o 1 1 1 -3 251.71 322.11 20.58 o 1 1 1 -2 104.98 103.14 21.74 o 1 1 1 -1 1443.01 1450.02 32.06 o 1 1 1 0 16349.20 15664.20 123.13 o 1 1 1 1 2121.82 2109.31 51.73 o 1 1 1 2 900.47 942.34 46.93 o 1 1 1 3 1177.45 1204.28 56.64 o 3 1 1 -3 22.58 44.41 20.59 < 3 1 1 -2 26.31 25.44 21.74 < 3 1 1 -1 180.45 347.16 35.62 o 3 1 1 0 6175.44 5900.52 117.89 o 3 1 1 1 3854.38 3824.57 113.89 o 3 1 1 2 293.55 269.92 58.52 o 3 1 1 3 786.33 948.42 99.21 o 5 1 1 -3 65.38 170.93 37.70 o 5 1 1 -2 48.79 173.48 47.42 o 5 1 1 -1 157.92 235.93 60.37 o 5 1 1 0 1413.19 1329.80 110.99 o 5 1 1 1 1811.06 1143.36 187.75 o 1 3 1 -3 0.88 36.55 11.80 o 1 3 1 -2 900.65 883.57 19.18 o 1 3 1 -1 425.77 439.55 15.03 o 1 3 1 0 1501.45 1607.15 31.88 o 1 3 1 1 13439.70 13223.30 137.42 o 1 3 1 2 21.07 63.38 24.06 < 1 3 1 3 362.49 394.33 42.79 o 3 3 1 -3 113.64 63.37 14.34 o 3 3 1 -2 605.39 571.14 33.07 o 3 3 1 -1 190.24 67.54 29.61 < 3 3 1 0 787.22 778.13 52.26 o 3 3 1 1 994.80 744.35 60.12 o 3 3 1 2 137.69 57.36 59.21 < 3 3 1 3 1275.87 1358.76 125.33 o 5 3 1 -3 148.56 184.58 41.17 o 5 3 1 -2 474.99 502.10 55.74 o 5 3 1 -1 73.94 94.60 59.45 < 5 3 1 0 266.65 556.03 94.14 o 1 5 1 -3 210.76 326.58 24.75 o 1 5 1 -2 352.43 301.11 21.97 o 1 5 1 -1 1297.55 1412.30 40.45 o 1 5 1 0 465.12 485.64 28.68 o 1 5 1 1 7422.82 7422.03 107.43 o 1 5 1 2 706.58 767.05 45.56 o 1 5 1 3 371.88 396.19 47.64 o 3 5 1 -3 11.51 91.60 20.12 o 3 5 1 -2 65.07 142.95 25.21 o 3 5 1 -1 820.35 705.97 43.94 o 3 5 1 0 5087.04 4994.72 145.48 o 3 5 1 1 1636.64 1455.88 94.10 o 3 5 1 2 760.58 777.75 83.49 o 3 5 1 3 346.77 394.35 96.22 o 5 5 1 -3 51.35 85.35 43.49 < 5 5 1 -2 85.22 145.03 50.89 < 5 5 1 -1 236.62 91.59 60.14 < 5 5 1 0 2500.42 2239.87 244.35 o 1 7 1 -3 581.04 700.95 44.40 o 1 7 1 -2 301.93 263.20 32.61 o 1 7 1 -1 48.72 68.93 28.68 < 1 7 1 0 50056.80 49826.90 376.82 o 1 7 1 1 3693.12 3618.93 100.26 o 1 7 1 2 1349.70 1348.90 77.69 o 1 7 1 3 42.93 136.70 46.72 < 3 7 1 -3 183.26 432.75 43.48 o 3 7 1 -2 105.07 178.57 37.01 o 3 7 1 -1 327.55 266.91 44.18 o 3 7 1 0 10584.30 11103.20 261.30 o 3 7 1 1 469.26 458.63 74.47 o 3 7 1 2 2838.45 2678.40 173.60 o 5 7 1 -3 83.39 129.53 54.13 < 5 7 1 -2 60.99 134.39 68.93 < 5 7 1 -1 6.96 136.24 85.82 < 1 9 1 -3 279.96 314.33 47.41 o 1 9 1 -2 648.76 572.39 52.96 o 1 9 1 -1 30.53 71.47 41.64 < 1 9 1 0 46.00 95.53 37.24 < 1 9 1 1 70.96 104.55 43.25 < 1 9 1 2 490.52 501.19 64.76 o 1 9 1 3 150.85 219.04 59.44 o 3 9 1 -3 54.17 72.63 41.40 < 3 9 1 -2 4.20 -3.70 49.50 < 3 9 1 -1 2854.32 2388.84 122.04 o 3 9 1 0 1843.67 1716.48 127.16 o 3 9 1 1 973.76 1128.08 178.30 o 5 9 1 -3 108.83 120.05 68.23 < 5 9 1 -2 5.17 177.88 118.20 < 1 11 1 -3 35.93 124.21 66.15 < 1 11 1 -2 206.82 210.25 60.83 o 1 11 1 -1 7819.67 8436.45 235.26 o 1 11 1 0 2835.93 2796.95 149.09 o 1 11 1 1 10787.00 10226.00 352.08 o 1 11 1 2 181.54 315.26 116.11 < 3 11 1 -3 82.32 -35.39 61.99 < 3 11 1 -2 20.47 66.85 82.35 < 3 11 1 -1 1053.10 913.46 266.87 o 0 0 2 0 2115.80 2040.82 73.00 o 0 0 2 2 2840.40 2730.39 64.59 o 2 0 2 -2 2679.58 2506.90 43.79 o 2 0 2 0 1621.23 1717.81 73.94 o 2 0 2 2 1378.08 1421.82 88.78 o 4 0 2 -2 3041.84 2755.48 118.73 o 4 0 2 0 922.47 969.84 104.29 o 4 0 2 2 1301.44 1652.89 202.10 o 0 2 2 0 21029.30 20106.00 133.64 o 0 2 2 1 1499.48 1477.39 29.33 o 0 2 2 2 727.00 658.63 27.28 o 0 2 2 3 551.11 551.96 36.30 o 2 2 2 -3 12.86 50.89 9.71 o 2 2 2 -2 36.42 98.77 15.03 o 2 2 2 -1 104.45 184.34 21.74 o 2 2 2 0 42656.30 42011.80 326.38 o 2 2 2 1 8166.55 8185.83 156.95 o 2 2 2 2 2968.56 2979.99 104.67 o 2 2 2 3 11.10 168.16 56.21 < 4 2 2 -3 451.01 427.36 38.85 o 4 2 2 -2 71.77 145.49 37.70 o 4 2 2 -1 777.54 951.58 69.84 o 4 2 2 0 14695.10 13563.60 300.31 o 4 2 2 1 8413.07 8458.05 282.04 o 4 2 2 2 65.27 -9.48 95.30 < 0 4 2 0 140492.00 139819.00 736.05 o 0 4 2 1 651.39 654.80 24.28 o 0 4 2 2 1193.21 1141.68 38.83 o 0 4 2 3 1450.86 1502.49 55.48 o 2 4 2 -3 628.70 695.49 25.20 o 2 4 2 -2 111.03 152.19 16.65 o 2 4 2 -1 78.82 107.09 18.04 o 2 4 2 0 53201.30 51326.60 359.31 o 2 4 2 1 8.32 28.45 32.15 < 2 4 2 2 2318.19 2542.96 101.70 o 2 4 2 3 5.92 135.78 55.28 < 4 4 2 -3 180.64 281.48 35.39 o 4 4 2 -2 297.64 459.10 41.17 o 4 4 2 -1 832.16 1024.67 73.54 o 4 4 2 0 15028.80 15844.80 302.90 o 4 4 2 1 1268.06 1053.29 102.67 o 4 4 2 2 395.18 606.90 160.05 o 0 6 2 0 5673.05 5654.16 141.90 o 0 6 2 1 755.30 804.70 40.47 o 0 6 2 2 6.81 45.34 25.44 < 0 6 2 3 309.01 324.03 37.93 o 2 6 2 -3 36.82 65.23 23.82 < 2 6 2 -2 899.28 1006.51 45.78 o 2 6 2 -1 13996.80 12996.70 157.56 o 2 6 2 0 41.35 108.02 32.38 o 2 6 2 1 517.87 521.75 54.81 o 2 6 2 2 3871.69 3827.22 150.65 o 2 6 2 3 314.39 274.08 65.22 o 4 6 2 -3 323.53 244.24 37.70 o 4 6 2 -2 687.09 945.16 73.31 o 4 6 2 -1 5993.05 5445.43 187.97 o 4 6 2 0 434.99 440.37 64.99 o 4 6 2 1 71.92 77.72 91.60 < 0 8 2 0 1257.07 1275.85 85.09 o 0 8 2 1 21163.70 21538.10 259.81 o 0 8 2 2 1473.87 1653.35 76.76 o 0 8 2 3 219.67 189.20 44.18 o 2 8 2 -3 47.18 86.28 31.69 < 2 8 2 -2 593.49 608.23 50.42 o 2 8 2 -1 1827.71 1993.94 84.15 o 2 8 2 0 286.36 381.86 51.81 o 2 8 2 1 27098.80 26695.70 409.65 o 2 8 2 2 15.39 49.50 61.99 < 2 8 2 3 196.08 341.40 99.23 o 4 8 2 -3 33.28 103.63 45.80 < 4 8 2 -2 1644.15 1465.64 104.28 o 4 8 2 -1 717.90 934.79 95.28 o 4 8 2 0 2546.49 2243.77 231.40 o 0 10 2 0 22104.60 22273.30 497.64 o 0 10 2 1 1142.91 1081.29 77.00 o 0 10 2 2 142.97 203.78 53.66 o 0 10 2 3 105.66 245.18 70.09 o 2 10 2 -3 1359.07 1529.34 96.19 o 2 10 2 -2 2248.55 2148.32 102.41 o 2 10 2 -1 25.10 117.97 55.51 < 2 10 2 0 15996.60 16133.90 366.57 o 2 10 2 1 887.51 978.70 129.97 o 4 10 2 -3 981.89 1123.44 104.99 o 4 10 2 -2 595.11 491.47 112.63 o 0 12 2 0 1533.52 1518.48 271.92 o 0 12 2 1 566.56 498.87 151.26 o 0 12 2 2 1995.82 1437.64 396.75 o 2 12 2 -3 40.14 -54.82 92.75 < 2 12 2 -2 25.59 206.79 200.78 < 1 1 3 -3 677.09 597.32 22.19 o 1 1 3 -2 2701.75 2763.17 39.42 o 1 1 3 -1 8050.91 8531.87 71.71 o 1 1 3 0 692.77 655.12 22.89 o 1 1 3 1 102342.00 100563.00 448.01 o 1 1 3 2 2800.95 2707.95 75.30 o 1 1 3 3 67.70 126.29 38.63 o 3 1 3 -3 0.11 37.93 14.80 < 3 1 3 -2 6316.28 6172.25 87.08 o 3 1 3 -1 273.80 182.94 30.30 o 3 1 3 0 7530.21 7412.30 143.21 o 3 1 3 1 44716.80 43573.70 456.43 o 3 1 3 2 3442.32 3230.83 142.81 o 3 1 3 3 5582.14 5460.80 228.22 o 5 1 3 -3 595.92 611.22 52.96 o 5 1 3 -2 4631.13 5355.72 163.29 o 5 1 3 -1 406.77 267.60 63.60 o 5 1 3 0 9195.62 9289.48 279.72 o 5 1 3 1 12975.90 12420.80 921.12 o 1 3 3 -3 937.29 989.14 38.37 o 1 3 3 -2 187.48 158.19 13.65 o 1 3 3 -1 1105.51 1159.51 28.89 o 1 3 3 0 277659.00 286385.00 1157.89 o 1 3 3 1 1008.87 1080.08 48.09 o 1 3 3 2 5003.39 5123.45 131.78 o 1 3 3 3 28.29 480.20 68.70 o 3 3 3 -3 1840.61 2089.71 59.38 o 3 3 3 -2 8.65 42.56 26.83 < 3 3 3 -1 46.28 239.86 45.34 o 3 3 3 0 121948.00 126627.00 890.28 o 3 3 3 1 3637.92 4029.30 150.65 o 3 3 3 2 12944.10 13224.40 324.55 o 3 3 3 3 1588.31 2079.61 151.91 o 5 3 3 -3 1648.47 2025.57 106.34 o 5 3 3 -2 8.74 164.46 54.36 o 5 3 3 -1 0.12 165.39 63.61 < 5 3 3 0 23974.00 25524.10 543.44 o 1 5 3 -3 1547.20 1414.57 48.31 o 1 5 3 -2 1418.70 1515.84 45.07 o 1 5 3 -1 790.38 712.85 33.06 o 1 5 3 0 1828.60 1977.61 55.24 o 1 5 3 1 217.32 240.54 30.30 o 1 5 3 2 12459.60 12471.80 204.45 o 1 5 3 3 3485.92 3650.82 129.39 o 3 5 3 -3 836.53 656.67 36.07 o 3 5 3 -2 789.35 877.77 47.17 o 3 5 3 -1 11821.60 11798.80 205.68 o 3 5 3 0 7276.76 7041.52 184.16 o 3 5 3 1 9618.04 10378.90 235.99 o 3 5 3 2 11857.00 11854.50 294.04 o 3 5 3 3 387.86 280.32 113.79 < 5 5 3 -3 0.84 36.32 44.64 < 5 5 3 -2 416.60 463.03 64.76 o 5 5 3 -1 5106.95 5718.16 216.23 o 5 5 3 0 3657.50 3010.97 273.18 o 1 7 3 -3 14.09 89.05 31.69 < 1 7 3 -2 4037.92 3737.06 94.23 o 1 7 3 -1 59444.70 60368.10 439.69 o 1 7 3 0 1370.20 1438.06 66.12 o 1 7 3 1 55873.50 55430.60 453.75 o 1 7 3 2 187.47 224.59 44.87 o 1 7 3 3 889.02 840.61 81.40 o 3 7 3 -3 65.87 81.19 34.23 < 3 7 3 -2 3808.83 3294.42 102.34 o 3 7 3 -1 15060.50 15291.20 256.98 o 3 7 3 0 447.06 387.40 64.07 o 3 7 3 1 43918.80 45622.70 636.83 o 3 7 3 2 462.93 485.93 103.15 o 5 7 3 -3 4.67 55.05 56.21 < 5 7 3 -2 3272.74 2943.82 164.56 o 5 7 3 -1 3378.05 3175.49 248.70 o 1 9 3 -3 565.80 434.56 52.50 o 1 9 3 -2 494.89 603.40 57.59 o 1 9 3 -1 154.53 247.26 43.02 o 1 9 3 0 22940.00 23692.70 333.25 o 1 9 3 1 2334.51 2466.54 111.65 o 1 9 3 2 192.12 266.23 61.99 o 1 9 3 3 2201.68 2278.58 145.88 o 3 9 3 -3 1920.95 1741.77 99.18 o 3 9 3 -2 3091.93 3598.09 142.37 o 3 9 3 -1 1.25 -9.72 56.90 < 3 9 3 0 17284.00 17614.20 395.97 o 3 9 3 1 3061.07 3018.10 586.65 o 5 9 3 -3 1918.19 1967.32 139.88 o 1 11 3 -3 2809.09 2970.58 155.57 o 1 11 3 -2 6967.22 6948.45 237.62 o 1 11 3 -1 12.93 132.08 68.47 < 1 11 3 0 464.06 501.66 76.56 o 1 11 3 1 769.17 738.67 117.72 o 1 11 3 2 6622.56 6355.09 568.39 o 3 11 3 -3 1586.60 1349.19 129.02 o 3 11 3 -2 881.53 547.63 121.41 o 3 11 3 -1 25.11 160.07 204.94 < 0 0 4 0 2405.60 2374.99 67.61 o 0 0 4 2 1351.61 1280.19 46.45 o 2 0 4 -2 74.91 48.80 25.21 < 2 0 4 0 3024.71 3048.49 86.14 o 2 0 4 2 1667.44 1811.01 122.75 o 4 0 4 -2 62.33 11.57 45.10 < 4 0 4 0 161.64 65.92 58.98 < 4 0 4 2 550.66 748.42 175.08 o 0 2 4 0 8017.75 8886.00 108.91 o 0 2 4 1 1680.40 1792.41 41.12 o 0 2 4 2 72.60 58.98 20.59 < 0 2 4 3 119.11 150.57 25.21 o 2 2 4 -3 154.06 195.20 16.19 o 2 2 4 -2 28.78 82.34 18.74 o 2 2 4 -1 612.28 710.55 32.83 o 2 2 4 0 554.17 709.23 41.62 o 2 2 4 1 357.49 403.81 42.32 o 2 2 4 2 6198.47 6249.85 156.26 o 2 2 4 3 162.16 221.35 53.43 o 4 2 4 -3 74.44 72.86 27.29 < 4 2 4 -2 13.62 34.70 34.47 < 4 2 4 -1 438.98 598.31 60.13 o 4 2 4 0 354.32 316.63 55.28 o 4 2 4 1 61.60 184.58 69.16 < 4 2 4 2 385.31 429.27 126.98 o 0 4 4 0 26281.20 25483.30 245.54 o 0 4 4 1 170.35 217.41 23.13 o 0 4 4 2 990.87 959.47 42.54 o 0 4 4 3 337.90 424.16 42.56 o 2 4 4 -3 8.03 55.98 16.89 o 2 4 4 -2 14.88 31.00 18.27 < 2 4 4 -1 1812.42 1633.70 55.47 o 2 4 4 0 2997.49 2848.24 90.79 o 2 4 4 1 317.48 352.25 50.19 o 2 4 4 2 1704.05 1569.30 91.78 o 2 4 4 3 89.96 89.75 61.06 < 4 4 4 -3 1.62 24.06 30.76 < 4 4 4 -2 53.87 117.27 44.64 < 4 4 4 -1 145.24 131.84 48.80 < 4 4 4 0 1390.86 1574.87 117.69 o 4 4 4 1 1741.41 1706.35 134.80 o 4 4 4 2 42.05 346.73 158.21 < 0 6 4 0 47.25 121.44 35.62 o 0 6 4 1 7014.83 6951.81 112.79 o 0 6 4 2 1719.34 1858.30 62.64 o 0 6 4 3 428.44 370.04 44.87 o 2 6 4 -3 37.27 45.80 25.44 < 2 6 4 -2 74.86 124.44 25.67 o 2 6 4 -1 0.38 63.84 28.22 < 2 6 4 0 2626.58 2893.21 100.53 o 2 6 4 1 8144.65 7669.20 187.13 o 2 6 4 2 249.04 188.74 52.27 o 2 6 4 3 274.71 332.60 71.70 o 4 6 4 -3 91.31 34.00 37.24 < 4 6 4 -2 17.79 13.18 41.17 < 4 6 4 -1 5.33 -46.72 52.28 < 4 6 4 0 1242.99 1231.81 100.82 o 4 6 4 1 855.38 1077.00 167.20 o 0 8 4 0 5591.54 5507.57 181.95 o 0 8 4 1 2595.21 2671.35 92.91 o 0 8 4 2 31.15 88.59 32.61 < 0 8 4 3 121.10 57.83 38.17 < 2 8 4 -3 237.40 359.43 43.95 o 2 8 4 -2 568.35 678.09 52.50 o 2 8 4 -1 120.80 136.24 39.32 o 2 8 4 0 2064.97 1890.80 89.93 o 2 8 4 1 3885.06 3595.55 149.04 o 2 8 4 2 156.20 185.97 65.46 < 2 8 4 3 135.96 82.81 110.56 < 4 8 4 -3 82.80 177.41 46.03 o 4 8 4 -2 29.71 71.94 50.43 < 4 8 4 -1 20.74 114.50 65.92 < 4 8 4 0 3483.06 3340.22 374.89 o 0 10 4 0 16673.10 16655.20 464.33 o 0 10 4 1 17.34 83.27 52.97 < 0 10 4 2 687.80 811.53 78.63 o 0 10 4 3 261.25 388.35 71.70 o 2 10 4 -3 18.17 176.03 55.28 o 2 10 4 -2 122.82 98.77 51.58 < 2 10 4 -1 1203.36 1174.48 95.50 o 2 10 4 0 13456.70 13206.30 313.56 o 2 10 4 1 187.91 252.12 104.55 < 4 10 4 -3 2.45 24.75 62.92 < 4 10 4 -2 4.03 -135.09 120.05 < 0 12 4 1 787.49 1094.37 414.67 < 1 1 5 -3 444.90 527.92 26.36 o 1 1 5 -2 653.68 641.33 25.66 o 1 1 5 -1 45.08 96.68 17.12 o 1 1 5 0 154980.00 151899.00 622.22 o 1 1 5 1 1317.18 1414.59 42.99 o 1 1 5 2 198.50 262.51 30.76 o 1 1 5 3 1684.12 1932.30 82.53 o 3 1 5 -3 0.15 40.94 19.20 < 3 1 5 -2 560.69 555.44 31.68 o 3 1 5 -1 3593.92 4018.01 83.83 o 3 1 5 0 76229.60 76894.10 576.65 o 3 1 5 1 5939.37 6410.10 166.93 o 3 1 5 2 627.01 722.26 77.01 o 3 1 5 3 258.70 542.39 85.81 o 5 1 5 -3 338.84 461.64 56.66 o 5 1 5 -2 125.44 188.28 46.49 o 5 1 5 -1 1641.65 1862.86 114.22 o 5 1 5 0 20195.40 19784.30 467.28 o 1 3 5 -3 19.15 59.68 24.98 < 1 3 5 -2 2803.95 2695.74 54.96 o 1 3 5 -1 23874.60 23315.70 186.24 o 1 3 5 0 210.86 233.37 28.68 o 1 3 5 1 253.53 326.34 31.45 o 1 3 5 2 172.88 170.70 35.62 o 1 3 5 3 534.73 585.34 57.12 o 3 3 5 -3 261.21 141.54 28.45 o 3 3 5 -2 3781.21 3637.45 89.59 o 3 3 5 -1 13107.30 11872.80 193.98 o 3 3 5 0 1025.82 1240.09 80.01 o 3 3 5 1 1976.13 2211.21 113.97 o 3 3 5 2 700.38 814.99 93.90 o 3 3 5 3 652.92 694.06 102.46 o 5 3 5 -3 323.51 333.75 51.58 o 5 3 5 -2 2869.55 2872.37 131.51 o 5 3 5 -1 3795.41 3608.65 177.24 o 5 3 5 0 4461.32 4518.54 313.33 o 1 5 5 -3 137.63 222.74 27.29 o 1 5 5 -2 599.55 635.47 37.00 o 1 5 5 -1 8463.33 8226.64 119.14 o 1 5 5 0 9344.11 9059.04 137.32 o 1 5 5 1 53777.80 53194.80 400.80 o 1 5 5 2 1588.61 1557.49 81.61 o 1 5 5 3 59.24 102.47 44.41 < 3 5 5 -3 218.99 96.45 28.68 o 3 5 5 -2 3249.00 3259.57 90.10 o 3 5 5 -1 1668.17 1864.94 92.93 o 3 5 5 0 15393.00 14981.60 293.33 o 3 5 5 1 29633.30 29006.90 470.17 o 3 5 5 2 687.22 602.00 80.71 o 3 5 5 3 968.69 825.59 267.80 o 5 5 5 -3 942.34 895.85 81.17 o 5 5 5 -2 2202.03 2369.33 133.16 o 5 5 5 -1 334.90 390.65 74.94 o 5 5 5 0 7050.56 6212.73 648.94 o 1 7 5 -3 2814.14 2941.39 95.90 o 1 7 5 -2 4415.19 4191.29 104.86 o 1 7 5 -1 1240.01 1460.34 65.90 o 1 7 5 0 70095.50 69302.90 539.41 o 1 7 5 1 175.11 207.01 39.32 o 1 7 5 2 157.12 203.77 45.57 o 1 7 5 3 233.51 339.54 65.92 o 3 7 5 -3 2314.52 2424.63 91.76 o 3 7 5 -2 745.66 685.91 56.89 o 3 7 5 -1 300.99 298.83 49.03 o 3 7 5 0 16437.70 16418.50 328.20 o 3 7 5 1 255.26 172.78 66.38 < 3 7 5 2 577.09 634.17 163.98 o 5 7 5 -3 1366.14 1259.51 104.28 o 5 7 5 -2 228.63 290.51 80.03 o 5 7 5 -1 649.47 674.17 227.58 < 1 9 5 -3 51.98 115.89 45.57 < 1 9 5 -2 729.05 877.65 68.22 o 1 9 5 -1 4488.41 4067.47 144.39 o 1 9 5 0 5867.25 5526.81 169.75 o 1 9 5 1 1658.10 1699.41 102.43 o 1 9 5 2 6473.40 6823.57 219.16 o 1 9 5 3 735.55 739.83 110.78 o 3 9 5 -3 157.39 147.11 48.34 o 3 9 5 -2 1052.96 1223.07 86.95 o 3 9 5 -1 10117.10 9819.15 272.96 o 3 9 5 0 119.55 235.70 100.85 < 5 9 5 -3 3.41 93.45 128.38 < 1 11 5 -3 513.32 449.38 119.34 o 1 11 5 -2 1703.12 1755.17 145.67 o 1 11 5 -1 13698.30 13978.30 394.03 o 1 11 5 0 0.90 -53.66 108.02 < 1 11 5 1 20520.30 20240.70 977.72 o 3 11 5 -3 58.82 -9.25 95.30 < 3 11 5 -2 1118.93 1178.92 410.93 < 0 0 6 0 269940.00 269988.00 2136.11 o 0 0 6 2 324.24 301.11 35.62 o 2 0 6 -2 101.40 75.63 28.45 < 2 0 6 0 144105.00 142823.00 1036.78 o 2 0 6 2 13546.30 13610.60 328.39 o 4 0 6 -2 64.45 116.11 52.04 < 4 0 6 0 32514.20 33039.50 615.21 o 4 0 6 2 7329.54 6477.06 1101.72 o 0 2 6 0 11178.30 11289.90 195.05 o 0 2 6 1 15236.50 15065.10 157.27 o 0 2 6 2 1267.65 1196.02 48.31 o 0 2 6 3 779.03 762.83 40.47 o 2 2 6 -3 810.43 736.60 35.84 o 2 2 6 -2 2220.87 2300.26 60.53 o 2 2 6 -1 765.12 664.30 39.77 o 2 2 6 0 376.97 563.15 37.24 o 2 2 6 1 35113.60 34398.40 339.47 o 2 2 6 2 14810.00 14790.10 238.51 o 2 2 6 3 1789.29 1566.12 96.87 o 4 2 6 -3 1.07 41.87 25.68 < 4 2 6 -2 1751.51 2086.97 89.46 o 4 2 6 -1 2374.56 2207.17 103.09 o 4 2 6 0 1907.68 1518.46 100.57 o 4 2 6 1 14711.40 15091.70 405.64 o 4 2 6 2 4229.44 4796.44 795.40 o 0 4 6 0 460.61 426.91 40.70 o 0 4 6 1 39091.70 38934.90 284.07 o 0 4 6 2 2815.36 2729.66 79.01 o 0 4 6 3 2.79 51.58 32.38 < 2 4 6 -3 97.76 101.54 22.90 o 2 4 6 -2 2141.04 1920.55 56.62 o 2 4 6 -1 3512.48 3907.10 100.47 o 2 4 6 0 2528.34 2443.34 78.80 o 2 4 6 1 47160.00 48526.50 527.75 o 2 4 6 2 5.22 -11.10 50.89 < 2 4 6 3 1049.36 838.27 90.19 o 4 4 6 -3 1.72 43.95 35.62 < 4 4 6 -2 3552.94 3122.36 128.23 o 4 4 6 -1 155.04 336.08 56.90 o 4 4 6 0 807.36 895.91 95.28 o 4 4 6 1 15326.90 16167.70 475.00 o 0 6 6 0 91718.00 92596.90 854.03 o 0 6 6 1 2431.37 2271.33 73.72 o 0 6 6 2 1039.70 1130.01 61.28 o 0 6 6 3 116.39 245.41 49.50 o 2 6 6 -3 1200.69 1280.44 63.12 o 2 6 6 -2 429.83 497.24 42.09 o 2 6 6 -1 719.46 800.60 55.96 o 2 6 6 0 77226.50 78681.40 663.97 o 2 6 6 1 121.04 121.43 49.50 < 2 6 6 2 1222.06 1300.01 97.81 o 2 6 6 3 1380.14 1506.95 118.16 o 4 6 6 -3 1561.19 1904.85 101.73 o 4 6 6 -2 111.01 226.68 51.35 o 4 6 6 -1 780.39 944.95 88.57 o 4 6 6 0 18775.50 19117.80 422.31 o 4 6 6 1 1445.87 1615.87 233.32 o 0 8 6 0 3214.25 3448.84 172.16 o 0 8 6 1 209.85 216.03 41.63 o 0 8 6 2 5030.87 4969.41 147.37 o 0 8 6 3 2182.58 2166.81 113.28 o 2 8 6 -3 877.47 1029.76 72.38 o 2 8 6 -2 126.33 115.88 35.62 o 2 8 6 -1 2.57 55.05 39.79 < 2 8 6 0 660.38 560.37 64.99 o 2 8 6 1 2280.65 2408.88 131.31 o 2 8 6 2 3836.54 3906.51 183.49 o 2 8 6 3 336.21 223.89 151.96 < 4 8 6 -3 398.87 409.38 60.37 o 4 8 6 -2 10.88 72.40 55.28 < 4 8 6 -1 1356.69 1617.73 154.24 o 0 10 6 0 472.69 470.66 89.74 o 0 10 6 1 16272.10 16170.70 350.42 o 0 10 6 2 227.06 306.01 69.85 o 0 10 6 3 451.14 462.57 116.34 o 2 10 6 -3 12.24 51.81 53.90 < 2 10 6 -2 239.21 377.71 74.71 o 2 10 6 -1 16602.60 16479.00 387.97 o 2 10 6 0 29.11 -9.71 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152.98 103.62 52.74 < 3 3 7 2 491.85 323.80 74.94 o 3 3 7 3 673.85 794.66 153.34 o 5 3 7 -3 0.56 -18.74 48.11 < 5 3 7 -2 85.15 27.29 55.74 < 5 3 7 -1 2.05 -4.63 67.31 < 5 3 7 0 1709.20 1354.26 241.39 o 1 5 7 -3 240.37 309.47 35.39 o 1 5 7 -2 457.02 433.63 34.92 o 1 5 7 -1 124.81 189.20 30.53 o 1 5 7 0 347.00 367.74 39.55 o 1 5 7 1 1886.03 2032.84 90.15 o 1 5 7 2 890.05 805.43 65.91 o 1 5 7 3 346.76 290.96 51.58 o 3 5 7 -3 355.57 534.95 44.41 o 3 5 7 -2 146.30 111.72 40.48 < 3 5 7 -1 233.39 241.24 49.27 o 3 5 7 0 3142.82 2746.96 130.35 o 3 5 7 1 48.13 52.04 66.39 < 3 5 7 2 1366.58 1232.02 138.05 o 5 5 7 -3 247.15 330.98 59.21 o 5 5 7 -2 62.80 72.63 58.06 < 5 5 7 -1 225.41 216.96 95.76 < 1 7 7 -3 3.70 8.56 36.78 < 1 7 7 -2 650.25 612.16 53.42 o 1 7 7 -1 3301.91 3376.94 109.76 o 1 7 7 0 9382.30 9628.17 188.91 o 1 7 7 1 175.49 240.55 50.65 o 1 7 7 2 493.41 506.04 63.37 o 1 7 7 3 508.54 542.59 66.84 o 3 7 7 -3 131.75 199.15 43.25 o 3 7 7 -2 122.24 68.23 43.48 < 3 7 7 -1 791.68 786.29 76.78 o 3 7 7 0 1434.17 1330.72 104.51 o 3 7 7 1 694.20 968.11 121.88 o 5 7 7 -3 81.62 203.78 68.70 < 5 7 7 -2 100.00 -63.38 84.66 < 1 9 7 -3 169.33 249.80 58.29 o 1 9 7 -2 99.10 137.63 45.57 o 1 9 7 -1 190.95 198.92 54.59 o 1 9 7 0 291.65 300.91 53.20 o 1 9 7 1 31.15 -10.41 45.80 < 1 9 7 2 179.09 257.21 76.56 o 1 9 7 3 105.68 198.92 147.57 < 3 9 7 -3 3.25 17.58 50.19 < 3 9 7 -2 317.98 615.93 71.47 o 3 9 7 -1 486.41 664.02 102.69 o 3 9 7 0 2500.49 2498.57 308.62 o 5 9 7 -3 8.20 -190.60 129.53 < 1 11 7 -3 254.02 29.84 188.04 < 1 11 7 -2 604.74 443.82 236.60 < 1 11 7 -1 1534.83 1415.82 468.24 o 1 11 7 0 2669.63 2211.60 316.70 o 3 11 7 -3 19.33 54.13 164.23 < 0 0 8 0 3914.32 4054.94 141.29 o 0 0 8 2 3232.07 3107.19 110.41 o 2 0 8 -2 4757.87 4247.74 106.39 o 2 0 8 0 121.02 168.15 46.49 o 2 0 8 2 178.73 117.50 72.40 < 4 0 8 -2 6349.24 5994.66 247.91 o 4 0 8 0 4860.28 5011.28 301.48 o 0 2 8 0 63437.10 62397.90 640.12 o 0 2 8 1 7308.89 6987.84 128.88 o 0 2 8 2 294.40 301.82 36.54 o 0 2 8 3 435.37 560.61 53.89 o 2 2 8 -3 9.86 22.67 24.75 < 2 2 8 -2 431.21 466.70 41.17 o 2 2 8 -1 217.84 237.54 34.69 o 2 2 8 0 77322.40 77330.80 566.66 o 2 2 8 1 20482.40 20623.20 316.16 o 2 2 8 2 862.72 858.88 74.69 o 2 2 8 3 111.12 125.83 64.07 < 4 2 8 -3 929.15 894.64 61.74 o 4 2 8 -2 684.37 796.23 68.68 o 4 2 8 -1 303.20 432.98 63.60 o 4 2 8 0 30671.90 29859.10 488.36 o 4 2 8 1 17184.70 16664.20 454.52 o 0 4 8 0 171727.00 170453.00 1143.08 o 0 4 8 1 1627.32 1678.04 66.11 o 0 4 8 2 1585.24 1593.97 68.43 o 0 4 8 3 2478.28 2653.03 101.92 o 2 4 8 -3 1801.46 1804.57 60.79 o 2 4 8 -2 69.98 66.62 33.08 < 2 4 8 -1 1320.23 1438.77 64.74 o 2 4 8 0 81502.40 82585.50 631.98 o 2 4 8 1 61.46 62.68 45.34 < 2 4 8 2 1234.84 1213.51 96.19 o 2 4 8 3 279.24 352.49 70.54 o 4 4 8 -3 835.05 942.11 73.07 o 4 4 8 -2 10.75 134.85 55.28 < 4 4 8 -1 2122.12 2248.46 133.62 o 4 4 8 0 25964.90 27096.00 493.92 o 4 4 8 1 473.32 640.20 153.11 o 0 6 8 0 6616.06 6605.96 193.19 o 0 6 8 1 7849.96 7714.76 161.05 o 0 6 8 2 1158.27 1136.26 75.15 o 0 6 8 3 3.20 -5.09 49.50 < 2 6 8 -3 111.25 127.91 35.85 o 2 6 8 -2 2919.78 3054.18 100.76 o 2 6 8 -1 24124.50 23842.80 340.51 o 2 6 8 0 94.37 173.02 50.66 o 2 6 8 1 992.79 1041.09 91.34 o 2 6 8 2 7041.56 7120.70 256.54 o 2 6 8 3 364.50 172.77 121.89 < 4 6 8 -3 18.38 15.27 47.42 < 4 6 8 -2 2109.87 2460.02 141.25 o 4 6 8 -1 10718.00 10357.40 329.90 o 4 6 8 0 334.49 126.29 143.63 < 0 8 8 0 781.69 748.36 91.35 o 0 8 8 1 31969.20 31936.80 413.00 o 0 8 8 2 2270.90 2341.56 117.67 o 0 8 8 3 400.21 420.71 65.22 o 2 8 8 -3 56.14 85.81 46.72 < 2 8 8 -2 1935.61 2039.34 114.67 o 2 8 8 -1 5392.69 5593.80 178.78 o 2 8 8 0 270.10 335.61 63.84 o 2 8 8 1 41530.10 39700.00 614.61 o 2 8 8 2 173.79 186.43 173.01 < 4 8 8 -3 395.91 345.54 73.55 o 4 8 8 -2 3235.52 3289.25 182.60 o 4 8 8 -1 1520.48 1635.03 339.68 o 0 10 8 0 18449.60 17880.70 810.18 o 0 10 8 1 1049.26 1255.01 160.03 o 0 10 8 2 1288.66 1148.34 231.70 o 0 10 8 3 825.53 374.88 237.05 < 2 10 8 -3 2719.30 2960.72 236.94 o 2 10 8 -2 3742.71 4118.09 267.85 o 2 10 8 -1 8.21 -78.88 131.38 < 2 10 8 0 12845.30 12033.20 1186.60 o 1 1 9 -3 359.36 365.88 32.38 o 1 1 9 -2 1083.58 1046.43 49.94 o 1 1 9 -1 1331.16 1324.21 56.18 o 1 1 9 0 11671.90 11134.20 143.43 o 1 1 9 1 38277.20 37736.10 342.48 o 1 1 9 2 2710.25 2748.51 100.99 o 1 1 9 3 1.78 43.49 55.75 < 3 1 9 -3 133.00 168.62 27.76 o 3 1 9 -2 1472.98 1462.03 68.89 o 3 1 9 -1 282.94 244.24 49.26 o 3 1 9 0 1055.71 1132.15 87.41 o 3 1 9 1 15532.30 14534.60 324.81 o 3 1 9 2 3833.51 3553.34 183.26 o 3 1 9 3 2699.53 1669.50 429.28 o 5 1 9 -3 18.94 8.33 57.83 < 5 1 9 -2 1077.69 1218.90 113.08 o 5 1 9 -1 303.58 200.53 70.08 < 1 3 9 -3 178.33 265.30 45.80 o 1 3 9 -2 243.78 222.96 34.92 o 1 3 9 -1 935.28 937.17 58.04 o 1 3 9 0 90599.60 91242.40 685.78 o 1 3 9 1 7053.28 7146.47 158.53 o 1 3 9 2 1603.71 1630.39 96.41 o 1 3 9 3 10.99 63.38 58.52 < 3 3 9 -3 162.74 308.78 45.80 o 3 3 9 -2 7.22 1.62 35.62 < 3 3 9 -1 1501.17 1784.21 103.12 o 3 3 9 0 25174.90 26257.40 431.12 o 3 3 9 1 63.77 193.84 71.01 < 3 3 9 2 5406.07 4995.46 260.82 o 5 3 9 -3 171.46 163.99 62.91 < 5 3 9 -2 51.26 134.62 69.62 < 5 3 9 -1 387.26 397.59 127.90 o 1 5 9 -3 416.36 420.93 45.79 o 1 5 9 -2 88.31 88.36 35.16 < 1 5 9 -1 4994.38 4770.59 125.86 o 1 5 9 0 867.60 764.04 57.58 o 1 5 9 1 7819.88 7548.82 182.07 o 1 5 9 2 4026.44 4244.61 164.28 o 1 5 9 3 1561.51 1503.14 114.45 o 3 5 9 -3 243.70 231.52 40.48 o 3 5 9 -2 59.68 94.14 41.17 < 3 5 9 -1 73.51 121.90 53.89 < 3 5 9 0 544.51 510.43 76.78 o 3 5 9 1 15971.50 17089.20 386.18 o 5 5 9 -3 5.14 -21.74 61.07 < 5 5 9 -2 28.54 114.50 78.65 < 1 7 9 -3 28.91 53.66 45.11 < 1 7 9 -2 41.01 66.85 40.48 < 1 7 9 -1 9698.19 10120.40 211.77 o 1 7 9 0 54.42 61.30 43.02 < 1 7 9 1 8865.99 8939.82 240.46 o 1 7 9 2 525.69 412.14 67.53 o 1 7 9 3 705.53 764.82 99.22 o 3 7 9 -3 215.56 119.58 49.03 < 3 7 9 -2 45.81 24.29 57.83 < 3 7 9 -1 1141.33 1149.75 101.29 o 3 7 9 0 21.20 3.70 74.02 < 3 7 9 1 9899.71 9653.12 798.52 o 5 7 9 -3 79.54 134.85 76.56 < 5 7 9 -2 261.60 -53.20 235.69 < 1 9 9 -3 1.51 122.60 62.92 < 1 9 9 -2 629.29 602.01 72.62 o 1 9 9 -1 888.76 966.44 92.04 o 1 9 9 0 21625.60 22245.10 413.49 o 1 9 9 1 27.88 -92.52 79.34 < 1 9 9 2 586.10 614.74 134.84 o 3 9 9 -3 124.62 90.67 65.23 < 3 9 9 -2 25.86 -12.03 79.57 < 3 9 9 -1 90.21 108.25 99.46 < 0 0 10 0 89015.70 89515.50 1309.49 o 0 0 10 2 673.54 692.38 70.76 o 2 0 10 -2 2105.50 2033.71 101.24 o 2 0 10 0 34297.60 33758.30 506.87 o 2 0 10 2 5943.11 5832.02 286.37 o 4 0 10 -2 1185.53 1309.70 131.57 o 4 0 10 0 13262.10 13855.10 513.01 o 0 2 10 0 493.94 551.11 84.41 o 0 2 10 1 94.81 143.87 39.55 o 0 2 10 2 347.67 387.86 52.27 o 0 2 10 3 18.93 90.67 42.33 < 2 2 10 -3 210.88 321.03 55.97 o 2 2 10 -2 66.07 85.58 46.49 < 2 2 10 -1 2471.84 2444.76 97.76 o 2 2 10 0 7871.05 8204.01 182.98 o 2 2 10 1 272.95 374.92 66.15 o 2 2 10 2 2218.70 2102.78 129.92 o 2 2 10 3 207.15 246.80 83.27 < 4 2 10 -3 576.36 488.21 51.80 o 4 2 10 -2 42.74 15.03 56.21 < 4 2 10 -1 1552.67 1423.61 111.91 o 4 2 10 0 4864.34 4335.71 222.72 o 4 2 10 1 69.34 16.89 219.51 < 0 4 10 0 6535.68 6532.50 219.27 o 0 4 10 1 10705.30 11311.00 212.99 o 0 4 10 2 1091.83 1034.07 69.83 o 0 4 10 3 47.66 79.57 45.10 < 2 4 10 -3 158.24 136.70 43.72 o 2 4 10 -2 576.18 550.42 58.51 o 2 4 10 -1 2910.29 3117.13 119.25 o 2 4 10 0 804.84 820.50 82.10 o 2 4 10 1 9338.11 9495.27 282.18 o 2 4 10 2 503.08 443.83 84.42 o 2 4 10 3 700.85 734.75 119.57 o 4 4 10 -3 26.49 64.54 55.05 < 4 4 10 -2 623.37 527.76 86.73 o 4 4 10 -1 1516.62 1745.97 135.04 o 4 4 10 0 1768.09 2169.96 232.14 o 0 6 10 0 6309.69 5822.46 252.37 o 0 6 10 1 95.73 43.49 46.95 < 0 6 10 2 179.15 148.49 50.65 < 0 6 10 3 205.86 202.39 65.46 o 2 6 10 -3 38.97 48.81 47.42 < 2 6 10 -2 283.76 380.24 58.29 o 2 6 10 -1 617.38 416.06 57.36 o 2 6 10 0 10524.30 11215.50 284.89 o 2 6 10 1 12.26 21.05 57.60 < 2 6 10 2 134.17 12.72 74.94 < 4 6 10 -3 158.99 194.76 62.22 o 4 6 10 -2 248.73 326.59 77.25 o 4 6 10 -1 270.21 136.23 97.38 < 0 8 10 0 2573.12 2567.05 176.38 o 0 8 10 1 2225.40 2075.10 124.38 o 0 8 10 2 1890.78 2053.32 129.71 o 0 8 10 3 537.00 595.09 82.34 o 2 8 10 -3 26.59 96.92 47.19 < 2 8 10 -2 64.96 75.87 55.28 < 2 8 10 -1 340.92 368.45 70.31 o 2 8 10 0 648.05 652.20 91.82 o 2 8 10 1 1745.15 1582.69 217.35 o 4 8 10 -3 21.70 -48.11 70.32 < 4 8 10 -2 59.45 95.76 221.82 < 0 10 10 0 728.97 394.09 302.97 < 0 10 10 1 2606.52 3145.34 491.94 o 2 10 10 -3 49.98 -139.94 248.66 < 2 10 10 -2 957.23 1027.26 318.21 o 1 1 11 -3 783.90 874.13 69.38 o 1 1 11 -2 337.59 309.92 49.26 o 1 1 11 -1 518.84 558.52 60.13 o 1 1 11 0 81523.10 81549.30 671.08 o 1 1 11 1 338.31 293.73 44.41 o 1 1 11 2 179.71 209.79 45.10 o 1 1 11 3 1712.52 1650.11 116.07 o 3 1 11 -3 148.67 94.14 43.25 < 3 1 11 -2 242.71 240.08 43.02 o 3 1 11 -1 781.83 917.87 72.15 o 3 1 11 0 40098.60 39321.00 578.10 o 3 1 11 1 8039.88 8347.32 292.27 o 3 1 11 2 95.16 66.62 136.93 < 5 1 11 -3 54.41 210.26 69.39 o 5 1 11 -2 184.99 255.12 86.51 < 1 3 11 -3 189.07 168.85 42.79 o 1 3 11 -2 3615.55 3648.65 140.71 o 1 3 11 -1 6298.69 6286.67 175.21 o 1 3 11 0 1380.23 1345.42 85.78 o 1 3 11 1 64.99 238.24 55.51 o 1 3 11 2 1351.08 1618.34 109.37 o 1 3 11 3 17.98 91.14 63.15 < 3 3 11 -3 23.63 25.68 42.56 < 3 3 11 -2 4351.48 4234.12 146.47 o 3 3 11 -1 3819.97 3847.79 172.38 o 3 3 11 0 5.22 23.83 66.39 < 3 3 11 1 275.19 369.61 89.51 o 3 3 11 2 2027.33 1775.88 386.11 o 5 3 11 -3 8.34 83.50 66.85 < 5 3 11 -2 3359.31 3041.87 267.18 o 1 5 11 -3 3.28 47.42 49.96 < 1 5 11 -2 190.77 188.51 53.43 o 1 5 11 -1 2850.81 2827.09 134.05 o 1 5 11 0 9937.36 9986.12 246.35 o 1 5 11 1 28217.20 28721.40 459.33 o 1 5 11 2 390.60 408.92 71.01 o 1 5 11 3 157.46 226.44 71.70 o 3 5 11 -3 427.75 343.22 61.29 o 3 5 11 -2 1652.74 1849.90 128.32 o 3 5 11 -1 108.47 114.96 61.30 < 3 5 11 0 12954.30 13300.20 358.80 o 3 5 11 1 19748.10 19785.70 694.68 o 5 5 11 -3 1059.75 1064.92 113.08 o 5 5 11 -2 1416.64 1636.22 217.59 o 1 7 11 -3 2761.37 3039.16 156.49 o 1 7 11 -2 1724.07 1698.46 109.82 o 1 7 11 -1 1.92 25.21 54.82 < 1 7 11 0 55289.80 55129.90 686.05 o 1 7 11 1 1365.82 1521.98 131.34 o 1 7 11 2 20.00 -40.25 80.50 < 1 7 11 3 692.40 927.64 188.95 o 3 7 11 -3 2140.54 2291.99 146.34 o 3 7 11 -2 178.72 148.26 69.16 < 3 7 11 -1 24.84 41.64 80.03 < 3 7 11 0 16247.90 15722.30 804.74 o 1 9 11 -3 63.79 240.10 105.71 < 1 9 11 -2 304.81 445.93 136.70 o 1 9 11 -1 3270.23 2649.97 245.93 o 1 9 11 0 3238.43 2805.10 292.62 o 1 9 11 1 1125.04 1297.55 393.13 o 3 9 11 -3 121.34 345.57 132.54 < 0 0 12 0 62789.40 63007.90 1300.47 o 0 0 12 2 119.64 78.18 65.00 < 2 0 12 -2 17.56 46.03 68.24 < 2 0 12 0 19869.10 18621.10 447.40 o 2 0 12 2 5093.21 4670.35 285.54 o 4 0 12 -2 113.11 7.40 78.64 < 4 0 12 0 4170.98 4610.45 899.40 o 0 2 12 0 11228.50 11241.50 384.74 o 0 2 12 1 8978.41 8855.79 238.76 o 0 2 12 2 41.06 -10.41 46.49 < 0 2 12 3 56.94 93.91 49.96 < 2 2 12 -3 196.52 157.98 52.74 < 2 2 12 -2 60.75 56.44 50.66 < 2 2 12 -1 262.94 320.80 55.05 o 2 2 12 0 654.26 713.23 79.56 o 2 2 12 1 15069.60 15057.10 390.32 o 2 2 12 2 5082.16 5120.93 232.64 o 2 2 12 3 352.55 439.45 188.96 < 4 2 12 -3 26.76 117.27 59.91 < 4 2 12 -2 37.41 142.26 68.47 < 4 2 12 -1 72.32 218.59 86.97 < 4 2 12 0 9.40 442.03 492.00 < 0 4 12 0 11.33 11.80 65.46 < 0 4 12 1 6911.00 7464.06 211.24 o 0 4 12 2 173.32 188.97 56.67 o 0 4 12 3 54.94 -14.57 50.89 < 2 4 12 -3 407.30 413.30 63.14 o 2 4 12 -2 28.85 96.46 52.97 < 2 4 12 -1 173.68 140.63 53.43 < 2 4 12 0 826.53 938.69 86.72 o 2 4 12 1 10242.50 10199.60 304.79 o 2 4 12 2 92.11 190.37 98.77 < 4 4 12 -3 222.35 208.17 62.91 o 4 4 12 -2 36.56 226.91 83.27 < 4 4 12 -1 0.70 72.17 103.40 < 0 6 12 0 23792.90 24626.10 611.29 o 0 6 12 1 1516.47 1456.00 109.83 o 0 6 12 2 1032.58 1108.16 95.04 o 0 6 12 3 71.25 230.61 81.65 < 2 6 12 -3 6.31 86.74 63.84 < 2 6 12 -2 6.06 5.55 57.13 < 2 6 12 -1 108.29 135.08 70.32 < 2 6 12 0 22550.10 23253.10 497.60 o 2 6 12 1 875.66 728.48 139.68 o 4 6 12 -3 5.85 42.33 83.27 < 4 6 12 -2 39.79 -25.68 89.52 < 0 8 12 0 358.07 182.49 135.77 < 0 8 12 1 320.09 289.35 105.93 < 0 8 12 2 1356.95 1522.47 239.33 o 0 8 12 3 256.30 -251.88 202.15 < 2 8 12 -3 8.62 177.65 99.93 < 2 8 12 -2 45.94 -7.17 86.74 < 2 8 12 -1 80.15 -27.76 124.90 < 1 1 13 -3 44.66 -44.87 55.28 < 1 1 13 -2 136.93 159.60 52.04 o 1 1 13 -1 240.60 249.80 63.37 o 1 1 13 0 5260.11 4926.39 179.00 o 1 1 13 1 10150.40 10245.90 265.51 o 1 1 13 2 101.86 176.49 69.16 < 1 1 13 3 8.34 42.56 81.19 < 3 1 13 -3 65.36 79.34 47.65 < 3 1 13 -2 486.42 622.38 77.48 o 3 1 13 -1 1.25 136.71 70.09 < 3 1 13 0 6445.42 5882.35 257.51 o 5 1 13 -3 237.06 173.01 81.19 < 1 3 13 -3 44.51 138.55 59.68 < 1 3 13 -2 120.82 109.18 55.05 < 1 3 13 -1 882.26 1025.38 95.28 o 1 3 13 0 55634.70 57192.80 688.03 o 1 3 13 1 84.30 105.01 65.92 < 1 3 13 2 1055.78 927.78 104.53 o 1 3 13 3 137.84 296.76 105.01 < 3 3 13 -3 185.30 268.31 64.30 o 3 3 13 -2 156.95 220.20 63.61 o 3 3 13 -1 168.49 95.53 69.85 < 3 3 13 0 23918.50 23207.30 628.83 o 3 3 13 1 1224.15 1086.40 546.43 < 5 3 13 -3 274.65 204.93 104.31 < 1 5 13 -3 48.31 29.84 72.86 < 1 5 13 -2 53.50 60.37 69.62 < 1 5 13 -1 1774.41 1795.09 136.87 o 1 5 13 0 3316.92 3502.14 192.52 o 1 5 13 1 2814.10 2936.55 175.21 o 1 5 13 2 1707.14 1848.81 185.21 o 1 5 13 3 664.95 795.82 226.42 o 3 5 13 -3 0.76 42.79 64.30 < 3 5 13 -2 44.50 176.72 73.56 < 3 5 13 -1 3771.43 3755.00 270.62 o 3 5 13 0 4992.34 4281.76 493.52 o 5 5 13 -3 40.17 246.34 308.33 < 1 7 13 -3 7.13 18.27 92.99 < 1 7 13 -2 1909.95 2044.56 192.83 o 1 7 13 -1 13520.30 13865.20 517.17 o 1 7 13 0 515.65 256.72 139.93 < 1 7 13 1 8873.03 8273.00 767.54 o 3 7 13 -3 5.16 65.23 142.26 < 3 7 13 -2 1341.53 1054.22 284.66 o 0 0 14 0 3761.68 3789.67 381.05 o 0 0 14 2 3687.74 3546.76 243.34 o 2 0 14 -2 3425.95 3127.72 253.52 o 2 0 14 0 5390.20 5654.44 307.92 o 4 0 14 -2 3772.58 3041.56 349.20 o 0 2 14 0 11407.30 11039.80 463.31 o 0 2 14 1 1905.94 1764.02 122.30 o 0 2 14 2 19.62 56.67 61.99 < 0 2 14 3 201.76 166.54 73.09 < 2 2 14 -3 14.42 9.48 65.46 < 2 2 14 -2 608.32 623.98 82.80 o 2 2 14 -1 14.17 -61.07 64.07 < 2 2 14 0 17664.90 18470.60 455.78 o 2 2 14 1 7668.15 7633.05 483.26 o 2 2 14 2 812.85 462.54 204.67 < 4 2 14 -3 151.11 146.41 83.50 < 4 2 14 -2 569.87 687.36 161.66 o 0 4 14 0 57547.40 59313.70 1161.35 o 0 4 14 1 1418.72 1579.29 139.43 o 0 4 14 2 935.28 927.58 119.33 o 0 4 14 3 1792.32 1718.60 185.43 o 2 4 14 -3 1166.05 1196.68 119.09 o 2 4 14 -2 147.26 121.90 69.39 < 2 4 14 -1 690.31 610.09 90.66 o 2 4 14 0 25970.50 26282.40 765.28 o 2 4 14 1 2811.24 3045.78 569.12 o 4 4 14 -3 487.79 376.76 145.94 < 4 4 14 -2 10.22 97.61 148.50 < 0 6 14 0 4828.44 5221.43 489.82 o 0 6 14 1 102.12 178.80 97.84 < 0 6 14 2 266.51 34.00 106.86 < 0 6 14 3 13.31 -150.81 160.30 < 2 6 14 -3 134.31 -156.36 121.43 < 2 6 14 -2 721.86 614.03 137.14 o 2 6 14 -1 3380.70 3129.50 359.41 o 1 1 15 -3 220.64 242.40 73.32 o 1 1 15 -2 322.60 352.95 80.26 o 1 1 15 -1 1093.38 1230.70 119.09 o 1 1 15 0 24.76 53.66 69.16 < 1 1 15 1 11598.30 11482.90 369.98 o 1 1 15 2 13.35 64.07 99.23 < 1 1 15 3 1.25 230.85 232.47 < 3 1 15 -3 309.80 429.28 80.26 o 3 1 15 -2 271.14 246.33 88.59 < 3 1 15 -1 115.88 284.74 157.29 < 1 3 15 -3 61.09 112.88 69.62 < 1 3 15 -2 7.35 -8.10 61.30 < 1 3 15 -1 500.14 560.86 86.04 o 1 3 15 0 19852.50 19847.00 451.89 o 1 3 15 1 401.29 329.12 123.97 < 1 3 15 2 845.83 947.49 213.92 o 3 3 15 -3 143.35 41.40 69.39 < 3 3 15 -2 30.70 32.61 120.05 < 3 3 15 -1 186.78 137.16 149.65 < 1 5 15 -3 13.77 109.64 129.76 < 1 5 15 -2 45.00 68.24 142.72 < 1 5 15 -1 413.90 488.25 161.21 o 1 5 15 0 521.17 478.99 146.17 o 3 5 15 -3 3.33 -58.29 116.35 < 0 0 16 0 80686.50 84434.20 2134.14 o 0 0 16 2 19.67 212.11 125.83 < 2 0 16 -2 92.88 111.72 112.18 < 0 2 16 0 1730.03 1644.41 205.55 o 0 2 16 1 42.64 116.12 81.65 < 0 2 16 2 140.91 594.68 136.93 o 0 2 16 3 229.44 349.03 150.34 < 2 2 16 -3 67.82 56.67 81.19 < 2 2 16 -2 493.09 443.37 108.70 o 2 2 16 -1 1063.28 613.05 148.00 o 2 2 16 0 6166.46 5669.75 488.53 o 4 2 16 -3 33.29 -89.52 163.77 < 0 4 16 0 2045.62 1534.02 581.70 < 0 4 16 1 9015.21 9014.85 823.37 o 2 4 16 -3 9.53 -43.72 143.64 < 2 4 16 -2 1177.66 1245.73 413.24 o 1 1 17 -3 357.40 398.98 161.44 < 1 1 17 -2 152.23 -98.07 150.35 < 1 1 17 -1 1307.14 1022.78 212.97 o 1 1 17 0 12287.60 12391.50 740.42 o 3 1 17 -3 140.12 -253.05 349.96 < 1 3 17 -2 786.35 967.63 260.18 o 1 3 17 -1 268.15 868.29 483.41 <